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11. 发明申请

US20090182183A1 PROPYLENE OLIGOMERIZATION PROCESS 有权
标题翻译：丙烯低聚过程
公开(公告)号：US20090182183A1
公开(公告)日：2009-07-16
申请号：US12014406
申请日：2008-01-15
申请人： Michael J. Keenan , Ramzi Y. Saleh , James C. Vartuli , Robert C. Lemon , Jean W. Beeckman , Christopher C. Boyer , Mitchell E. Loescher
发明人： Michael J. Keenan , Ramzi Y. Saleh , James C. Vartuli , Robert C. Lemon , Jean W. Beeckman , Christopher C. Boyer , Mitchell E. Loescher
IPC分类号： C07C2/24
CPC分类号： C07C2/10 , C07C2521/06 , C07C2523/30 , Y02P20/52
摘要： A process for the oligomerization of propylene is disclosed wherein a tungstated zirconia catalyst prepared as a distillation structure is used in a reaction distillation zone under conditions of temperature and pressure to concurrently react the propylene to produce oligomers thereof and separate the oligomer products from unreacted propylene by fractional distillation in a distillation column reactor. Compared to the prior art tubular or plug flow reactors, lower temperatures and pressures are used to produce higher conversions and selectivities to preferred isomeric forms useful for preparing neo acids.
摘要翻译：公开了一种用于丙烯低聚的方法，其中在反应蒸馏区中在温度和压力条件下使用制备为蒸馏结构的钨酸氧化锆催化剂，以同时使丙烯反应生成其低聚物，并将低聚物产物与未反应的丙烯分离在蒸馏塔反应器中进行分馏。与现有技术的管状或活塞式流动反应器相比，使用较低的温度和压力来产生较高的转化率和选择性，以用于制备新酸的优选异构形式。

12. 发明授权

US07145049B2 Oligomerization process 有权
标题翻译：低聚过程
公开(公告)号：US07145049B2
公开(公告)日：2006-12-05
申请号：US10898506
申请日：2004-07-23
申请人： Mitchell E. Loescher , David G. Woods , Michael J. Keenan , Steven E. Silverberg , Paul W. Allen
发明人： Mitchell E. Loescher , David G. Woods , Michael J. Keenan , Steven E. Silverberg , Paul W. Allen
IPC分类号： C07C2/04 , C07C2/02
CPC分类号： C07C2/12 , C07C2529/70 , Y02P20/127 , C07C11/02
摘要： Alkenes, such as normal butenes in a mixed C4 stream are oligomerized, preferably to dimers, which are dimerized in a distillation column reactor over ZSM-57 zeolite catalyst at high conversions and high selectivity to octenes. Prior to oligomerization the mixed C4 stream is pretreated to remove dimethyl ether, butadienes and sulfur compounds.
摘要翻译：烯烃，例如混合的C 4 H 4流中的正丁烯通过ZSM-57沸石催化剂在蒸馏塔反应器中以高转化率和对辛烯的高选择性被二聚体低聚，优选二聚体。在低聚之前，将混合的C 4 H 3流预处理以除去二甲醚，丁二烯和硫化合物。

13. 发明授权

US6136991A Glycidyl ester adducts having increased glass transition temperatures 失效
公开(公告)号：US6136991A
公开(公告)日：2000-10-24
申请号：US967634
申请日：1997-11-10
申请人： Richard William Ryan , Gerald G. McGlamery, Jr. , Ralph Martin Kowalik , Michael J. Keenan
发明人： Richard William Ryan , Gerald G. McGlamery, Jr. , Ralph Martin Kowalik , Michael J. Keenan
IPC分类号： C07D301/32 , C07D303/16
CPC分类号： C07D301/32 , C07D303/16
摘要： The invention provides for a purified glycidyl ester product prepared from neo acids wherein said ester product is recovered as a light fraction from a glycidyl ester reaction product composition that has been subjected to conditions of temperature and vacuum in a thin film, short pass distillation evaporator, said purified glycidyl ester product further characterized that its polymerizable reaction product with methacrylic acid has a higher effective glass transition temperature as compared with the polymerizable reaction product with methacrylic acid of said glycidyl ester reaction product composition prior to purification.

14. 发明授权

US5401891A Production of polymerization grade dicyclopentadiene 失效
标题翻译：生产聚合级二环戊二烯
公开(公告)号：US5401891A
公开(公告)日：1995-03-28
申请号：US169847
申请日：1993-12-17
申请人： Michael J. Keenan , David W. Sharp , Robert C. Schucker
发明人： Michael J. Keenan , David W. Sharp , Robert C. Schucker
IPC分类号： B01D61/36 , B01D71/54 , B01D71/64 , B01D71/74 , C07C2/44 , C07C2/50 , C07C7/144 , C07C13/61 , C07C7/00 , C07C1/00
CPC分类号： C07C13/61 , C07C2/44 , C07C2103/68
摘要： A process for purifying crude dicyclopentadiene which comprises the steps of: cracking the crude dicyclopentadiene to form a monomeric-containing effluent which comprises at least one monomer selected from the group consisting of: C.sub.4 acyclic dienes, C.sub.5 acyclic dienes, cyclopentadiene and methylcyclopentadiene; separating the monomeric-containing effluent into a cyclopentadiene-enriched stream and a cyclopentadiene-poor stream; dimerizing the cyclopentadiene-enriched stream to form a dimerizer effluent; contacting a membrane separator under pervaporation conditions with the dimerizer effluent wherein the C.sub.4 acyclic dienes, C.sub.5 acyclic dienes and cyclopentadiene permeate through the membrane separator and wherein a dicyclopentadiene product having a purity of at least about 98% is retained as retentate.
摘要翻译：一种用于纯化粗二环戊二烯的方法，其包括以下步骤：裂解粗二环戊二烯以形成含单体的流出物，其包含至少一种选自以下的单体：C 4无环二烯，C5无环二烯，环戊二烯和甲基环戊二烯; 将含单体的流出物分离成富含环戊二烯的流和不饱和环戊二烯流; 使富含环戊二烯的流二聚化以形成二聚体流出物; 使膜分离器在渗透蒸发条件下与二聚化器流出物接触，其中C4无环二烯，C5无环二烯和环戊二烯渗透通过膜分离器，并且其中保留纯度至少为约98％的二环戊二烯产物作为保留物。

15. 发明授权

US5103058A Process for producing imines and/or amines from alcohols 失效
标题翻译：从醇生产亚胺和/或胺的方法
公开(公告)号：US5103058A
公开(公告)日：1992-04-07
申请号：US609209
申请日：1990-11-05
申请人： Roy L. Pruett , Michael J. Keenan , Edmund J. Mozeleski
发明人： Roy L. Pruett , Michael J. Keenan , Edmund J. Mozeleski
IPC分类号： B01J23/06 , C07B61/00 , C07C209/52 , C07C209/62 , C07C211/03 , C07C211/08 , C07C249/02 , C07C251/08
CPC分类号： C07C209/62 , C07C249/02
摘要： Process for producing aliphatic imines and/or amines from aliphatic monohydric alcohols, such as higher molecular weight oxo alcohols, including ether alcohols, comprising the steps of dehydrogenating the alcohol to an aldehyde in situ in the presence of a zinc oxide and/or zinc salt/metal hydroxide dehydrogenation catalyst and a soluble amount of a primary aliphatic amine which condenses immediately with the aldehyde under reflux conditions, with continuous water removal, to form the corresponding aliphatic imine (Schiff base). The corresponding aliphatic amine can be formed by reducing or reductively aminating the imine in known manner to form corresponding primary, secondary or tertiary amines as desired. The step of forming the imine is most critical, and the present zinc/metal hydroxide dehydrogenation catalyst system has been found to provide a gentle, inexpensive and efficient conversion of the alcohol to the aldehyde for reaction with the gradually-added primary amine, coupled with the continuous removal of the water of condensation in order to prevent undesired secondary reactions which reduce the yield.
摘要翻译：用于由脂族一元醇如高分子量羰基合成醇（包括醚醇）生产脂族亚胺和/或胺的方法，包括以下步骤：在氧化锌和/或锌盐存在下使醇原位脱氢 /金属氢氧化物脱氢催化剂和可溶量的伯脂肪胺，其在回流条件下立即与醛冷凝，并连续除水，形成相应的脂族亚胺（席夫碱）。相应的脂族胺可以通过以已知方式还原或还原胺化亚胺形成，以根据需要形成相应的伯，仲或叔胺。形成亚胺的步骤是至关重要的，并且已经发现现有的锌/金属氢氧化物脱氢催化剂体系可以提供温和，便宜和有效的醇转化为醛，以与逐渐加入的伯胺反应，加上连续除去冷凝水，以防止不希望的二次反应降低产率。

16. 发明授权

US5731486A Process for preparing 3-methyl-2-pentene 失效
公开(公告)号：US5731486A
公开(公告)日：1998-03-24
申请号：US503134
申请日：1995-07-17
申请人： Dan E. Hendriksen , Gerald G. McGlamery , Michael J. Keenan , Derrick D. Pete
发明人： Dan E. Hendriksen , Gerald G. McGlamery , Michael J. Keenan , Derrick D. Pete
IPC分类号： C07C2/30 , C07C11/113 , C07C51/14 , C07C2/04 , C07C2/24 , C07C2/26 , C07C2/34
CPC分类号： C07C2/30 , C07C11/113 , C07C51/14
摘要： A method for producing 3-methyl-2-pentene which is substantially free of any other C.sub.6 olefin, except 2-ethyl-1-butene, by first producing a stream that contains 2-ethyl-1-butene from the trimerization of ethylene, and second by recovering the 2-ethyl-1-butene as 3-methyl-2-pentene via etherification, separation of the ether, and decomposition of the ether back to predominantly 3-methyl-2-pentene with some 2-ethyl-1-butene.

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