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11. 发明授权

US4297501A Process for the preparation of urethanes 失效
标题翻译：制备聚氨酯的方法
公开(公告)号：US4297501A
公开(公告)日：1981-10-27
申请号：US125394
申请日：1980-02-27
申请人： Robert Becker , Johann Grolig , Christian Rasp
发明人： Robert Becker , Johann Grolig , Christian Rasp
IPC分类号： B01J27/10 , B01J21/00 , B01J23/00 , B01J23/56 , B01J23/89 , B01J27/00 , B01J31/00 , B01J31/28 , C07C67/00 , C07C239/00 , C07C269/04 , C07C125/065
CPC分类号： C07C269/04
摘要： A process for producing urethanes by reacting primary amines, carbon monoxide and organic hydroxyl compounds in the presence of molecular oxygen and/or organic nitro compounds as oxidizing agents and a catalyst system comprising a noble metal and/or a compound of a noble metal of the 8th subgroup of the Periodic System of Elements and a compound capable of undergoing Redox reactions under reaction conditions of the 3rd to 5th main group and/or 1st to 8th subgroup of the Periodic System of Elements.
摘要翻译：在分子氧和/或有机硝基化合物作为氧化剂存在下使伯胺，一氧化碳和有机羟基化合物反应制备氨基甲酸酯的方法和包含贵金属和/或贵金属的化合物的催化剂体系元素周期元素第8族和能够在元素周期表第3至第5主族和/或第1至第8族的反应条件下进行氧化还原反应的化合物。

12. 发明授权

US4262130A Process for the production of urethanes 失效
标题翻译：生产聚氨酯的工艺
公开(公告)号：US4262130A
公开(公告)日：1981-04-14
申请号：US112780
申请日：1980-01-17
申请人： Robert Becker , Johann Grolig , Christian Rasp
发明人： Robert Becker , Johann Grolig , Christian Rasp
IPC分类号： C07B61/00 , B01J23/00 , B01J23/44 , B01J23/74 , B01J23/89 , B01J27/10 , B01J27/128 , B01J31/02 , C07C67/00 , C07C239/00 , C07C269/00 , C07C125/065 , C07C125/073
CPC分类号： B01J23/8906 , B01J27/10
摘要： The present invention relates to an improved process for the production of urethanes (carbamic acid esters) by the reaction of organic nitro compounds with carbon monoxide and organic compounds containing at least one hydroxy group in the presence of palladium and/or palladium compounds and a cocatalyst which consists of a mixture of one or more iron oxides and/or iron hydroxides and activating chloride-containing additives.
摘要翻译：本发明涉及通过有机硝基化合物与一氧化碳和含有至少一个羟基的有机化合物在钯和/或钯化合物和助催化剂的存在下反应制备氨基甲酸酯（氨基甲酸酯）的改进方法其由一种或多种氧化铁和/或氢氧化铁和活化的含氯化物的添加剂的混合物组成。

13. 发明授权

US4151262A Process for the catalytic conversion of organic chlorine compounds 失效
标题翻译：有机氯化合物的催化转化工艺
公开(公告)号：US4151262A
公开(公告)日：1979-04-24
申请号：US868551
申请日：1978-01-11
申请人： Christian Rasp , Gerhard Scharfe
发明人： Christian Rasp , Gerhard Scharfe
IPC分类号： B01J23/00 , C01B7/01 , C01B32/50 , C01B7/00 , B01J8/00 , C01B7/08
CPC分类号： C01B7/01
摘要： A process has been developed for the catalytic conversion of organic chlorine compounds into carbon dioxide and hydrogen chloride, using molecular oxygen, in which process the catalyst system is provided by using platinum in a first catalyst zone and palladium in a second catalyst zone.
摘要翻译：已经开发了一种使用分子氧将有机氯化合物催化转化成二氧化碳和氯化氢的方法，在该方法中，通过在第一催化剂区中使用铂和在第二催化剂区中使用钯来提供催化剂体系。

14. 发明授权

US5883291A Heat exchange media for the thermal cracking of carbamic acid esters 失效
标题翻译：用于氨基甲酸酯热裂解的热交换介质
公开(公告)号：US5883291A
公开(公告)日：1999-03-16
申请号：US812610
申请日：1997-03-06
申请人： Dieter Schleenstein , Christian Rasp , Georg Ronge , Oswald Wilmes
发明人： Dieter Schleenstein , Christian Rasp , Georg Ronge , Oswald Wilmes
IPC分类号： C07C263/04 , C07C265/04 , C07C265/14 , C07C269/06 , C07C271/20 , C07C263/00
CPC分类号： C07C263/04 , Y02P20/127 , Y02P20/582
摘要： Inert, thermally stable high-boiling solvents which have a defined boiling point or which boil over a narrow range are used as heat exchange media during thermal cracking of carbamic acid esters (urethane cracking).
摘要翻译：在氨基甲酸酯（氨基甲酸酯裂解）的热裂解过程中，作为热交换介质，使用具有规定沸点或沸点在较窄范围内的热稳定型高沸点溶剂。

15. 发明授权

US5731458A Process for thermally cracking carbamic acid esters 失效
标题翻译：热裂解氨基甲酸酯的方法
公开(公告)号：US5731458A
公开(公告)日：1998-03-24
申请号：US811801
申请日：1997-03-06
申请人： Jurgen Dahmer , Dieter Schleenstein , Heinrich Steude , Oswald Wilmes , Christian Rasp , Georg Ronge , Klaus Nachtkamp , Wilfried Litz , Stephan Kabelac
发明人： Jurgen Dahmer , Dieter Schleenstein , Heinrich Steude , Oswald Wilmes , Christian Rasp , Georg Ronge , Klaus Nachtkamp , Wilfried Litz , Stephan Kabelac
IPC分类号： C07C263/04 , C07C265/04 , C07C265/14 , C07C269/06 , C07C271/20
CPC分类号： C07C263/04 , Y02P20/127 , Y02P20/582
摘要： This present invention relates to a process for thermally cracking carbamic acid esters into the corresponding isocyanate and hydroxyl compounds in the liquid phase, wherein the reaction proceeds as a reactive rectification in the stripping zone of a column and in an inert, high-boiling solvent, which acts as a buffer to keep the reaction away from the evaporator region of the column.
摘要翻译：本发明涉及一种将氨基甲酸酯热裂解成液相中相应的异氰酸酯和羟基化合物的方法，其中反应在塔的汽提区和惰性高沸点溶剂中作为反应性精馏进行，其用作缓冲剂以使反应远离柱的蒸发器区域。

16. 发明授权

US5439869A Thermoreactive recording material of particular stability 失效
标题翻译：特别稳定的热敏记录材料
公开(公告)号：US5439869A
公开(公告)日：1995-08-08
申请号：US69963
申请日：1993-05-28
申请人： Gunter Klug , Pieter Ooms , Christian Rasp
发明人： Gunter Klug , Pieter Ooms , Christian Rasp
IPC分类号： B41M5/333 , C09D5/26 , D21H19/00 , B41M5/26
CPC分类号： B41M5/3335
摘要： New thermoreactive recording materials contain a mixture containing at least one specifically modified bisphenol carboxylic acid and at least one basic compound. They are distinguished by good stabilization of the color even upon extended storage, good light stabilities and excellent stabilities to water, plasticizers, greases and ingredients of text-marking pens.
摘要翻译：新的热反应性记录材料含有含有至少一种特别改性的双酚羧酸和至少一种碱性化合物的混合物。它们的特征在于即使延长储存，良好的光稳定性和对水，增塑剂，润滑脂和文字标记笔的成分的极好的稳定性，颜色也能稳定。

17. 发明授权

US4770804A Thickening systems for high water based functional fluids and the high water based functional fluids containing these thickening systems 失效
标题翻译：用于高水性功能流体的增稠系统和含有这些增稠系统的高水性功能流体
公开(公告)号：US4770804A
公开(公告)日：1988-09-13
申请号：US900064
申请日：1986-08-25
申请人： Karl-Heinz Hentschel , Christian Rasp , Siegfried Kussi , Udo-Winfried Hendricks
发明人： Karl-Heinz Hentschel , Christian Rasp , Siegfried Kussi , Udo-Winfried Hendricks
IPC分类号： C10M173/00 , C10M173/02 , C10N30/02 , C10N40/08 , C10N40/20 , C10N60/00 , C21D1/60
CPC分类号： C10M173/02 , C10M2201/02 , C10M2209/104 , C10M2215/042 , C10M2217/042 , C10M2217/043 , C10M2217/044 , C10M2217/045 , C10M2219/044 , C10M2223/04 , C10M2223/042 , C10M2223/043 , C10N2240/08 , C10N2250/02
摘要： The invention relates to the use of combinations of water-soluble polymeric polyether polyols, in which at least 50% of the terminal hydroxyl groups are blocked by reaction with a monoisocyanate incorporating a long-chain aliphatic hydrocarbon radical, and certain surfactants as thickener systems for high water based functional fluids and to the thickened high water based functional fluids.
摘要翻译：本发明涉及使用水溶性聚醚多元醇的组合，其中至少50％的末端羟基通过与包含长链脂族烃基的单异氰酸酯反应而被阻断，以及某些表面活性剂作为增稠剂体系高水性功能流体和增稠的高水性功能流体。

18. 发明授权

US4339592A Process for the production of urethanes 失效
标题翻译：生产聚氨酯的工艺
公开(公告)号：US4339592A
公开(公告)日：1982-07-13
申请号：US238518
申请日：1981-02-26
申请人： Robert Becker , Christian Rasp , Gunter Stammann , Johann Grolig
发明人： Robert Becker , Christian Rasp , Gunter Stammann , Johann Grolig
IPC分类号： C07C269/00 , B01J23/89 , B01J27/00 , B01J27/06 , B01J27/10 , B01J31/00 , B01J31/28 , B01J31/34 , C07B61/00 , C07C67/00 , C07C239/00 , C07C271/26 , C07C271/28 , C07C125/073
CPC分类号： B01J27/06 , B01J23/8906
摘要： A urethane is produced by reacting an organic nitro compound with carbon monoxide and an organic compound containing at least one hydroxyl group in the presence of a catalyst and a co-catalyst. This reaction is conducted in the liquid phase at elevated temperature and pressure. The catalyst employed is an element and/or compound of an element from the group of noble metals of the 8th Secondary Group of the Periodic Table. The co-catalyst used is formed from (1) a component taken from the group consisting of iron oxychloride, a mixture of iron compounds containing iron oxychloride and oxide-chloride combinations and (2) metallic iron or an iron alloy in finely divided or high surface form. The oxides which may be used in the oxide-chloride combinations of co-catalyst component (1) are the oxides and/or oxide hydrates of tetravalent tin, trivalent chromium, hexavalent molybdenum, hexavalent tungsten, pentavalent vanadium, divalent iron and trivalent iron. The chlorides which may be used in this oxide-chloride combination are chlorides of the elements of Groups IIIA, IVA, VA and IB to VIIIB of the Periodic Table and/or hydrochlorides of tertiary amines.
摘要翻译：氨基甲酸酯是通过有机硝基化合物与一氧化碳和含有至少一个羟基的有机化合物在催化剂和助催化剂的存在下反应生成的。该反应在升高的温度和压力下在液相中进行。所使用的催化剂是来自元素周期表第八族中的贵金属的元素和/或化合物。所使用的助催化剂由（1）由三氯氧化铁组成的组分，含有氯氧化铁的铁化合物和氧化物 - 氯化物组合的混合物组成的组分和（2）细碎或高分的金属铁或铁合金表面形式。可用于助催化剂组分（1）的氧化物 - 氯化物组合的氧化物是四价锡，三价铬，六价钼，六价钨，五价钒，二价铁和三价铁的氧化物和/或氧化物水合物。可用于该氧化物 - 氯化物组合中的氯化物是元素周期表IIIA，IVA，VA和IB至VIIIB族元素的氯化物和/或叔胺的盐酸盐。

19. 发明授权

US5314982A Process for the preparation of polyurea greases 失效
标题翻译：聚脲润滑脂的制备工艺
公开(公告)号：US5314982A
公开(公告)日：1994-05-24
申请号：US945867
申请日：1992-09-17
申请人： Christian Rasp , Ralf Timmermann , Hermann Perrey , Bernhard Lehmann , Siegfried Kussi
发明人： Christian Rasp , Ralf Timmermann , Hermann Perrey , Bernhard Lehmann , Siegfried Kussi
IPC分类号： C08G18/32 , C10M119/24 , C10N20/06 , C10N50/10 , C10N70/00 , C08G18/08
CPC分类号： C08G18/3228 , C08G18/2865 , C10M119/24 , C10M2217/042 , C10M2217/043 , C10N2220/02
摘要： The invention relates to a new three-part process, which can also be employed on a large industrial scale, for the preparation of polyurea lubricating greases, which is characterised(a) in that polyureas which carry oleophilic groups are prepared by reaction of diisocyanates with amines either in the absence of a solvent on a reaction screw at 80.degree.-120.degree. C., preferably at 85.degree.-95.degree. C., (variant A) or in a toluene medium at 20.degree.-80.degree. C., preferably at 30.degree.-60.degree. C., (variant B),(b) in that, after complete reaction, the polyureas prepared according to (a) are ground in the solid, dry state to give powders (at least 70% by weight of the powder having particle sizes of about 100-400.mu.) and(c) in that the ground crude product, after being made into a "paste" (wetted) at elevated temperature in the base oil employed (10-30 minutes at 140.degree.-180.degree. C.) and cooled again to room temperature, is processed to a grease by complete homogenisation--if appropriate in several passes--in a high-pressure homogeniser under a pressure of 400-1,500 bar (spontaneous heating occurring up to about 100.degree. C.),greases having readily reproducible and essentially the same properties as in the case of the previously customary in situ manufacture being produced.
摘要翻译：本发明涉及一种新的三部分方法，其也可用于大型工业规模，用于制备聚脲润滑脂，其特征在于（a）通过二异氰酸酯与二异氰酸酯反应制备携带亲油基团的聚脲在80°-120℃，优选85℃-95℃，（变体A）或在20-80℃的甲苯介质中，在反应螺杆上不存在溶剂的胺，优选在30°-60℃，（变体B），（b），完全反应后，根据（a）制备的聚脲在固体，干燥状态下研磨，得到粉末（至少70重量％的颗粒大小为100-400微米的粉末）和（c）因为所研磨的粗产物在所用基础油中在升高的温度下制成“糊”（润湿）（在140℃下10-30分钟 DEG-180℃），并再次冷却至室温，通过完全均化（如果合适的话）在几种情况下加工成润滑脂在400-1,500巴的压力（自发加热直到约100℃）下进入高压均化器，具有与先前常规原位制造情况相同的容易重复性和基本上相同性质的润滑脂生产。

20. 发明授权

US4973414A Polyethers, process for their preparation and lubricants containing these polyethers 失效
标题翻译：聚醚，其制备方法和含这些聚醚的润滑剂
公开(公告)号：US4973414A
公开(公告)日：1990-11-27
申请号：US194706
申请日：1988-05-17
申请人： Dittmar Nerger , Karl-Heinz Hentschel , Christian Rasp , Pramod Gupta , Siegfried Kussi
发明人： Dittmar Nerger , Karl-Heinz Hentschel , Christian Rasp , Pramod Gupta , Siegfried Kussi
IPC分类号： C10M109/02 , C07C43/11 , C08G65/26 , C08G65/28 , C08G65/30 , C10M107/34 , C10M111/04 , C10M145/34 , C10M145/36 , C10M159/12 , C10M169/04 , C10N20/04 , C10N30/08 , C10N30/10
CPC分类号： C07C43/11 , C08G65/2606 , C08G65/30 , C10M107/34 , C10M111/04 , C10M145/36 , C10M169/041 , C10M2203/1006 , C10M2203/1025 , C10M2203/1045 , C10M2203/1065 , C10M2203/1085 , C10M2205/0206 , C10M2205/028 , C10M2209/1033 , C10M2209/1045 , C10M2209/1055 , C10M2209/1065 , C10M2209/107 , C10M2209/1075 , C10M2209/108 , C10M2209/1085 , C10M2209/1095 , C10N2220/02 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Monofunctional polyethers having hydroxyl groups contain as built-in terminal groups or monomers(a) 1 to 30% by weight of one or more C.sub.4 - to C.sub.24 -alkylmonophenols,(b) 1 to 30% by weight of one or more C.sub.8 - to C.sub.24 -monoalkanols,(c) 1 to 30% by weight of one or more C.sub.10 - to C.sub.20 -1,2-epoxyalkanes and(d) 45 to 80% by weight of propylene oxide or a lower alkylene oxide mixture consisting mainly of propylene oxidethe sum of components (a) to (d) adding up to 100% by weight, and have average molecular weights of 600 to 2,500.These polyethers are prepared by anionic epoxide polymerization and used as lubricants and components of lubricants.
摘要翻译：具有羟基的单官能聚醚包含内置的末端基团或单体（a）1至30重量％的一种或多种C 4至C 24烷基单酚，（b）1至30重量％的一个或多个C 8 - C24-单链烷醇，（c）1至30重量％的一种或多种C10至C20-1,2-环氧烷烃和（d）45至80重量％的环氧丙烷或主要由丙烯组成的低级烯化氧混合物氧化组分（a）至（d）的总和，加入至100重量％，平均分子量为600至2,500。这些聚醚通过阴离子环氧化物聚合制备，并用作润滑剂和润滑剂组分。

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