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11. 发明申请

US20060149083A1 Method for the decarboxylation of dicarboxylic acids 失效
标题翻译：二羧酸脱羧的方法
公开(公告)号：US20060149083A1
公开(公告)日：2006-07-06
申请号：US10538995
申请日：2003-12-04
申请人： Sigurd Buchholz , Alexander Klausener , Reinhard Langer , Leslaw Mleczko , Gunter Leverkusen
发明人： Sigurd Buchholz , Alexander Klausener , Reinhard Langer , Leslaw Mleczko , Gunter Leverkusen
IPC分类号： C07D495/02
CPC分类号： C07D495/04 , C07D333/38 , Y02P20/582
摘要： The invention relates to a method for the thermal decarboxylation of dicarboxylic acids, in particular to 3,4-ethylene dioxythiophene-2,5-dicarboxylic acid as an educt. According to said method the educt is used in solid form and/or the reaction is carried out in the presence of a plurality of fluidised bed bodies. No solvents are used in the reaction and the decarboxylation product that is formed during the reaction is carried away from the reaction zone in gaseous form.
摘要翻译：本发明涉及一种二羧酸热脱羧的方法，特别涉及作为溶出物的3,4-亚乙基二氧噻吩-2,5-二羧酸的热脱羧方法。根据所述方法，溶出物以固体形式使用和/或反应在多个流化床体的存在下进行。在反应中没有使用溶剂，并且在反应期间形成的脱羧产物以气态形式从反应区带走。

12. 发明授权

US06953559B2 Method for producing highly pure, granular silicon 失效
标题翻译：高纯度颗粒状硅的制造方法
公开(公告)号：US06953559B2
公开(公告)日：2005-10-11
申请号：US10450123
申请日：2001-11-21
申请人： Leslaw Mleczko , Sigurd Buchholz , Maria Pilar Ezpeleta Tejero , Felix-Karl Oliver Schlüter
发明人： Leslaw Mleczko , Sigurd Buchholz , Maria Pilar Ezpeleta Tejero , Felix-Karl Oliver Schlüter
IPC分类号： C01B33/027 , C01B33/029 , H01L31/18 , C01B33/02
CPC分类号： C01B33/027 , C01B33/029 , H01L31/1804 , Y02E10/547 , Y02P70/521
摘要： The invention relates to a method for producing highly pure, granular silicon by decomposing a gas containing silicon in a procedure comprising at least two operating states, at least one state comprising the increased formation of nucleus particles from the decomposition of said gas containing silicon and at least one other state comprising the increased separation of the silicon with expansion of the diameter of the silicon granules. The invention also relates to the use of silicon produced in this way and to highly pure, granular silicon particles which are characterised by a coreless structure.
摘要翻译：本发明涉及通过在包含至少两种操作状态的方法中分解含硅气体来生产高纯度颗粒状硅的方法，至少一种状态包括从所述含硅气体的分解增加形成的核粒子，以及在至少一个其他状态包括随着硅颗粒直径的扩大而增加硅的分离。本发明还涉及以这种方式制造的硅以及以无芯结构为特征的高纯度颗粒状硅颗粒的用途。

13. 发明授权

US06852301B2 Method for producing silane 失效
标题翻译：硅烷的制造方法
公开(公告)号：US06852301B2
公开(公告)日：2005-02-08
申请号：US10450207
申请日：2001-11-21
申请人： Hans-Dieter Block , Leslaw Mleczko , Andreas Bulan , Rainer Weber , Sigurd Buchholz , Torsten Sill
发明人： Hans-Dieter Block , Leslaw Mleczko , Andreas Bulan , Rainer Weber , Sigurd Buchholz , Torsten Sill
IPC分类号： C01B33/04 , C01B33/18
CPC分类号： C01B33/046 , C01B33/043 , C01B33/18
摘要： The invention relates to a method for producing silane (SiH4) by a) reacting metallurgical silicon with silicon tetrachloride (SiCl4) and hydrogen (H2), to form a crude gas stream containing trichlorosilane (SiHCl3) and silicon tetrachloride (SiCl4), b) removing impurities from the resulting crude gas stream by washing with condensed chlorosilanes, c) condensing and subsequently, separating the purified crude gas stream by distillation, d) returning the partial stream consisting essentially of SiCl4 to the reaction of metallurgical silicon with SiCl4 and H2, e) disproportionating the partial stream containing SiHCl3, to form SiCl4 and SiH4 and f) returning the SiH4 formed by disproportionation to the reaction of metallurgical silicon with SiCl4 and H2, the crude gas stream containing trichlorosilane and silicon tetrachloride being liberated from solids as far as possible by gas filtration before being washed with the condensed chlorosilanes. The washing process with the condensed chlorosilanes is carried out at a pressure of 25 to 40 bar and at a temperature of at least 150° C. in a single-stage distillation column and is carried out in such a way that 0.1 to 3 wt. % of the crude gas stream containing trichlorosilane and silicon tetrachloride is recovered in the form of a condensed liquid phase consisting essentially of SiCl4, this liquid phase then being removed from the SiCl4 circuit and expanded to a pressure of 1 bar outside said SiCl4 circuit and cooled to a temperature of 10 to 40° C., whereby dissolved impurities separate out and are then removed by filtration.
摘要翻译：本发明涉及一种通过以下步骤制备硅烷（SiH 4）的方法：a）使冶金硅与四氯化硅（SiCl 4）和氢（H 2）反应，形成含有三氯硅烷（SiHCl 3）和四氯化硅（SiCl 4）的粗气流，b）通过用冷凝的氯硅烷洗涤从所得粗气流中除去杂质，c）冷凝并随后通过蒸馏分离纯化的粗气流，d）将基本上由SiCl 4组成的部分流返回到冶金硅与SiCl 4和H 2的反应中， e）歧化含SiHCl3的部分流，以形成SiCl4和SiH4，以及f）将通过歧化形成的SiH 4返回至冶金硅与SiCl4和H2的反应，将含有三氯硅烷和四氯化硅的粗气流从固体释放至在用冷凝的氯硅烷洗涤之前可能通过气体过滤。冷凝氯硅烷的洗涤过程在单级蒸馏塔中在25至40巴的压力和至少150℃的温度下进行，并以0.1至3重量％含有三氯硅烷和四氯化硅的粗气流的％以基本上由SiCl 4组成的冷凝液相的形式回收，然后将该液相从SiCl4回路除去并在SiCl 4回路外扩张至1巴的压力，并冷却温度为10〜40℃，由此分离出溶解的杂质，然后通过过滤除去。

14. 发明授权

US06441108B1 Gas-phase polymerization in a bell-shaped reactor 失效
标题翻译：钟形反应器中的气相聚合
公开(公告)号：US06441108B1
公开(公告)日：2002-08-27
申请号：US09529069
申请日：2000-04-06
申请人： Friedrich Haendeler , Heiko Herold , Leslaw Mleczko , Claus Riehle , Franz-Josef Mersmann , Jürgen Schneider , Michael Dauben
发明人： Friedrich Haendeler , Heiko Herold , Leslaw Mleczko , Claus Riehle , Franz-Josef Mersmann , Jürgen Schneider , Michael Dauben
IPC分类号： C08F234
CPC分类号： C08F10/00 , B01J8/1872 , B01J8/24 , B01J2219/00087 , B01J2219/00108 , B01J2219/1946 , Y10S526/901 , Y10S526/918 , C08F2/01 , C08F2/34
摘要： The present invention relates to a process for the continuous discharge of pre-classified polymer particles, particularly rubber particles, from a gas phase polymerization reactor, comprising the steps of classifying the polymer in a classifier, discharging the particles with a sufficient size and conveying the undersized particles back into the gas phase polymerization reactor.
摘要翻译：本发明涉及一种从气相聚合反应器中连续排放预分解聚合物颗粒，特别是橡胶颗粒的方法，包括以下步骤：在分级机中分级聚合物，排出足够大小的颗粒并输送小尺寸的颗粒回到气相聚合反应器中。

15. 发明授权

US08614355B2 Catalyst and process for hydrogenating organic compounds 失效
标题翻译：用于氢化有机化合物的催化剂和方法
公开(公告)号：US08614355B2
公开(公告)日：2013-12-24
申请号：US12997301
申请日：2009-06-03
申请人： Aurel Wolf , Volker Michele , Jens Aβmann , Leslaw Mleczko
发明人： Aurel Wolf , Volker Michele , Jens Aβmann , Leslaw Mleczko
IPC分类号： C07C209/00
CPC分类号： C07C209/36 , B01J21/185 , B01J27/24 , B82Y30/00 , C07C211/46
摘要： The invention relates to a catalyst and to a process for hydrogenating organic compounds. In particular, the invention is directed to a process and catalyst for hydrogenating organic compounds with hydrogen. The organic compounds are subjected to hydrogenation in the presence of a catalyst comprising nitrogen-doped carbon nanotubes as a catalytically active component, wherein the proportion of nitrogen in the nanotubes is in the range of from about 0.05 to 20 wt. %.
摘要翻译：本发明涉及一种催化剂和一种氢化有机化合物的方法。特别地，本发明涉及用氢氢化有机化合物的方法和催化剂。有机化合物在含有掺杂氮的碳纳米管作为催化活性组分的催化剂存在下进行氢化，其中纳米管中的氮的比例在约0.05至20重量％的范围内。％。

16. 发明申请

US20130011328A1 PREPARATION OF CNTS 审中-公开
标题翻译： CNTS的准备
公开(公告)号：US20130011328A1
公开(公告)日：2013-01-10
申请号：US13574321
申请日：2011-01-20
申请人： Ralph Weber , Volker Michele , Leslaw Mleczko
发明人： Ralph Weber , Volker Michele , Leslaw Mleczko
IPC分类号： D01F9/12 , B82Y40/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/168
摘要： The present invention relates to a process comprising the steps a) synthesis of carbon nanotubes, b) optional inerting and c) cooling of the product. The process permits problem-free handling and packing of the carbon nanotube material that is produced.
摘要翻译：本发明涉及包括以下步骤的方法：a）碳纳米管的合成，b）任选的惰性化和c）产物的冷却。该方法允许无问题地处理和包装所生产的碳纳米管材料。

17. 发明申请

US20120256121A1 METHOD FOR PRODUCING GRAPHENE SOLUTIONS, GRAPHENE ALKALI METAL SALTS, AND GRAPHENE COMPOSITE MATERIALS 审中-公开
标题翻译：生产石墨溶液的方法，石墨烯金属盐和石墨复合材料
公开(公告)号：US20120256121A1
公开(公告)日：2012-10-11
申请号：US13508189
申请日：2010-11-08
申请人： Aurel Wolf , Giulio Lolli , Leslaw Mleczko , Oliver Felix-Karl Schluter
发明人： Aurel Wolf , Giulio Lolli , Leslaw Mleczko , Oliver Felix-Karl Schluter
IPC分类号： H01B1/04 , C09K5/00 , C01B31/30 , B82Y40/00 , B82Y30/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/19 , C01B32/194 , C01B32/196 , C01B2204/04
摘要： The present invention relates to a process for preparing graphene solutions by means of alkali metal salts, to graphene solutions, to processes for preparing graphene alkali metal salts, to graphene alkali metal salts and to graphene composite materials and to processes for producing the graphene composite materials.
摘要翻译：本发明涉及通过碱金属盐制备石墨烯溶液，石墨烯溶液，制备石墨烯碱金属盐的方法，石墨烯碱金属盐和石墨烯复合材料的方法以及用于生产石墨烯复合材料的方法。

18. 发明申请

US20120252662A1 NITROGEN DOPED CARBON NANOTUBES WITH METAL NANOPARTICLES 审中-公开
标题翻译：具有金属纳米颗粒的氮化碳纳米管
公开(公告)号：US20120252662A1
公开(公告)日：2012-10-04
申请号：US13515470
申请日：2010-12-14
申请人： Jens Assmann , Aurel Wolf , Leslaw Mleczko , Oliver Felix-Karl Schlueter
发明人： Jens Assmann , Aurel Wolf , Leslaw Mleczko , Oliver Felix-Karl Schlueter
IPC分类号： B01J31/02 , B01J37/16 , B82Y30/00 , B82Y40/00
CPC分类号： B01J21/185 , B01J23/42 , B01J35/006 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/174
摘要： The invention relates to nitrogen-doped carbon nanotubes (NCNT), the surface of which is charged with metal nanoparticles, and to a method for the production thereof and use thereof as a catalyst.
摘要翻译：本发明涉及其表面带有金属纳米颗粒的氮掺杂碳纳米管（NCNT）及其生产方法及其作为催化剂的用途。

19. 发明授权

US08168745B2 Process for the preparation of poly- and oligothiophenes on an industrial scale 失效
标题翻译：在工业规模下制备聚和低聚噻吩的方法
公开(公告)号：US08168745B2
公开(公告)日：2012-05-01
申请号：US12665917
申请日：2008-07-23
申请人： Björn Henninger , Frank Rauscher , Leslaw Mleczko
发明人： Björn Henninger , Frank Rauscher , Leslaw Mleczko
IPC分类号： C08G75/00
CPC分类号： C08G61/126
摘要： Process for industrial scale synthesis of poly- and oligothiophenes, which works in concentrated solution. In this process, a solution which comprises an organometallic thiophene reagent is added to a second solution which comprises a catalyst.
摘要翻译：用于工业规模合成多聚和低聚噻吩的方法，其在浓缩溶液中起作用。在该方法中，将包含有机金属噻吩试剂的溶液加入到包含催化剂的第二溶液中。

20. 发明授权

US07985395B2 Thermally stable catalyst for hydrogen chloride gas phase oxidation 失效
标题翻译：用于氯化氢气相氧化的热稳定催化剂
公开(公告)号：US07985395B2
公开(公告)日：2011-07-26
申请号：US12665848
申请日：2008-06-26
申请人： Aurel Wolf , Leslaw Mleczko , Oliver Felix-Karl Schlüter , Stephan Schubert
发明人： Aurel Wolf , Leslaw Mleczko , Oliver Felix-Karl Schlüter , Stephan Schubert
IPC分类号： C01B7/04 , B01J23/00 , B01J21/00 , B01J20/00
CPC分类号： B01J23/12 , B01J23/18 , B01J23/22 , B01J23/24 , B01J23/32 , B01J23/63 , B01J23/66 , B01J23/83 , B01J37/0201 , C01B7/04
摘要： Catalyst for oxidation reactions which comprises at least one constituent active in the catalysis of hydrogen chloride oxidation and support therefor, which support is based on uranium oxide. The catalyst is notable for a high stability and activity.
摘要翻译：用于氧化反应的催化剂，其包含至少一种在催化氯化氢氧化和活化的组分中的活性，所述催化剂基于氧化铀。催化剂具有很高的稳定性和活性。

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