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    • 17. 发明授权
    • Method of making a ceramic composite by infiltration of a ceramic preform
    • 通过陶瓷预制件的渗透制造陶瓷复合材料的方法
    • US5628938A
    • 1997-05-13
    • US342483
    • 1994-11-18
    • D. SangeetaSvante ProchazkaKrishan L. Luthra
    • D. SangeetaSvante ProchazkaKrishan L. Luthra
    • C04B35/573B05B3/00
    • C04B35/573
    • A method for making a composite ceramic article by infiltration of a sintered ceramic preform with an infiltrate phase. The ceramic preform is made by directionally solidifying a liquid medium containing a dispersion of ceramic particles to produce a green, porous ceramic preform a plurality of interconnected lamelli that are partially separated from one another by complementary interlamellar regions, removing the solidified liquid medium and sintering the ceramic preform. This method may be used to make silicon carbide composites where a silicon carbide preform is first infiltrated with carbon to coat the lamelli of the preform, followed by infiltration of the carbon coated preform with molten silicon, whereby the molten silicon and carbon react to form silicon carbide in the interlamellar regions. The ceramic preform may also be coated with a thin, diffusion-inhibiting ceramic layer prior to infiltration in order to prevent interdiffusion between the lamelli of the preform and the infiltrate phase, and provide a plurality of mechanically weak, crack deflecting interfaces within the composite article.
    • 一种通过浸渗相的烧结陶瓷预型体的渗透制造复合陶瓷制品的方法。 通过定向凝固含有陶瓷颗粒分散体的液体介质来制造陶瓷预制件,以通过互补的层间区域彼此部分地分离出多个相互连接的薄片以形成多孔互连的薄片,除去固化的液体介质并烧结 陶瓷预制件。 该方法可用于制造碳化硅复合材料,其中碳化硅预成型件首先用碳渗透以涂覆预成型件的薄片,随后用熔融硅渗透碳涂覆的预制件,由此熔融硅和碳反应形成硅 在层间区域的碳化物。 陶瓷预制件还可以在渗透之前涂覆有薄的扩散抑制性陶瓷层,以防止预成型件的薄片与渗透相之间的相互扩散,并且在复合制品内提供多个机械弱的裂纹偏转界面 。