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    • 123. 发明申请
    • Highly Efficient Material Spraying Type Carbon Nanostructure Synthesizing Method and Apparatus
    • 高效材料喷涂型碳纳米结构合成方法与装置
    • US20070253890A1
    • 2007-11-01
    • US11628304
    • 2004-06-04
    • Yoshikazu NakayamaTakeshi NagasakaToru SakaiTakeshi HayashiHiroyuki TsuchiyaXu LiToshikazu Nosaka
    • Yoshikazu NakayamaTakeshi NagasakaToru SakaiTakeshi HayashiHiroyuki TsuchiyaXu LiToshikazu Nosaka
    • C01B31/02D01F9/127
    • B82Y40/00B82Y30/00C01B32/05C01B32/152C01B32/162C01B32/18
    • Developed are a synthesizing method for carbon nanostructures where the generation of tar-like byproducts is reduced and carbon nanostructures are generated highly efficiently, and a unit therefor. A highly efficient material spraying type carbon nanostructure synthesizing apparatus according to the present invention is formed of a catalyst body that is placed inside a reaction tube, a heating unit that is provided in order to heat the vicinity of this catalyst body to the temperature range where carbon nanostructures are generated, a material gas supplying pipe for introducing a material gas into reaction tube which is provided in such a manner that an end of this supplying pipe is placed in proximity to catalyst body, and a preheating unit for preheating the material gas supplying pipe to a temperature range where no tar-like products are generated from a material gas. No tar-like substance is generated in the material gas supplying pipe, and the material gas is directly sprayed against the catalyst body, skipping the middle temperature range. Therefore, the probability of reaction occurring is high, and the yield in the generation of carbon nanostructures is high. Most of the material gas is consumed; thus, no tar-like substance is generated inside reaction tube.
    • 开发了碳纳米结构的合成方法,其中焦油样副产物的产生被减少并且碳纳米结构产生高效率,并且其单位。 根据本发明的高效材料喷涂型碳纳米结构合成装置由放置在反应管内的催化剂体形成,加热单元是为了将该催化剂体的附近加热到其温度范围, 产生碳纳米结构,用于将材料气体引入到反应管中的材料气体供给管,该反应管以使得该供给管的端部放置在催化剂体附近的方式设置,以及用于预热材料气体供给的预热单元 管道到材料气体不产生焦油状产品的温度范围。 在原料气体供给管中不产生焦油状物质,原料气体直接喷射在催化剂体上,跳过中间温度范围。 因此,反应发生的可能性高,碳纳米结构产生的产率高。 大部分原料气被消耗; 因此,在反应管内不产生焦油状物质。
    • 125. 发明申请
    • Method and apparatus for high-efficiency synthesis of carbon nanostructure, and carbon nanostructure
    • 用于高效合成碳纳米结构和碳纳米结构的方法和装置
    • US20070037370A1
    • 2007-02-15
    • US10551051
    • 2004-03-23
    • Osamu SuekaneToshikazu NosakaYoshikazu NakayamaLujun PanTakeshi NagasakaToru SakaiHiroyuki TsuchiyaToshiki GotoXu Li
    • Osamu SuekaneToshikazu NosakaYoshikazu NakayamaLujun PanTakeshi NagasakaToru SakaiHiroyuki TsuchiyaToshiki GotoXu Li
    • H01L21/20
    • B82Y30/00B82Y40/00C01B32/162C01B2202/30
    • Developed is high-efficiency synthesis method and apparatus capable of promoting the initial growth of carbon nanostructure by eliminating the initial fluctuation time and rising time in raw gas flow quantity. A high-efficiency synthesis method of carbon nanostructure according to the present invention is a high-efficiency synthesis method of carbon nanostructure, the method comprising: bringing raw material gas and a catalyst into contact with each other under reactive conditions so as to produce a carbon nanostructure, wherein: the initiation of contact of the raw material gas with the catalyst is carried out instantaneously. Reaction conditions such as temperature and raw material gas concentration are set so as to meet those for catalyst growth, and under the reaction conditions, the initiation of contact of raw material gas G with catalyst 6 is carried out instantaneously. Consequently, the initial growth of carbon nanostructure is positively carried out, and the height growth and thickness growth thereof can be effected in high efficiency. Further, high-density growth and short-time high-speed growth can be realized. The catalyst includes any forms of catalyst such as catalyst substrate, catalyst structure, catalyst powders and catalyst pellet. It is especially preferred to employ a system wherein the feed and interruption of the raw material gas G are intermittently controlled by means of an electromagnetic three-way valve 24.
    • 开发了通过消除原始气体流量的初始波动时间和上升时间,可以促进碳纳米结构初始生长的高效合成方法和装置。 根据本发明的碳纳米结构的高效合成方法是碳纳米结构的高效合成方法,该方法包括:使原料气体和催化剂在反应条件下彼此接触,以产生碳 纳米结构,其中:原料气体与催化剂的接触开始立即进行。 反应条件如温度和原料气体浓度设定为满足催化剂生长的条件,在反应条件下,原料气体G与催化剂6的接触开始立即进行。 因此,积极地进行碳纳米结构的初始生长,并且可以高效率地实现其高度生长和厚度生长。 此外,可以实现高密度生长和短时高速生长。 催化剂包括任何形式的催化剂,如催化剂底物,催化剂结构,催化剂粉末和催化剂颗粒。 特别优选采用通过电磁三通阀24间歇地控制原料气体G的进料和中断的系统。
    • 126. 发明授权
    • Efficient speakerphone anti-howling system
    • 高效扬声器防啸声系统
    • US5646990A
    • 1997-07-08
    • US531993
    • 1995-09-21
    • Xu Li
    • Xu Li
    • G10K15/00H03H17/00H04B3/20H04B3/23H04M1/60H04M9/08
    • H04M9/082
    • A cost-effective anti-howling system and method enables fast detection of the presence of true double talk, and substantially eliminates undesirable howling attributable to sudden changes in the acoustic echo path between a speakerphone microphone and loudspeaker during speakerphone conversations. Speakerphone embodiments include a delay-compensated and normalized cross-product calculation performed by a system processor having at least two memory buffers. One buffer is associated with the loudspeaker signal and the other buffer is associated with the microphone signal. The delay-compensated cross-product of the microphone voice signal input and the loudspeaker voice signal output is determined and normalized by energy estimates of the two signals to reduce the calculation error made by variance in the signal level.
    • 具有成本效益的反啸叫系统和方法能够快速检测真实双重通话的存在,并且基本上消除了由于扬声器话筒和扬声器之间的扬声器话音对话期间的声学回声路径的突然变化引起的不期望的嚎叫。 免提电话实施例包括由具有至少两个存储器缓冲器的系统处理器执行的延迟补偿和归一化的交叉乘积计算。 一个缓冲器与扬声器信号相关联,另一个缓冲器与麦克风信号相关联。 通过两个信号的能量估计来确定和归一化麦克风语音信号输入和扬声器语音信号输出的延迟补偿交叉积,以减少由信号电平的变化引起的计算误差。
    • 127. 发明授权
    • Device for collecting airborne particulate samples
    • 用于收集空气中颗粒样品的装置
    • US5243864A
    • 1993-09-14
    • US745686
    • 1991-08-16
    • George R. DunmyreCarol F. HagertyXu Li
    • George R. DunmyreCarol F. HagertyXu Li
    • G01N1/22G01N1/28
    • G01N1/2214G01N2001/2223G01N2001/2833
    • A collection device in which the particle collection surface, tacky due to the presence of aqueous polyvinyl alcohol thereon, is periodically or continually hydrated, rehydrated or replenished. This perpetuated hydration of the polyvinyl alcohol collection surface maintains particle collection effectiveness which would be reduced upon dehydration of the aqueous polyvinyl alcohol to a nontacky anhydrous polymer. In one preferred embodiment of the invention, the collection surface is kept in continuous saturation with aqueous polyvinyl alcohol by means of a wick connecting the collection surface and a reservoir of aqueous polyvinyl alcohol. Other hydration arrangements are included within the scope of the invention. The polyvinyl alcohol collection surface, with perpetuated hydration, enables reliable capture and retention of particles, and the polyvinyl alcohol itself does not interfere with analysis by SEM, TEM or other methods.
    • 收集装置,其中颗粒收集表面由于其上的聚乙烯醇水溶性的存在而发粘,定期或不断地水合,再水合或补充。 聚乙烯醇收集表面的这种持续的水合保持了颗粒收集效率,这将在将聚乙烯醇水溶液脱水成非粘性无水聚合物后降低。 在本发明的一个优选实施方案中,通过连接收集表面的芯和聚乙烯醇水溶液储存器将收集表面与聚乙烯醇水溶液连续饱和。 其他水合装置也包括在本发明的范围内。 具有持续水合的聚乙烯醇收集表面能够可靠地捕获和保留颗粒,并且聚乙烯醇本身不会通过SEM,TEM或其它方法干扰分析。