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11. 发明申请

US20120172645A1 Olefin Oligomerization catalysts and Methods of Making and Using Same 审中-公开
标题翻译：烯烃低聚催化剂及其制备和使用方法
公开(公告)号：US20120172645A1
公开(公告)日：2012-07-05
申请号：US12980457
申请日：2010-12-29
申请人： Orson L. Sydora
发明人： Orson L. Sydora
IPC分类号： C07C2/34 , B01J31/14 , B01J37/08 , C07C2/26
CPC分类号： C07F9/46 , B01J31/143 , B01J31/189 , B01J2231/20 , B01J2531/62 , C07C2/36 , C07C2531/24 , C07F11/00 , Y02P20/52 , C07C11/02 , C07C11/107
摘要： This disclosure provides for a process for preparing a catalyst system comprising a) contacting a metal compound, a diphosphino aminyl ligand metal complex, and a metal alkyl for a time period to form a mixture; and b) aging the mixture. The disclosure also provides for olefin oligomerization process comprising: a) contacting i) a metal compound, ii) a diphosphino aminyl ligand, and iii) a metal alkyl to form a mixture; b) aging the mixture; c) contacting the aged mixture with an olefin monomer; and d) forming an olefin oligomer product.
摘要翻译：本公开内容提供了一种制备催化剂体系的方法，包括：a）使金属化合物，二膦基乙炔基配体金属络合物和金属烷基接触一段时间以形成混合物; 和b）老化混合物。本公开还提供了烯烃低聚方法，其包括：a）使i）金属化合物，ii）二膦基乙烯基配体和iii）金属烷基接触以形成混合物; b）老化混合物; c）使老化的混合物与烯烃单体接触; 和d）形成烯烃低聚物产物。

12. 发明授权

US08680003B2 Phosphinyl amidine compounds, metal complexes, catalyst systems, and their use to oligomerize or polymerize olefins 有权
标题翻译：磷化脒化合物，金属络合物，催化剂体系及其烯烃低聚或聚合的用途
公开(公告)号：US08680003B2
公开(公告)日：2014-03-25
申请号：US13519825
申请日：2010-12-29
申请人： Orson L. Sydora , Michael Carney , Brooke L. Small , Jeffery C. Gee , Steven Hutchison
发明人： Orson L. Sydora , Michael Carney , Brooke L. Small , Jeffery C. Gee , Steven Hutchison
IPC分类号： B01J31/18 , C07D265/30 , C07D233/54 , C07F9/28
CPC分类号： C07F11/005 , B01J31/143 , B01J31/18 , B01J31/188 , B01J31/189 , B01J31/2295 , B01J2231/20 , B01J2531/62 , B01J2531/824 , B01J2531/828 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07C2/32 , C07C2/36 , C07C2531/14 , C07C2531/24 , C07D233/54 , C07D265/30 , C07F9/28 , C07F9/46 , C07F9/5004 , C07F9/5022 , C07F9/6533 , C07F9/6539 , C07F11/00 , C07F19/005 , C08F4/78 , C08F10/00 , C08F110/02 , C08F210/16 , C08G61/04 , C08F4/69068 , C08F210/14
摘要： N2-phosphinyl amidine compounds, N2-phosphinyl amidinates, N2-phosphinyl amidine metal salt complexes, N2-phosphinyl amidinate metal salt complexes are described. Methods for making N2-phosphinyl amidine compounds, N2-phosphinyl amidinates, N2-phosphinyl amidine metal salt complexes, and N2-phosphinyl amidinate metal salt complexes are also disclosed. Catalyst systems utilizing the N2-phosphinyl amidine metal salt complexes and N2-phosphinyl amidinate metal salt complexes are also disclosed along with the use of the N2-phosphinyl amidine compounds, N2-phosphinyl amidinates, N2-phosphinyl amidine metal salt complexes, and N2-phosphinyl amidinate metal salt complexes for the oligomerization and/or polymerization of olefins.
摘要翻译：描述了N2-氧膦基脒化合物，N2-氧膦基脒基化物，N2-氧膦基脒金属盐络合物，N2-氧膦基脒基金属盐络合物。还公开了制备N 2 - 氧膦基脒化合物，N 2 - 氧膦基脒基，N 2 - 氧膦基脒金属盐络合物和N 2 - 氧膦酰基脒基金属盐络合物的方法。还公开了使用N 2 - 氧膦基脒金属盐络合物和N 2 - 氧膦基脒基金属盐络合物的催化剂体系以及使用N 2 - 氧膦基脒化合物，N 2 - 氧膦基脒基化物，N 2 - 氧膦基脒金属盐络合物和N 2 - 氧化脒基金属盐络合物，用于烯烃的低聚和/或聚合。

13. 发明授权

US08865610B2 Phosphinyl guanidine compounds, metal salt complexes, catalyst systems, and their use to oligomerize or polymerize olefins 有权
标题翻译：膦基胍化合物，金属盐络合物，催化剂体系及其烯烃低聚或聚合的用途
公开(公告)号：US08865610B2
公开(公告)日：2014-10-21
申请号：US13490319
申请日：2012-06-06
申请人： Orson L. Sydora , Brooke L. Small , Michael J. Carney
发明人： Orson L. Sydora , Brooke L. Small , Michael J. Carney
IPC分类号： B01J31/02 , C07F9/02
CPC分类号： B01J31/189 , B01J2231/20 , B01J2531/62 , C07C2/26 , C07C11/02
摘要： The present application relates to N2-phosphinyl guanidine metal salt complexes. The present application also relates to catalyst systems comprising N2-phosphinyl guanidine metal salt complexes and processes for making catalyst systems comprising N2-phosphinyl guanidine metal salt complexes. The present application also relates to utilizing N2-phosphinyl guanidine metal salt complexes in processes of oligomerizing or polymerizing olefins.
摘要翻译：本申请涉及N2-氧膦基胍金属盐络合物。本申请还涉及包含N 2 - 氧膦基胍金属盐络合物的催化剂体系和用于制备包含N 2 - 氧膦基胍金属盐络合物的催化剂体系的方法。本申请还涉及在烯烃低聚或聚合过程中利用N 2 - 氧膦基胍金属盐络合物。

14. 发明申请

US20130150593A1 ANHYDROUS CHROMIUM(III) HALIDE COMPLEX PREPARATION 有权
标题翻译：无机铬（III）卤化物复合制备
公开(公告)号：US20130150593A1
公开(公告)日：2013-06-13
申请号：US13323265
申请日：2011-12-12
申请人： Orson L. Sydora
发明人： Orson L. Sydora
IPC分类号： C07D307/08
CPC分类号： C07F11/005
摘要： This disclosure provides a process for preparing an anhydrous chromium(III) halide complex, comprising contacting a chromium(III) halide hydrate, a water absorption agent, and a coordinating solvent, L, and forming a chromium(III) halide complex having the formula CrX3.mL, wherein X is a halide and m is the number of moles of L per mole of chromium. This process is exemplified in the preparation of the substantially anhydrous or anhydrous CrCl3(THF)3, the process comprising contacting CrCl3.6H2O, tetrahydrofuran, and 3 Å, 4 Å, 5 Å, 10×, or 13× molecular sieves; forming CrCl3(THF)3; and isolating the CrCl3(THF)3 having a water content of less than or equal to 100 ppm.
摘要翻译：本公开内容提供了制备无水氯化铬（III）络合物的方法，包括使卤化铬（III）水溶液，吸水剂和配位溶剂L接触，形成具有式 CrX3.mL，其中X是卤化物，m是每摩尔铬的L摩尔数。该方法在制备基本上无水或无水的CrCl 3（THF）3时举例说明，该方法包括使CrCl3·6H2O，四氢呋喃和3，4，5，10x或13x分子筛接触; 形成CrCl 3（THF）3; 并分离出含水量小于或等于100ppm的CrCl 3（THF）3。

15. 发明申请

US20100274065A1 OLIGOMERIZATION CATALYST SYSTEM AND PROCESS FOR OLIGOMERIZING OLEFINS 有权
标题翻译：低分子化催化剂体系和低聚烯烃的方法
公开(公告)号：US20100274065A1
公开(公告)日：2010-10-28
申请号：US12771122
申请日：2010-04-30
申请人： Orson L. Sydora
发明人： Orson L. Sydora
IPC分类号： C07C2/24 , B01J31/14 , C07C2/02
CPC分类号： B01J31/181 , B01J31/0244 , B01J31/122 , B01J31/143 , B01J31/1608 , B01J2231/20 , B01J2531/0288 , B01J2531/62 , C07C2/32 , C07C2531/14 , C07C2531/18 , C07C2531/34 , Y02P20/582 , C07C11/107
摘要： Among other things, this disclosure provides an olefin oligomerization system and process, the system comprising: a) a transition metal compound; b) a pyrrole compound having a hydrogen atom on at the 5-position or the 2- and 5-position of a pyrrole compound and having a bulky substituent located on each carbon atom adjacent to the carbon atom bearing a hydrogen atom at the 5-position or the 2- and 5-position of a pyrrole compound. These catalyst system have significantly improved productivities, selectivities to 1-hexene, and provides higher purity 1-hexene within the C6 fraction than catalyst systems using 2,4-dimethylpyrrole.
摘要翻译：除此之外，本公开提供烯烃低聚体系和方法，该体系包括：a）过渡金属化合物; b）在吡咯化合物的5-位或2-和5-位上具有氢原子的吡咯化合物，并且位于与在5-位上具有氢原子的碳原子相邻的每个碳原子上具有庞大取代基的吡咯化合物，位置或吡咯化合物的2-和5-位。这些催化剂体系对使用2,4-二甲基吡咯的催化剂体系具有显着提高的生产率，对1-己烯的选择性，并且在C6馏分内提供更高纯度的1-己烯。

16. 发明申请

US20100113852A1 OLIGOMERIZATION CATALYST SYSTEM AND PROCESS FOR OLIGOMERIZING OLEFINS 有权
标题翻译：低分子化催化剂体系和低聚烯烃的方法
公开(公告)号：US20100113852A1
公开(公告)日：2010-05-06
申请号：US12609272
申请日：2009-10-30
申请人： Orson L. Sydora
发明人： Orson L. Sydora
IPC分类号： C07C2/24 , B01J31/02 , C08F4/42 , B01J31/34 , B01J21/02
CPC分类号： B01J31/122 , B01J31/0237 , B01J31/0239 , B01J31/0244 , B01J31/143 , B01J2231/20 , B01J2531/62 , Y02P20/582 , Y10S585/903
摘要： Among other things, this disclosure provides an olefin oligomerization system and process, the system comprising: a) a transition metal compound; b) a pyrrole compound having independently-selected C1 to C18 organyl groups at the 2- and 5-positions, wherein at least one of the organyl group alpha-carbon atoms attached to the 2- and 5-positions of the pyrrole compound is a secondary carbon atoms; and c) a metal alkyl. For example, the 2,5-diethylpyrrole (2,5-DEP)-based catalyst systems can afford a productivity increases over unsubstituted pyrrole catalyst systems, non-2,5-disubstituted catalyst systems, and 2,5-dimethylpyrrole (2,5-DMP) catalyst systems.
摘要翻译：除此之外，本公开提供烯烃低聚体系和方法，该体系包括：a）过渡金属化合物; b）在2-和5-位具有独立选择的C1至C18有机基团的吡咯化合物，其中与吡咯化合物的2-和5-位连接的至少一个有机基团的α-碳原子是次级碳原子; 和c）金属烷基。例如，基于2,5-二乙基吡咯（2,5-DEP）的催化剂体系可以提供比未取代的吡咯催化剂体系，非2,5-二取代的催化剂体系和2,5-二甲基吡咯（2， 5-DMP）催化剂体系。

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