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11. 发明授权

US08114372B2 Hierarchical mesoporous carbon, method of manufacturing the same, and fuel cell using the same 有权
标题翻译：分层介孔碳，其制造方法和使用其的燃料电池
公开(公告)号：US08114372B2
公开(公告)日：2012-02-14
申请号：US12168284
申请日：2008-07-07
申请人： Chan-ho Pak , Hyuk Chang , Ji-man Kim
发明人： Chan-ho Pak , Hyuk Chang , Ji-man Kim
IPC分类号： C01B31/00 , B01J19/08 , H01M8/10 , B01J21/18
CPC分类号： B01J21/18 , B01J29/0308 , B01J35/1066 , B01J37/0018 , C01B32/00 , H01M4/9016 , H01M4/9083 , H01M8/1011 , Y02E60/523 , Y02P70/56
摘要： A hierarchical mesoporous carbon is provided in which a total volume of mesopores of the hierarchical mesoporous carbon is 80% or greater of a total volume of pores of the hierarchical mesoporous carbon; a volume of mesopores with a average diameter greater than 20 nm and no greater than 50 nm is 3% or greater of the total volume of the pores; and a volume of mesopores with a average diameter greater than 2 nm and no greater than 10 nm is 65% or greater of the total volume of the pores. The hierarchical mesoporous carbon, which also contains macropores, has an optimized mesoporous distribution characteristic, and has an increased total volume of pores, thereby having a significantly improved catalytic activity when used as a catalyst support. When such a supported catalyst including the hierarchical mesoporous carbon as a support is used in a fuel cell, supply of fuel and transporting of byproducts are facilitated.
摘要翻译：提供了分级介孔碳，其中分层介孔碳的介孔的总体积为分级介孔碳的总体积的80％或更大; 平均直径大于20nm且不大于50nm的介孔的体积为孔的总体积的3％或更大; 并且平均直径大于2nm且不大于10nm的体积的介孔为孔的总体积的65％或更大。还含有大孔的层状中孔碳具有优化的介孔分布特征，并且具有增加的孔体积，从而当用作催化剂载体时具有显着改善的催化活性。当在燃料电池中使用包含分层介孔碳作为载体的这种负载型催化剂时，燃料的供给和副产物的输送变得容易。

12. 发明申请

US20080107956A1 CATALYST USED TO FORM FUEL CELL AND FUEL CELL USING THE SAME 审中-公开
标题翻译：用于形成燃料电池和燃料电池的催化剂
公开(公告)号：US20080107956A1
公开(公告)日：2008-05-08
申请号：US11690341
申请日：2007-03-23
申请人： Dae-jong Yoo , Chan-ho Pak , Hyuk Chang , Sang-hoon Joo
发明人： Dae-jong Yoo , Chan-ho Pak , Hyuk Chang , Sang-hoon Joo
IPC分类号： H01M4/92 , B01J23/14 , B01J23/42 , B01J23/44 , B01J23/46 , B01J23/52 , H01M4/88 , H01M4/90
CPC分类号： H01M4/92 , H01M4/8657 , H01M4/8885
摘要： A catalyst, a method of preparing the catalyst, and a fuel cell using the catalyst. The catalyst includes a catalyst metal particle, and a porous coating layer of a conductive ceramic material disposed on the surface of the catalyst metal particle. The catalyst has a methanol tolerance index of 80%, or more, a smaller particle size than a commercially available Pt-black catalyst manufactured through a polyol process. The catalyst can include a PT catalyst metal particle that is surface treated, or coated, with a conductive ceramic ATO. The catalyst has an excellent ORR activity in the presence of methanol, and an enhanced tolerance with respect to methanol. A fuel cell, including an electrode manufactured using the catalyst, has a high energy density and a high fuel efficiency.
摘要翻译：催化剂，制备催化剂的方法和使用该催化剂的燃料电池。催化剂包括催化剂金属颗粒和设置在催化剂金属颗粒表面上的导电陶瓷材料的多孔涂层。与通过多元醇法制造的市售Pt-black催化剂相比，催化剂的甲醇耐受指数为80％以上，粒径小。催化剂可以包括用导电陶瓷ATO进行表面处理或涂覆的PT催化剂金属颗粒。该催化剂在甲醇存在下具有优异的ORR活性，并且相对于甲醇具有增强的耐受性。包括使用该催化剂制造的电极的燃料电池具有高能量密度和高燃料效率。

13. 发明申请

US20060116284A1 Mesoporous carbon composite containing carbon nanotube 失效
公开(公告)号：US20060116284A1
公开(公告)日：2006-06-01
申请号：US11265177
申请日：2005-11-03
申请人： Chan-ho Pak , Hyuk Chang , Dae-jong Yoo , Ji-man Kim
发明人： Chan-ho Pak , Hyuk Chang , Dae-jong Yoo , Ji-man Kim
IPC分类号： B01J21/18
CPC分类号： B01J21/185 , B01J23/42 , B01J29/0308 , B01J35/10 , B01J35/1061 , B82Y30/00 , C01B33/124 , C01B37/02 , C04B35/14 , C04B35/521 , C04B35/524 , C04B35/80 , C04B35/83 , C04B38/00 , C04B38/0045 , C04B38/045 , C04B2111/0081 , C04B2111/00853 , C04B2235/3201 , C04B2235/3217 , C04B2235/483 , C04B2235/5288 , C04B2235/6028 , H01M4/8673 , H01M4/92 , H01M4/926 , H01M2008/1095 , C04B14/026 , C04B28/24 , C04B38/0054 , C04B28/26 , C04B38/0022 , C04B38/0064
摘要： Provided are a CNT-mesoporous silica composite, a CNT-mesoporous carbon composite, a supported catalyst using the CNT-mesoporous carbon composite as a support, and a fuel cell using the supported catalyst as the anode, cathode, or both anode and cathode. The CNT-mesoporous carbon composite is prepared using the CNT-mesoporous silica composite. The CNT-mesoporous carbon composite has a high electrical conductivity due to the CNTs contained therein, and thus, when the CNT-mesoporous carbon composite is used in an electrode of a fuel cell, the fuel cell has a remarkably improved performance relative to the conventional catalyst support which does not contain CNTs.

14. 发明授权

US08791043B2 Ordered mesoporous carbon composite catalyst, method of manufacturing the same, and fuel cell using the same 有权
标题翻译：有序介孔碳复合催化剂，其制造方法和使用其的燃料电池
公开(公告)号：US08791043B2
公开(公告)日：2014-07-29
申请号：US12650750
申请日：2009-12-31
申请人： Chan-ho Pak , Hyuk Chang , Ji-man Kim , Jeong-kuk Shon
发明人： Chan-ho Pak , Hyuk Chang , Ji-man Kim , Jeong-kuk Shon
IPC分类号： B01J23/16 , B01J23/44 , B01J23/46 , B01J23/75 , B01J23/745 , B01J23/755 , H01M4/36 , C01B31/00
CPC分类号： H01M4/90 , H01M4/8814 , H01M4/8825 , H01M4/9083 , H01M4/926 , H01M8/1004 , Y02P70/56
摘要： An ordered mesoporous carbon (OMC) composite catalyst includes an OMC; and metal particles and at least one component selected from a group consisting of nitrogen and sulfur included in the OMC. The ordered mesoporous carbon composite catalyst may be formed by impregnating an ordered mesoporous silica with a mixture of at least one selected from the group consisting of a nitrogen-containing carbon precursor, and a sulfur-containing carbon precursor, a metal precursor, and a solvent; drying and heat-treating the impregnated OMS; carbonizing the dried and heat-treated OMS to obtain a carbon-OMS composite; and removing the OMS from the carbon-OMS composite. A fuel cell may contain the OMC composite catalyst.
摘要翻译：有序介孔碳（OMC）复合催化剂包括OMC; 和金属颗粒和至少一种选自包含在OMC中的氮和硫的组分。有序介孔碳复合催化剂可以通过用选自含氮碳前体和含硫碳前体，金属前体和溶剂中的至少一种的混合物浸渍有序介孔二氧化硅来形成 ; 干燥和热处理浸渍的OMS; 对干燥和热处理的OMS进行碳化以获得碳-OMS复合材料; 并从碳-OMS复合材料中除去OMS。燃料电池可以包含OMC复合催化剂。

15. 发明授权

US08083905B2 Carbon nanotubes for fuel cells, method for manufacturing the same, and fuel cell using the same 有权
标题翻译：燃料电池用碳纳米管及其制造方法以及使用该碳纳米管的燃料电池
公开(公告)号：US08083905B2
公开(公告)日：2011-12-27
申请号：US12511468
申请日：2009-07-29
申请人： Won-bong Choi , Jae-uk Chu , Chan-ho Pak , Hyuk Chang
发明人： Won-bong Choi , Jae-uk Chu , Chan-ho Pak , Hyuk Chang
IPC分类号： C01B31/00 , D01F9/12
CPC分类号： H01M4/8605 , B82Y30/00 , B82Y40/00 , C01B32/162 , H01M4/9083 , H01M4/926 , H01M2008/1095 , Y10S977/70 , Y10S977/701 , Y10S977/72 , Y10S977/743 , Y10S977/843 , Y10S977/847
摘要： The internal and external walls of the carbon nanotubes are doped with nano-sized metallic catalyst particles uniformly to a degree of 0.3-5 mg /cm2. The carbon nanotubes are grown over a carbon substrate using chemical vapor deposition or plasma enhanced chemical vapor deposition. Since the carbon nanotubes have a large specific surface area, and metallic catalyst particles are uniformly distributed over the internal and external walls thereof, the reaction efficiency in an electrode becomes maximal when the carbon nanotubes are used for the electrode of a fuel cell. The carbon nanotubes fabricated using the method can be applied to form a large electrode. The carbon nanotubes grown over the carbon substrate can be readily applied to an electrode of a fuel cell, providing economical advantages and simplifying the overall electrode manufacturing process. A fuel cell using as the carbon nanotubes for its electrode provides improved performance.
摘要翻译：碳纳米管的内壁和外壁均匀掺杂有纳米尺寸的金属催化剂颗粒至0.3-5mg / cm2的程度。使用化学气相沉积或等离子体增强化学气相沉积在碳衬底上生长碳纳米管。由于碳纳米管具有大的比表面积，并且金属催化剂颗粒均匀地分布在其内壁和外壁上，所以当将碳纳米管用于燃料电池的电极时，电极中的反应效率最大。使用该方法制造的碳纳米管可以应用于形成大电极。生长在碳基板上的碳纳米管可以容易地应用于燃料电池的电极，提供经济的优点并简化整个电极的制造过程。使用作为其电极的碳纳米管的燃料电池提供改进的性能。

16. 发明授权

US07994088B2 Supported catalyst, method of preparing the same, and fuel cell using the same 有权
标题翻译：负载催化剂，其制备方法和使用其的燃料电池
公开(公告)号：US07994088B2
公开(公告)日：2011-08-09
申请号：US11708600
申请日：2007-02-21
申请人： Chan-ho Pak , Dae-jong Yoo , Sang-hoon Joo , Hyuk Chang , Seol-ah Lee
发明人： Chan-ho Pak , Dae-jong Yoo , Sang-hoon Joo , Hyuk Chang , Seol-ah Lee
IPC分类号： H01M4/88 , B01J21/18 , B01J23/00 , B01J23/40 , B01J23/74 , H01M4/02 , H01M4/36 , H01M4/92 , H01M4/94 , H01M4/90
CPC分类号： H01M4/926 , H01M4/8657 , H01M4/8814 , H01M4/885 , H01M4/92 , H01M4/921 , H01M8/1007 , H01M8/1011 , Y02E60/523 , Y02P70/56
摘要： A method of preparing a supported catalyst, a supported catalyst prepared by the method, and a fuel cell using the supported catalyst. In particular, a method of preparing a supported catalyst by preparing a primary supported catalyst containing catalytic metal particles that are obtained by a primary gas phase reduction reaction of a portion of the final loading amount of a catalytic metal, and reducing the remaining portion of the catalytic metal by a secondary liquid phase reduction reaction using the primary supported catalyst. The supported catalyst contains catalytic metal particles having a very small average particle size, which are uniformly distributed on a carbon support at a high concentration, and thus exhibits maximal catalyst activity. A fuel cell produced using the supported catalyst has improved efficiency.
摘要翻译：制备载体催化剂的方法，通过该方法制备的负载催化剂和使用负载型催化剂的燃料电池。特别是制备负载型催化剂的方法，该方法是通过制备含有催化金属颗粒的主载体催化剂，所述催化剂金属颗粒是通过催化金属的最终负载量的一部分的一次气相还原反应获得的，并且还原剩余部分催化金属通过使用主要负载催化剂的二次液相还原反应。载体催化剂含有平均粒径非常小的催化金属颗粒，其以高浓度均匀分布在碳载体上，因此表现出最大的催化剂活性。使用负载型催化剂制造的燃料电池具有提高的效率。

17. 发明授权

US07732094B2 Mesoporous carbon composite, method of preparing the same, and fuel cell using the mesoporous carbon composite 失效
标题翻译：介孔碳复合材料，其制备方法和使用介孔碳复合材料的燃料电池
公开(公告)号：US07732094B2
公开(公告)日：2010-06-08
申请号：US11443165
申请日：2006-05-31
申请人： Chan-ho Pak , Yeong-suk Choi , Hyuk Chang , Sang Hoon Joo
发明人： Chan-ho Pak , Yeong-suk Choi , Hyuk Chang , Sang Hoon Joo
IPC分类号： H01M4/60 , H01M4/62 , H01M4/88 , B01J31/00
CPC分类号： B01J21/18 , B01J23/42 , B01J29/0308 , B01J35/10 , B01J35/1023 , B01J35/1047 , B01J35/1061 , B01J37/0018 , B01J37/084 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M8/08 , H01M8/086 , H01M8/10 , H01M8/1007 , H01M8/1011 , Y02E60/523 , Y02P70/56
摘要： A mesoporous carbon composite includes mesoporous carbon having mesopores; a conductive polymer coated on only an outer surface of the mesoporous carbon; and an organic electrolyte. The mesoporous carbon composite may be prepared by impregnating an ordered mesoporous silica (OMS) with a mixture comprising a carbon precursor, an acid, and a solvent; heat-treating and carbonizing the impregnated OMS to form an OMS-carbon composite; mixing the OMS-carbon composite with a monomer that forms a conductive polymer and a solvent to provide a surface of the OMS-carbon composite with the monomer; polymerizing the monomer to obtain a conductive polymer-coated OMS-carbon composite; removing the OMS from the composite to obtain a conductive polymer-coated mesoporous carbon; and doping the conductive polymer-coated mesoporous carbon with an organic electrolyte. A supported catalyst and a fuel cell include the mesoporous carbon composite.
摘要翻译：介孔碳复合材料包括具有中孔的中孔碳; 只涂覆在介孔碳外表面上的导电聚合物; 和有机电解质。介孔碳复合材料可以通过用含有碳前体，酸和溶剂的混合物浸渍有序介孔二氧化硅（OMS）来制备; 对浸渍的OMS进行热处理和碳化以形成OMS-碳复合材料; 将OMS-碳复合物与形成导电聚合物和溶剂的单体混合以提供OMS-碳复合材料与单体的表面; 聚合单体以获得导电聚合物涂覆的OMS-碳复合材料; 从复合材料中除去OMS以获得导电聚合物涂覆的介孔碳; 并用有机电解质掺杂导电聚合物涂覆的中孔碳。载体催化剂和燃料电池包括介孔碳复合材料。

18. 发明授权

US07670582B2 Mesoporous carbon and method of producing the same 有权
标题翻译：介孔碳及其制备方法
公开(公告)号：US07670582B2
公开(公告)日：2010-03-02
申请号：US11434113
申请日：2006-05-16
申请人： Chan-ho Pak , Sang-hoon Joo , Hyuk Chang , Ji-man Kim , Hyung-ik Lee
发明人： Chan-ho Pak , Sang-hoon Joo , Hyuk Chang , Ji-man Kim , Hyung-ik Lee
IPC分类号： C01B31/00 , B01J21/18 , H01M4/96
CPC分类号： B01J21/18 , B01J23/42 , B01J37/0018 , B01J37/084 , C01B32/00 , H01M4/8605 , H01M4/8807 , H01M4/885 , H01M4/8882 , H01M4/9083 , H01M4/92 , H01M4/921 , H01M4/926 , H01M4/96 , H01M8/086 , H01M8/1011 , H01M2008/1095 , Y02E60/523 , Y02P70/56
摘要： Provided are a mesoporous carbon and a method of preparing the same, where the mesoporous carbon is prepared using phenanthrene as a carbon source and a mesoporous silica as a template. The mesoporous carbon has a significantly low plane resistance, which can be obtained without sacrificing other physical properties, and thus obtains a high conductivity and effectively transfers electrical energy. Accordingly, a fuel cell electrode or a fuel cell which is produced using the mesoporous carbon as a conductive material has high efficiency. Furthermore, the mesoporous carbon may be used in various electrochemical devices as a conductive material.
摘要翻译：提供介孔碳及其制备方法，其中介孔碳是使用菲作为碳源和介孔二氧化硅作为模板制备的。中孔碳具有显着低的平面电阻，其可以在不牺牲其他物理性能的情况下获得，从而获得高导电性并有效转移电能。因此，使用介孔碳作为导电材料制造的燃料电池电极或燃料电池具有高效率。此外，介孔碳可以用作各种电化学装置中的导电材料。

19. 发明授权

US07518045B2 Method of preparing carbon nanocages 失效
标题翻译：碳纳米线的制备方法
公开(公告)号：US07518045B2
公开(公告)日：2009-04-14
申请号：US11140979
申请日：2005-06-01
申请人： Chan-ho Pak , Hyuk Chang , Jian Nong Wang
发明人： Chan-ho Pak , Hyuk Chang , Jian Nong Wang
IPC分类号： C01B31/04
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/18 , Y10S977/843
摘要： The present invention provides a simple method of mass producing high purity carbon nanocages. The method of preparing carbon nanocages comprises introducing an inert gas into a reactor equipped with a spray nozzle and raising the temperature of the reactor to a pyrolysis temperature of a catalyst compound. The method further comprises spraying a reactant including the catalyst compound and a carbon-containing compound into the reactor through the spray nozzle, wherein the ratio of a space velocity of the inert gas to a space velocity of the reactant is 100 or more.
摘要翻译：本发明提供了大规模生产高纯碳纳米笼的简单方法。制备碳纳米笼的方法包括将惰性气体引入装有喷嘴的反应器中，并将反应器的温度升高至催化剂化合物的热解温度。该方法还包括通过喷嘴将包含催化剂化合物和含碳化合物的反应物喷射到反应器中，其中惰性气体的空速与反应物的空速之比为100以上。

20. 发明申请

US20070269699A1 Catalyst coated membrane, membrane electrode assembly containing the same, method of producing the same, and fuel cell including the membrane electrode assembly 审中-公开
标题翻译：催化剂涂膜，含有其的膜电极组件，其制造方法和包括膜电极组件的燃料电池
公开(公告)号：US20070269699A1
公开(公告)日：2007-11-22
申请号：US11708599
申请日：2007-02-21
申请人： Chan-ho Pak , Seol-ah Lee , Hyuk Chang , Ji-rae Kim , Dae-jong Yoo , Sang-hoon Joo
发明人： Chan-ho Pak , Seol-ah Lee , Hyuk Chang , Ji-rae Kim , Dae-jong Yoo , Sang-hoon Joo
IPC分类号： H01M8/10
CPC分类号： H01M4/921 , H01M4/8657 , H01M4/8668 , H01M4/881 , H01M4/8814 , H01M4/8828 , H01M4/8875 , H01M4/8882 , H01M4/926 , H01M4/928
摘要： A catalyst coated membrane (CCM) comprising an anode catalyst layer having a first catalyst layer composed of a non-supported catalyst and a second catalyst layer composed of a supported catalyst, a cathode catalyst layer composed of a supported catalyst, and an electrolyte membrane interposed between the anode catalyst layer and a cathode catalyst layer, the first catalyst layer of the anode catalyst layer being disposed adjacent to the electrolyte membrane; a membrane electrode assembly (MEA) comprising the catalyst coated membrane; a method of preparing the membrane electrode assembly; and a fuel cell comprising the membrane electrode assembly, are provided. The CCM, which comprises a bilayered anode catalyst layer including the first catalyst layer composed of a non-supported catalyst and the second catalyst layer composed of a supported catalyst, exhibits reduced electrical resistance and interfacial resistance, and has increased catalyst availability. The use of the CCM and an MEA having the same results in a decrease in the interfacial resistance between the electrodes and the electrolyte membrane, a decrease in the amount of the catalyst used in the electrode catalyst layer, and a decrease in the thickness deviation in the electrode layers. The fuel cell employing the MEA exhibits maximal activity of the supported catalyst, and has improved cell characteristics such as output voltage, output density, efficiency, and the like.
摘要翻译：一种催化剂涂覆膜（CCM），其包括具有由非负载型催化剂构成的第一催化剂层和由负载型催化剂构成的第二催化剂层的阳极催化剂层，由负载型催化剂构成的阴极催化剂层和插入在阳极催化剂层和阴极催化剂层之间，阳极催化剂层的第一催化剂层设置在电解质膜附近; 包含所述催化剂涂覆膜的膜电极组件（MEA）一种制备膜电极组件的方法; 以及包括膜电极组件的燃料电池。包含由非载体催化剂构成的第一催化剂层和由负载型催化剂构成的第二催化剂层的双层阳极催化剂层的CCM显示出降低的电阻和界面电阻，并且提高了催化剂的可利用性。使用具有相同结果的CCM和MEA在电极和电解质膜之间的界面电阻降低，电极催化剂层中使用的催化剂量的减少以及厚度偏差的降低电极层。使用MEA的燃料电池显示出负载型催化剂的最大活性，并且具有改善的电池特性，例如输出电压，输出密度，效率等。

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