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11. 发明授权

US5434118A Catalytically active gel and a process for its preparation 失效
标题翻译：催化活性凝胶及其制备方法
公开(公告)号：US5434118A
公开(公告)日：1995-07-18
申请号：US134854
申请日：1993-10-12
申请人： Angela Carati , Enrico Davini , Mario G. Clerici , Giuseppe Bellussi
发明人： Angela Carati , Enrico Davini , Mario G. Clerici , Giuseppe Bellussi
IPC分类号： B01J21/08 , B01J23/08 , B01J23/14 , B01J23/22 , B01J27/18 , B01J37/00 , B01J37/03 , C01B33/16 , C07B33/00 , C07B37/02 , C07B61/00 , C07C2/10 , C07C2/58 , C07C2/66 , C07C11/02 , C07C15/02 , C07C37/60 , C07C249/04 , C07C251/44 , C07D301/19 , C07D303/04 , C07D303/14 , B01J21/12
CPC分类号： C07D301/19 , B01J21/08 , B01J37/033 , C07C2/10 , C07C2/66 , C07C249/04 , C07C37/60 , C07D303/04 , C07D303/14 , C07C2521/08 , C07C2523/08 , C07C2523/745
摘要： A catalytically active gel product is described consisting of a silica matrix which is amorphous to x-rays with uniform porosity, monomodal pore distribution and high surface area, within which one or more metal oxides possessing catalytic activity are dispersed. A process for preparing this catalytic gel is also described.
摘要翻译：描述了一种催化活性凝胶产物，其由具有均匀孔隙率，单峰孔分布和高表面积的x射线无定形的二氧化硅基质组成，其中分散了一种或多种具有催化活性的金属氧化物。还描述了制备该催化凝胶的方法。

12. 发明授权

US09522394B2 Mixed oxides of transition metals, hydrotreatment catalysts obtained therefrom and preparation process 有权
标题翻译：过渡金属的混合氧化物，由此获得的加氢处理催化剂及其制备方法
公开(公告)号：US09522394B2
公开(公告)日：2016-12-20
申请号：US14007913
申请日：2012-03-22
申请人： Angela Carati , Maria Frederica Gagliardi , Marco Massimo Ferrari , Stefano Zanardi , Marcello Marella , Michele Tomaselli
发明人： Angela Carati , Maria Frederica Gagliardi , Marco Massimo Ferrari , Stefano Zanardi , Marcello Marella , Michele Tomaselli
IPC分类号： B01J31/34 , B01J23/00 , B01J23/888 , B01J37/20 , B01J37/03 , B01J37/10 , B01J35/00 , B01J35/10 , B01J37/00 , C10G45/08 , C10G45/50
CPC分类号： B01J23/8885 , B01J23/002 , B01J31/34 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0009 , B01J37/031 , B01J37/04 , B01J37/10 , B01J37/20 , B01J2523/00 , C10G45/08 , C10G45/50 , B01J2523/31 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/41
摘要： New sulfide metal catalysts are described, containing Ni, Mo and W, an element Z selected from Si, Al and mixtures thereof, and possibly an organic residue, obtained by sulfidation of mixed oxide precursors, also new, characterized in that they comprise an amorphous phase and a wolframite isostructural crystalline phase, the crystallinity degree of said mixed oxides being higher than 0 and lower than 100%, preferably higher than 0 and lower than 70%. The catalysts of the invention are useful as hydrotreatment catalysts, and in particular as hydrodesulfurization, hydrodenitrogenation and/or hydrodearomatization catalysts.
摘要翻译：描述了新的硫化物金属催化剂，其包含Ni，Mo和W，选自Si，Al及其混合物的元素Z，以及可能的通过混合氧化物前体的硫化获得的有机残基，其也是新的，其特征在于它们包含无定形所述混合氧化物的结晶度高于0且低于100％，优选高于0且低于70％。本发明的催化剂可用作加氢处理催化剂，特别是加氢脱硫，加氢脱氮和/或加氢脱芳构化催化剂。

13. 发明申请

US20100191009A1 ORGANIC-INORGANIC HYBRID SILICATES AND METAL-SILICATES HAVING AN ORDERED STRUCTURE 有权
标题翻译：有机无机混合硅酸盐和具有订购结构的金属硅酸盐
公开(公告)号：US20100191009A1
公开(公告)日：2010-07-29
申请号：US12376704
申请日：2007-08-03
申请人： Giuseppe Bellussi , Angela Carati , Caterina Rizzo , Urbano Diaz Morales , Stefano Zanardi , Wallace O'Neil Parker , Roberto Millini
发明人： Giuseppe Bellussi , Angela Carati , Caterina Rizzo , Urbano Diaz Morales , Stefano Zanardi , Wallace O'Neil Parker , Roberto Millini
IPC分类号： C07F7/08
CPC分类号： C09C1/3081 , C01B33/44 , C01B37/00 , C01B39/00 , C01B39/02 , C01P2002/72 , C01P2002/74 , C01P2002/86 , C01P2006/17 , C07F7/1804
摘要： The present invention relates to new organic-inorganic hybrid silicates and metal-silicates called ECS, characterized by an X-ray powder diffraction pattern with reflections exclusively at angular values higher than 4.0° of 2Θ, preferably at angular values higher than 4.7°, and an ordered structure containing structural units having formula (a) wherein R is an organic group: Formula (a) and possibly containing one or more elements T selected from groups III B, IV B, V B and transition metals, with a Si/(Si+T) molar ratio in said structure higher than 0.3 and lower than or equal to 1, wherein Si is the silicon contained in the structural unit (a). A process is also described, starting from disilanes, for the preparation of these materials, which does not include the use of templates or surfactants. These materials can be used as molecular sieves, adsorbents, in the field of catalysis, in the field of electronics, in the field of sensors, in the field of nanotechnologies.
摘要翻译：本发明涉及称为ECS的新的有机 - 无机杂化硅酸盐和金属硅酸盐，其特征在于具有专门在高于4.0°的角度值为2θ，优选高于4.7°的角度值的反射的X射线粉末衍射图，以及含有具有式（a）的结构单元的有序结构，其中R是有机基团：式（a）并且可能含有选自IIIB，IVB，VB族和过渡金属的一种或多种元素T，其中Si /（Si + T）的摩尔比高于0.3且小于或等于1，其中Si是结构单元（a）中所含的硅。还描述了从二硅烷开始制备这些材料的方法，其不包括使用模板或表面活性剂。这些材料可用作纳米技术领域的电子领域，传感器领域的催化剂领域的分子筛，吸附剂。

14. 发明授权

US07419930B2 Catalytic composition for the aromatization of hydrocarbons 失效
标题翻译：用于碳氢化合物芳构化的催化组合物
公开(公告)号：US07419930B2
公开(公告)日：2008-09-02
申请号：US11585256
申请日：2006-10-24
申请人： Angela Carati , Marco Tagliabue , Carlo Perego , Roberto Millini , Stefano Amarilli , Giuseppe Terzoni
发明人： Angela Carati , Marco Tagliabue , Carlo Perego , Roberto Millini , Stefano Amarilli , Giuseppe Terzoni
IPC分类号： B01J29/06
CPC分类号： B01J29/405 , B01J29/40 , B01J29/48 , B01J2229/18 , C07C2/84 , C10G50/00 , C07C15/02
摘要： The present invention regards a catalytic composition comprising gallium, at least one element chosen in the group of the lanthanides, and a zeolite belonging to the MFI, MEL or MFI/MEL families, the crystal lattice of which is made up of silicon oxide and at least one metal oxide chosen from among aluminum oxide, boron oxide and gallium oxide. Preferably, in the catalytic compositions of the present invention a zeolite is used belonging to the MFI family characterized by crystallites which for at least 90% have diameters smaller than 500 Å and which can form agglomerates of submicron dimensions characterized by possessing at least 30% of the extrazeolitic porosity in the region of the mesopores. The catalytic compositions of the present invention can, in addition, contain rhenium. These catalytic compositions are useful in processes of aromatization of hydrocarbons containing from 3 to 6 carbon atoms, preferably, hydrocarbon mixtures containing olefins.
摘要翻译：本发明涉及包含镓，至少一种选自镧系元素的元素和属于MFI，MEL或MFI / MEL族的沸石的催化组合物，其晶格由氧化硅和选自氧化铝，氧化硼和氧化镓中的至少一种金属氧化物。优选地，在本发明的催化组合物中，属于MFI族的沸石，其特征在于微晶，其至少90％的直径小于500，并且可以形成亚微米尺度的附聚物，其特征在于具有至少30％中孔区域中的超沸石孔隙度。另外，本发明的催化剂组合物可以含有铼。这些催化组合物可用于含有3至6个碳原子的烃，优选含有烯烃的烃混合物的芳构化方法。

15. 发明授权

US07018595B2 Process for preparing bound zeolites 有权
公开(公告)号：US07018595B2
公开(公告)日：2006-03-28
申请号：US10315022
申请日：2002-12-10
申请人： Angela Carati , Giuseppe Bellussi , Maria Angela Mantegazza , Giudo Petrini
发明人： Angela Carati , Giuseppe Bellussi , Maria Angela Mantegazza , Giudo Petrini
IPC分类号： C01B33/26 , C01B37/00
CPC分类号： C01B37/005 , B01J29/06 , B01J29/40 , B01J2229/32 , C01B37/02 , C01B39/40 , Y10S423/22 , Y10S423/29
摘要： A process is described for the preparation of zeolitic catalysts in the form of microspheres, comprising zeolite and oligomeric silica, characterized by a high mechanical resistance. The process consists in subjecting to rapid drying the suspension, to which tetra-alkylorthosilicate is optionally added, resulting from the synthesis of zeolite by hydrothermal treatment at autogenous pressure of the reagent mixture containing tetra-alkylammoniumhydroxide as templating agent, and subjecting the product resulting from the drying to calcination.

16. 发明授权

US06495733B1 Superacid catalyst for the hydroisomerization of n-paraffins 失效
标题翻译：用于正链烷烃加氢异构化的超强酸催化剂
公开(公告)号：US06495733B1
公开(公告)日：2002-12-17
申请号：US09673644
申请日：2000-10-31
申请人： Stefano Peratello , Angela Carati
发明人： Stefano Peratello , Angela Carati
IPC分类号： B01J27053
CPC分类号： B01J37/033 , B01J27/053 , C07C5/2791 , C07C9/00
摘要： A superacid catalyst comprising: zirconium oxide on whose surface sulfate groups are present, in a quality corresponding to total coverage of the surface of the zirconium oxide by means of a monolayer of these sulfate groups, optionally containing a noble metal in a quantity ranging from 0.1 to 3% by weight, with a porosity ranging from 0.1 to 0.30 cm3/g, consisting of at least 70% of pores with a diameter ranging from 1 to 4 nm, prepared by a process which comprises: (a) hydrolyzing derivate of zirconium in a basic medium in the presence of a tetra-alkylammonium hydroxide (TAA), sulfuric acid and acetylacetone (AcAc); (b) drying the product of step (a) and calcining the dried material at a temperature ranging from 250 to 650° C. (c) optionally treating the product resulting from step (b) with an aqueous solution of a compound of a noble metal, and drying and calcining the treated product.
摘要翻译：一种超酸催化剂，其包含：其表面硫酸基团存在的氧化锆，其质量对应于这些硫酸盐基团的单层的氧化锆表面的总覆盖度，任选地含有量为0.1的贵金属至3重量％，孔隙率为0.1至0.30cm 3 / g，由至少70％的直径范围为1至4nm的孔组成，该方法包括：（a）水解锆衍生物在碱性介质中，在四烷基氢氧化铵（TAA），硫酸和乙酰丙酮（AcAc）的存在下;（b）干燥步骤（a）的产物并在250至650℃的温度范围内煅烧干燥的材料（c）任选地用贵金属化合物的水溶液处理由步骤（b）得到的产物，并干燥并煅烧处理过的产品。

17. 发明授权

US5908968A Difunctional catalyst effective in wax hydroisomerization and process for preparing it 失效
标题翻译：在蜡加氢异构化中有效的双官能催化剂及其制备方法
公开(公告)号：US5908968A
公开(公告)日：1999-06-01
申请号：US975276
申请日：1997-11-20
申请人： Angela Carati , Cristina Flego , Vincenzo Calemma
发明人： Angela Carati , Cristina Flego , Vincenzo Calemma
IPC分类号： B01J29/86 , C10G45/64 , C07C5/13
CPC分类号： B01J29/86 , C10G45/64
摘要： Process for the hydroisomerization of n-paraffins in the presence of a difunctional catalyst which comprises:(a) a porous crystalline material isostructural with beta-zeolite selected from boro-silicate (BOR-B) and boro-alumino-silicate (Al-BOR-B) in which the molar SiO.sub.2 :Al.sub.2 O.sub.3 ratio is higher than 300:1;(b) one or more metal(s) belonging to Group VIIIA, selected from platinum and palladium, in an amount comprised within the range of from 0.05 to 5% by weight.
摘要翻译：在双官能催化剂存在下正构烷烃的加氢异构化方法，其包括：（a）使用选自硼硅酸盐（BOR-B）和硼铝硅酸盐（Al-BOR）的β-沸石同构结构的多孔结晶材料 -B），其中SiO 2：Al 2 O 3摩尔比高于300:1; （b）选自铂和钯的属于VIIIA族的一种或多种金属，其量为0.05-5重量％。

18. 发明授权

US09765266B2 Catalytic system and process for the hydroconversion of heavy oil products 有权
公开(公告)号：US09765266B2
公开(公告)日：2017-09-19
申请号：US12996782
申请日：2009-06-08
申请人： Giuseppe Bellussi , Giacomo Rispoli , Angela Carati
发明人： Giuseppe Bellussi , Giacomo Rispoli , Angela Carati
IPC分类号： C10G45/04 , B01J29/04 , B01J23/16 , C10G47/02 , C10G47/26 , B01J23/882 , B01J23/883 , B01J27/051 , B01J29/06 , B01J29/072 , B01J29/16 , B01J29/70 , B01J29/76 , B01J35/00 , B01J37/20 , C10G45/08 , C10G45/12 , C10G45/46 , C10G45/50 , C10G45/54 , C10G47/20
CPC分类号： C10G45/04 , B01J23/882 , B01J23/883 , B01J27/051 , B01J29/041 , B01J29/061 , B01J29/072 , B01J29/166 , B01J29/7007 , B01J29/7615 , B01J35/0006 , B01J37/20 , C10G45/08 , C10G45/12 , C10G45/46 , C10G45/50 , C10G45/54 , C10G47/20 , C10G2300/1003 , C10G2300/1011 , C10G2300/1033 , C10G2300/1074 , Y02P30/20
摘要： Catalytic system which can be used in processes for the hydroconversion of heavy oils by means of hydrotreatment in slurry phase, characterized in that it comprises: a catalyst, having the function of hydrogenating agent, containing MoS2 or WS2 or mixtures thereof in lamellar form or an oil-soluble precursor thereof; a co-catalyst, having nanometric or micronic particle-sizes, selected from cracking and/or denitrogenation catalysts. The co-catalyst preferably consists of zeolites having small-sized crystals and with a low aggregation degree between the primary particles, and/or oxides or sulfides or precursors of sulfides of Ni and/or Co in a mixture with Mo and/or W.

19. 发明申请

US20140323291A1 MIXED OXIDES OF TRANSITION METALS, HYDROTREATMENT CATALYSTS OBTAINED THEREFROM AND PREPARATION PROCESS 有权
标题翻译：过渡金属的混合氧化物，由其获得的加氢催化剂和制备方法
公开(公告)号：US20140323291A1
公开(公告)日：2014-10-30
申请号：US14007913
申请日：2012-03-22
申请人： Angela Carati , Maria Frederica Gagliardi , Marco Massimo Ferrari , Stefano Zanardi , Marcello Marella , Michele Tomaselli
发明人： Angela Carati , Maria Frederica Gagliardi , Marco Massimo Ferrari , Stefano Zanardi , Marcello Marella , Michele Tomaselli
IPC分类号： B01J31/34
CPC分类号： B01J23/8885 , B01J23/002 , B01J31/34 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J37/0009 , B01J37/031 , B01J37/04 , B01J37/10 , B01J37/20 , B01J2523/00 , C10G45/08 , C10G45/50 , B01J2523/31 , B01J2523/68 , B01J2523/69 , B01J2523/847 , B01J2523/41
摘要： New sulfide metal catalysts are described, containing Ni, Mo and W, an element Z selected from Si, Al and mixtures thereof, and possibly an organic residue, obtained by sulfidation of mixed oxide precursors, also new, characterized in that they comprise an amorphous phase and a wolframite iso structural crystalline phase, the crystallinity degree of said mixed oxides being higher than 0 and lower than 100%, preferably higher than 0 and lower than 70%. The catalysts of the invention are useful as hydrotreatment catalysts, and in particular as hydrodesulfurization, hydrodenitrogenation and/or hydrodearomatization catalysts.
摘要翻译：描述了新的硫化物金属催化剂，其包含Ni，Mo和W，选自Si，Al及其混合物的元素Z，以及可能的通过混合氧化物前体的硫化获得的有机残基，其也是新的，其特征在于它们包含无定形所述混合氧化物的结晶度高于0且低于100％，优选高于0且低于70％。本发明的催化剂可用作加氢处理催化剂，特别是加氢脱硫，加氢脱氮和/或加氢脱芳构化催化剂。

20. 发明申请

US20120059181A1 HYBRID, ORGANIC-INORGANIC, CRYSTALLINE, POROUS SILICATES AND METAL-SILICATES 有权
标题翻译：混合有机无机，结晶，多孔硅酸盐和金属硅酸盐
公开(公告)号：US20120059181A1
公开(公告)日：2012-03-08
申请号：US13254999
申请日：2010-02-25
申请人： Giuseppe Bellussi , Angela Carati , Mariangela Cozzolino , Caterina Rizzo , Stefano Zanardi
发明人： Giuseppe Bellussi , Angela Carati , Mariangela Cozzolino , Caterina Rizzo , Stefano Zanardi
IPC分类号： C07F7/08 , C07F9/08 , C07F15/02
CPC分类号： C01B37/00 , C01P2002/72
摘要： The present invention relates to new hybrid, organic-inorganic hybrid silicates and metal-silicates characterized by a crystalline structure containing structural units having formula (a), wherein R is an organic group possibly containing one or more element T selected from Group IIIB, IVB, VB and from transition metals. A process starting from cyclic trisilanes for the preparation of said materials, is also described. These materials can be used as molecular sieves, adsorbents, in the field of catalysis, in the field of electronics, in the field of sensors, in the area of nanotechnology.
摘要翻译：本发明涉及新型混合有机 - 无机杂化硅酸盐和金属硅酸盐，其特征在于含有具有式（a）的结构单元的晶体结构，其中R是可能含有一种或多种选自IIIB族，IVB族元素的有机基团，VB和过渡金属。还描述了从用于制备所述材料的环状三硅烷开始的方法。这些材料可用作催化领域的分子筛，吸附剂，电子领域，传感器领域，纳米技术领域。

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