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    • 115. 发明授权
    • Amide derivatives
    • 酰胺衍生物
    • US06444849B1
    • 2002-09-03
    • US09469354
    • 1999-12-22
    • Ryoichi AndoMakoto KawamuraNoriko ChibaKazutoshi Watanabe
    • Ryoichi AndoMakoto KawamuraNoriko ChibaKazutoshi Watanabe
    • C07C23305
    • C07D307/79C07C237/42C07C2601/08C07C2601/14C07D209/18C07D317/60C07D333/60
    • A compound represented by the following general formula (1); wherein X represents R1(R2)(R3)C— where R1 represents a C3-C8 cycloalkyl group, an optionally substituted C6-C14 aryl group, an optionally substituted heterocyclic residue, an optionally substituted C6-C14 aryloxy group, or an optionally substituted C7-C15 arylmethyl group; R2 and R3 independently represent hydrogen atom or a C1-C5 alkyl group, or R2 and R3 may combine to represent a C2-C7 alkylene group; or X represents R7—A— wherein R7 represents (i) a C1-C10 alkyl group which may optionally be substituted with an optionally substituted C6-C14 aryl group, an optionally substituted fluorenyl group or an optionally substituted heterocyclic group, (ii) an optionally substituted C6-C14 aryl group or (iii) an optionally substituted heterocyclic group, and A represents an oxygen atom or —N—R8 where R8 represents hydrogen atom or a C1-C5 alkyl group, Y represents an oxygen atom or a sulfur atom, R4 and R5 independently represent hydrogen atom or a C1-C5 alkyl group; and R6 represents hydrogen atom, a C1-C5 alkyl group which may optionally be substituted with a hydroxyl group, a hydroxyl group or a C1-C5 alkoxy group, provided that the compounds wherein R7 is a benzyl group, A and Y are an oxygen atom, R4 and R5 are hydrogen atom, and R6 is a propyl group are excluded, or a salt thereof, or a solvate thereof or a hydrate thereof.
    • 由以下通式(1)表示的化合物:其中X表示R 1(R 2)(R 3)C-,其中R 1表示C 3 -C 8环烷基,任选取代的C 6 -C 14芳基,任选取代的杂环残基, 任选取代的C 6 -C 14芳氧基,或任选取代的C 7 -C 15芳基甲基; R2和R3独立地表示氢原子或C1-C5烷基,或R2和R3可以组合以表示C2-C7亚烷基; 或X表示R7-A,其中R7表示(i)可任选被任选取代的C 6 -C 14芳基取代的C 1 -C 10烷基,任选取代的芴基或任选取代的杂环基,(ii)任选地 取代的C 6 -C 14芳基或(iii)任选取代的杂环基,A表示氧原子或-N-R 8,其中R 8表示氢原子或C 1 -C 5烷基,Y表示氧原子或硫原子, R4和R5独立地表示氢原子或C1-C5烷基; 并且R 6表示氢原子,可任选被羟基,羟基或C 1 -C 5烷氧基取代的C 1 -C 5烷基,条件是其中R 7为苄基,A和Y为氧的化合物为氧 原子,R 4和R 5为氢原子,并且R 6为丙基,或其盐,或其溶剂合物或其水合物。
    • 117. 发明授权
    • Method for pattern dyeing of textile fabrics containing blends of
cellulose regenerated fiber
    • 含有纤维素再生纤维共混物的纺织品图案染色方法
    • US5902355A
    • 1999-05-11
    • US53079
    • 1998-04-01
    • Ituo KurahasiHiroaki TanibeKikuo KakizakiMakoto Kawamura
    • Ituo KurahasiHiroaki TanibeKikuo KakizakiMakoto Kawamura
    • D06P1/00D06P3/60D06P3/82D06P5/04D06P5/08D06P5/22D06P3/86D06P3/87
    • D06P3/8219D06P1/0096D06P3/6016D06P3/828D06P5/04D06P5/08D06P5/22Y10S8/921
    • A method for dying-finishing of textile fabrics which contain modified cellulose regenerated fiber capable of dyeing with cationic dyes which contains an insoluble polymer which is obtained by cross-linking a dihydroxydiphenylsulfone-sulfonate condensate with epoxy compounds having at least two epoxy groups in the molecule, and at least one kind of fiber selected from ordinary cellulose regenerated fiber, cotton and wool, the method comprising steps ofdying of the textile fabrics containing modified cellulose regenerated fiber with a dyeing solution containing cationic dyes alone or containing the cationic dyes and dyes other than cationic dyes by one-bath dying method, concentration of the cationic dyes being decided for the modified cellulose regenerated fiber weight and concentration of the dyes other than cationic dyes being decided for the whole weight of the textile fabric,treating the dyed textile fabric sequentially with an aqueous solution of tannic acid for applying tannic acid 1.5-7% of the weight of the modified cellulose regenerated fiber, and after thattreating it with an aqueous solution of tartar emetic for applying tartar emetic 0.5-2.5% of the weight of the modified cellulose regenerated fiber.
    • 一种纺织品的染色方法,其包含能够用阳离子染料染色的改性纤维素再生纤维的染色方法,所述改性纤维素再生纤维含有不溶性聚合物,其通过在分子中具有至少两个环氧基团的环氧化合物交联二羟基二苯基砜磺酸盐缩合物 以及选自普通纤维素再生纤维,棉和羊毛中的至少一种纤维,所述方法包括以下步骤:将含有改性纤维素再生纤维的纺织品染色为单独含有阳离子染料或含有阳离子染料和染料的染色溶液 比阳离子染料通过单浴染色方法,阳离子染料的浓度决定于改性纤维素再生纤维的重量,除了阳离子染料以外的染料的浓度决定于织物的整个重量,顺序地处理染色的织物 用单宁酸的水溶液施用丹宁酸 酸为改性纤维素再生纤维重量的1.5-7%,然后用鞑靼酒精水溶液处理,用于施用0.5〜2.5%改性纤维素再生纤维重量的鞑靼呕吐物。
    • 118. 发明授权
    • Microcapsule-containing oil-based coating liquid, ink, coated sheet, and
method of preparing the same
    • 含微胶囊的油性涂料液,油墨,涂布片及其制备方法
    • US5646203A
    • 1997-07-08
    • US413690
    • 1995-03-30
    • Kei EtohAkira HirasawaHisano HigurashiMakoto Kawamura
    • Kei EtohAkira HirasawaHisano HigurashiMakoto Kawamura
    • B41M5/165B41M5/28C09D11/02C08K5/053B32B5/18C08J9/32C08K7/22
    • C09D11/02B41M5/165B41M5/287Y10T428/249997Y10T428/2984Y10T428/2985Y10T428/2987Y10T428/2989
    • A microcapsule-containing oil-based coating liquid wherein the coating liquid comprises a hydrophobic core material-containing microcapsule particles dispersed individually in a state of primary particle in an oil varnish for ink use or a resin for coating use, and a solvent having an affinity for both the varnish or the resin and the surface of the microcapsule wall material in a state of having been attracted with the affinity to both the varnish or the resin and the surface layer of the microcapsule wall material. The preferred solvent is a lower divalent or multivalent alcohol.A preparative method of the foregoing coating liquid by utilizing vacuum distillation is also proposed.A sheet, like a duplicating sheet of paper coated with the foregoing oil-based coating liquid is further provided.According to the present invention, a water-based microcapsules system can be advantageously converted into an oil-based one without coagulating the primary microcapsule particles. There is no hardening and breakdown of the wall material during the process, and the original strength and the flexibility of the microcapsule wall material can be retained intact. Conventional pressure transferring-type printing machine may be employed to printing a selected area of the sheet.
    • 一种含微胶囊的油性涂布液,其中,所述涂布液包含分散在油墨用油性油墨中的一次粒子状态的分散的含疏水性芯材料的微胶囊粒子,或者涂布用树脂,以及具有亲和性的溶剂 对于清漆或树脂以及微胶囊壁材料的表面以与清漆或树脂和微胶囊壁材料的表面层的亲和性吸引的状态。 优选的溶剂是低级二价或多价醇。 还提出了通过利用真空蒸馏的上述涂布液的制备方法。 进一步提供如同涂覆有上述油性涂料的复印纸一样的片材。 根据本发明,可以有利地将水性微胶囊体系转化为油性微胶囊体系而不使一级微胶囊颗粒凝结。 在该过程中没有壁材料的硬化和分解,并且微胶囊壁材料的原始强度和柔韧性可以保持完整。 传统的压力传送型印刷机可用于印刷片材的选定区域。