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101. 发明授权

US4301166A Hydroxyethyl-azole compounds, their production and their medicinal use 失效
标题翻译：羟乙基唑化合物，其生产及其药用
公开(公告)号：US4301166A
公开(公告)日：1981-11-17
申请号：US92806
申请日：1979-11-09
申请人： Erik Regel , Karl H. Buchel , Ingo Haller , Manfred Plempel
发明人： Erik Regel , Karl H. Buchel , Ingo Haller , Manfred Plempel
IPC分类号： C07D249/04 , A61K31/40 , A61K31/41 , A61K31/415 , A61P31/04 , C07C29/40 , C07C45/46 , C07D233/60 , C07D249/08 , C07D521/00 , A01N43/50 , A01N43/82
CPC分类号： C07D231/12 , C07C29/40 , C07C45/46 , C07D249/08
摘要： The invention relates to hydroxyethyl-azole compounds and methods for their preparation. Also included in the invention are compositions containing said hydroxyethyl-azole compounds and methods for the use of said compounds and compositions as antimycotic agents.
摘要翻译：本发明涉及羟乙基唑化合物及其制备方法。本发明还包括含有所述羟乙基 - 唑类化合物的组合物和使用所述化合物和组合物作为抗真菌剂的方法。

102. 发明授权

US4278098A 2,6,6-Trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanols and -1,3-cyclohexadiene-1-methanols and organoleptic uses thereof 失效
标题翻译： 2,6,6-三甲基-α-（异）丙烯-1-环己烯-1-甲醇和1,3-环己二烯-1-甲醇及其感官用途
公开(公告)号：US4278098A
公开(公告)日：1981-07-14
申请号：US119858
申请日：1980-02-08
申请人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
发明人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
IPC分类号： A24B15/30 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C11B9/00 , A24B3/12 , A24B15/36
CPC分类号： C11B9/0034 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C07C403/08 , C07B2200/09 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma, smoking tobacco flavor and aroma and perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, smoking tobacco, perfume and perfumed article aroma and/or flavor imparting materials of 2,6,6-trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanol and -1,3-cyclohexadiene-1-methanol derivatives or one or more of their geometric or stereoisomers as defined by the generic structure: ##STR1## wherein one of R.sub.1, R.sub.2 or R.sub.3 is methyl and the other two of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; the dashed line is a carbon-carbon double bond or a carbon-carbon single bond; with the proviso that when R.sub.1 is hydrogen, the dashed line is a carbon-carbon double bond.Addition of one or more of the 2,6,6-trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanols or -1,3-cyclohexadiene-1-methanols of our invention to consumable materials is indicated to produce:A. In foodstuffs, chewing gums, toothpastes and medicinal products, sweet, camphoraceous, damascenone, raspberry-like, raspberry juice-like, rosey, woody/ionone-like, oriental, tobacco-like, tea-like, grape-like, fruity and ionone-like aromas and flavor notes;B. In perfumes, colognes and perfumed articles, leathery, hay, woody, mustard, minty, spicey (clove) and pulegone-like aromas and hay/tobacco and honey ionone-like topnotes with safronal-like nuances; andC. In tobaccos and tobacco flavors, a sweet-musty, hay-tobacco-like, fruity-raspberry, ionone-like aroma prior to smoking and a fruity tobacco-like, Virginia tobacco-like aroma on smoking both in the main stream and in the side stream.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和香气，吸烟烟草风味和香气以及香料和香料制品香气增强，增强和赋予组合物的方法和组合物; 以及2,6,6-三甲基-α-（异）丙烯基-1-环己烯-1-甲醇的食品，口香糖，牙膏，药用产品，吸烟烟草，香料和香料制品香气和/或调味材料，以及 -1,3-环己二烯-1-甲醇衍生物或其一般结构定义的其几何或立体异构体中的一种或多种：其中R 1，R 2或R 3中的一个为甲基，R 1，R 2和R 3中的另外两个为表示氢; 虚线是碳 - 碳双键或碳 - 碳单键; 条件是当R1是氢时，虚线是碳 - 碳双键。将本发明的一种或多种2,6,6-三甲基-α-（异）丙烯-1-环己烯-1-甲醇或-1,3-环己二烯-1-甲醇添加到消耗材料中被指示产生：A.在食品，口香糖，牙膏和药用产品中，甜，樟脑，大马士革，覆盆子样，覆盆子汁，玫瑰，木/紫罗兰酮样，东方，烟草状，茶状，葡萄状，水果和紫罗兰酮样香气和风味香气; B.香水，古龙水和香水制品，革质，干草，木质，芥末，小茴香，香料（丁香）和香菇样香气和干草/烟草和蜂蜜类似紫罗兰酮的顶峰，具有丰富的细微差别; 在烟草和烟草香料中，在吸烟之前是一种甜味，干草烟样，果香 - 覆盆子，类胡萝卜素的香气，并且在主流中吸烟时具有类似烟草般的弗吉尼亚烟草样香气并在旁边的流。

103. 发明授权

US4275087A Flavoring with 2,6,6-trimethyl-.alpha.-propenyl-1,3-cyclohexadiene-1-methanol substances 失效
标题翻译：用2,6,6-三甲基-α-丙烯基-1,3-环己二烯-1-甲醇物质调味
公开(公告)号：US4275087A
公开(公告)日：1981-06-23
申请号：US120102
申请日：1980-02-08
申请人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
发明人： Richard A. Wilson , William L. Schreiber , Braja D. Mookherjee , Jacob Kiwala , Joaquin F. Vinals , Manfred H. Vock , Gilbert Stork , Frederick L. Schmitt
IPC分类号： A23L27/20 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C11B9/00 , A23L1/226 , A23L1/235
CPC分类号： C11B9/0034 , A24B15/34 , C07C29/09 , C07C29/40 , C07C29/68 , C07C33/14 , C07C403/08 , C07B2200/09 , C07C2101/16
摘要： Processes and compositions are described for use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma, smoking tobacco flavor and aroma and perfume and perfumed article aroma augmenting, enhancing and imparting compositions; and as foodstuff, chewing gum, toothpaste, medicinal product, smoking tobacco, perfume and perfumed article aroma and/or flavor imparting materials of 2,6,6-trimethyl-.alpha.-(iso)propenyl-1-cyclohexene-1-methanol and -1,3-cyclohexadiene-1-methanol derivatives or one or more of their geometric or stereoisomers as defined by the generic structure: ##STR1## wherein one of R.sub.1, R.sub.2 or R.sub.3 is methyl and the other two of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; the dashed line is a carbon-carbon double bond or a carbon-carbon single bond; with the proviso that when R.sub.1 is hydrogen, the dashed line is a carbon-carbon double bond.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和香气，吸烟烟草风味和香气以及香料和香料制品香气增强，增强和赋予组合物的方法和组合物; 以及2,6,6-三甲基-α-（异）丙烯基-1-环己烯-1-甲醇的食品，口香糖，牙膏，药用产品，吸烟烟草，香料和香料制品香气和/或调味材料，以及 -1,3-环己二烯-1-甲醇衍生物或其一般结构定义的其几何或立体异构体中的一种或多种：其中R 1，R 2或R 3中的一个为甲基，R 1，R 2和R 3中的另外两个为表示氢; 虚线是碳 - 碳双键或碳 - 碳单键; 条件是当R1是氢时，虚线是碳 - 碳双键。

104. 发明授权

US4263149A 2-Oxabicyclooctane derivatives for augmenting or enhancing the flavor of foodstuffs 失效
标题翻译： 2-氧杂二环辛烷衍生物，用于增强或增强食品的风味
公开(公告)号：US4263149A
公开(公告)日：1981-04-21
申请号：US46361
申请日：1979-06-07
申请人： Mark A. Sprecker , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Mark A. Sprecker , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/40 , C07C29/40 , C07D493/08 , C11B9/00 , D06M13/18 , D06M13/16
CPC分类号： C07D493/08 , A24B15/403 , C07C29/40 , C11B9/0034 , C11B9/008 , C07C2101/16
摘要： Described are derivatives of 2-oxabicyclo[2.2.2]octanes and precursors therefor, cyclohexenemethanols as well as lower alkyl esters of said cyclohexenemethanols. The oxabicyclooctanes are useful in perfumery and foodstuff, medicinal product and tobacco flavors. The cyclohexenemethanols are useful as precursors for the oxabicyclooctanes and are, themselves, useful for their organoleptic properties in perfumery and flavors as are the esters of said cyclohexenemethanols.
摘要翻译：描述的是2-氧杂二环[2.2.2]辛烷及其前体，环己烯甲醇以及所述环己烯甲醇的低级烷基酯的衍生物。氧杂双环辛烷可用于香料和食品，药用产品和烟草香精。环己烯甲醇可用作氧杂双环辛烷的前体，它们本身可用于香料和香料中的感官特性，以及所述环己烯甲醇的酯类。

105. 发明授权

US4256121A Use of 2-oxabicyclooctane derivatives in augmenting or enhancing the aroma or taste of smoking tobacco and smoking tobacco articles 失效
标题翻译：使用2-氧杂二环辛烷衍生物来增强或增强吸烟烟草和烟草制品的香气或味道
公开(公告)号：US4256121A
公开(公告)日：1981-03-17
申请号：US49205
申请日：1979-06-15
申请人： Mark A. Sprecker , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Mark A. Sprecker , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A23L27/20 , A24B15/34 , A24B15/40 , C07C29/40 , C07D493/08 , C07F3/02 , A24B3/12
CPC分类号： C07D493/08 , A23L27/2052 , A24B15/345 , C07C29/40 , C07C403/08 , C07F3/02 , C07C2101/16
摘要： Described is a process for augmenting or enhancing the aroma or taste of a smoking tobacco comprising the step of intimately admixing with a smoking tobacco, an aroma or taste augmenting or enhancing quantity of an oxabicyclo chemical compound having the structure: ##STR1## wherein R.sub.2 is C.sub.2 -C.sub.5 alkyl or alkenyl; R.sub.4 is hydrogen, methyl or ethyl; R.sub.7 is hydrogen or methyl; and R.sub.8 is hydrogen or methyl with the proviso that when R.sub.4 is methyl or ethyl R.sub.7 and R.sub.8 are not both hydrogen and that at least one of R.sub.7 and R.sub.8 is methyl.Also described is a smoking tobacco article comprising a cylindrical shaped mass of smoking tobacco encased in a wrapper, said wrapper and said smoking tobacco being in contact with a porous filter, and being in intimate contact with either said filter, said wrapper or said shaped tobacco mass, at least one oxabicyclo chemical compound having the structure: ##STR2## wherein R.sub.2 is C.sub.2 -C.sub.5 alkyl or alkenyl; R.sub.4 is hydrogen, methyl or ethyl; R.sub.7 is hydrogen or methyl with the proviso that when R.sub.4 is methyl or ethyl, R.sub.7 and R.sub.8 are not both hydrogen and that at least one of R.sub.7 and R.sub.8 is methyl.
摘要翻译：描述了用于增强或增强烟草香气或味道的方法，其包括与吸烟烟草，香味或味道增强或增强量的具有以下结构的氧杂双环化合物紧密混合的步骤：其中R2是 C 2 -C 5烷基或烯基; R4是氢，甲基或乙基; R7是氢或甲基; 并且R 8是氢或甲基，条件是当R 4是甲基或乙基时，R 7和R 8不是氢，并且R 7和R 8中的至少一个是甲基。还描述了一种烟草制品，其包括包裹在包装纸中的吸烟烟草的圆柱形块状物，所述包装物和所述吸烟烟草与多孔过滤器接触，并与所述过滤器，所述包装物或所述成形烟草紧密接触至少一种具有以下结构的氧杂双环化合物：其中R2是C2-C5烷基或烯基; R4是氢，甲基或乙基; R 7是氢或甲基，条件是当R 4是甲基或乙基时，R 7和R 8不都是氢，并且R 7和R 8中的至少一个是甲基。

106. 发明授权

US4247423A Cyclohexenemethanols and their lower esters in perfume compositions 失效
标题翻译：环己烯甲醇及其在香料组合物中的低级酯
公开(公告)号：US4247423A
公开(公告)日：1981-01-27
申请号：US85891
申请日：1979-10-17
申请人： Mark A. Sprecker , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
发明人： Mark A. Sprecker , Frederick L. Schmitt , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala
IPC分类号： A24B15/40 , C07C29/40 , C07D493/08 , C11B9/00 , A61K7/46
CPC分类号： C07D493/08 , A24B15/403 , C07C29/40 , C11B9/0034 , C11B9/008 , C07C2101/16
摘要： Described are derivatives of 2-oxabicyclo[2.2.2]octanes and precursors therefor, cyclohexenemethanols as well as lower alkyl esters of said cyclohexenemethanols. The oxabicyclooctanes are useful in perfumery and foodstuff, medicinal product and tobacco flavors. The cyclohexenemethanols are useful as precursors for the oxabicyclooctanes and are, themselves, useful for their organoleptic properties in perfumery and flavors as are the esters of said cyclohexenemethanols.
摘要翻译：描述的是2-氧杂二环[2.2.2]辛烷及其前体，环己烯甲醇以及所述环己烯甲醇的低级烷基酯的衍生物。氧杂双环辛烷可用于香料和食品，药用产品和烟草香精。环己烯甲醇可用作氧杂双环辛烷的前体，它们本身可用于香料和香料中的感官特性，以及所述环己烯甲醇的酯类。

107. 发明授权

US4239765A Fluorenyl-azolylmethyl-carbinol compounds and their medicinal use 失效
标题翻译：芴基 - 唑基甲基 - 甲醇化合物及其药用
公开(公告)号：US4239765A
公开(公告)日：1980-12-16
申请号：US92804
申请日：1979-11-09
申请人： Erik Regel , Karl Buchel , Ingo Haller , Manfred Plempel
发明人： Erik Regel , Karl Buchel , Ingo Haller , Manfred Plempel
IPC分类号： A61K31/40 , A61K31/41 , A61K31/415 , A61P31/04 , C07C29/40 , C07C49/813 , C07D233/60 , C07D249/08 , C07D521/00 , C07D249/12
CPC分类号： C07D231/12 , C07C29/40 , C07C49/813 , C07D249/08 , C07C2103/18
摘要： The invention relates to fluorenylazolylmethylcarbinols and methods for their preparation. Also included are compositions containing said fluorenylazolylmethyl-carbinols and methods for the use of said carbinols and compositions containing them as antimycotic agents.
摘要翻译：本发明涉及芴基唑基甲基甲醇及其制备方法。还包括含有所述芴基甲基 - 甲醇的组合物和使用所述甲醇的方法和含有它们的组合物作为抗真菌剂。

108. 发明授权

US4219489A Synthesis of steroids 失效
标题翻译：类固醇的合成
公开(公告)号：US4219489A
公开(公告)日：1980-08-26
申请号：US939595
申请日：1978-09-05
申请人： William S. Johnson , Leonard A. Bunes
发明人： William S. Johnson , Leonard A. Bunes
IPC分类号： C07C29/00 , C07C29/10 , C07C29/147 , C07C29/36 , C07C29/40 , C07C29/58 , C07C33/30 , C07C35/21 , C07C45/29 , C07C45/59 , C07C45/66 , C07C45/67 , C07D309/08 , C07D317/12 , C07D339/06 , C07F9/655 , C07J1/00 , C07J9/00 , C07J11/00 , C07J61/00
CPC分类号： C07J61/00 , C07C29/00 , C07C29/103 , C07C29/147 , C07C29/36 , C07C29/40 , C07C29/58 , C07C33/30 , C07C35/21 , C07C403/02 , C07C45/292 , C07C45/59 , C07C45/66 , C07C45/67 , C07C45/676 , C07D309/08 , C07D317/12 , C07D339/06 , C07F9/65525 , C07J1/0011 , C07J1/0014 , C07J11/00 , C07J9/00 , C07B2200/09 , C07C2101/02 , C07C2101/16 , C07C2102/24
摘要： Method and compounds are provided for use in the synthesis of steroids wherein a polyolefin is provided having an initiating group having a chalcogen atom in juxtaposition to a double bond, so as to be capable of bond formation to close to form a ring and having a terminating group involving pi unsaturation (a double or triple bond) conjugated to an aromatic ring. Upon acid catalysis, sigma bonds are formed through the interaction of a carbocation formed at the carbon atom bonded to the chalcogen atom and the double bond intermediate the initiating group and the terminating group, which close to form rings of a steroid nucleus, the carbocation interacting with the pi unsaturation conjugated with the aromatic group and being captured by a nucleophile present in the acidic reaction medium. The resulting steroid product may then be modified in known ways to produce known steroids.
摘要翻译：提供了用于合成类固醇的方法和化合物，其中提供了具有与双键并列的具有硫属原子的引发基团的聚烯烃，以便能够形成键以形成环并具有终止涉及与芳环缀合的不饱和键（双键或三键）的基团。在酸催化下，σ键通过在与硫属原子键合的碳原子上形成的碳阳离子和接近形成类固醇核环的起始基团和末端基团之间的双键的相互作用形成，碳阳离子相互作用其中pI不饱和键与芳族基团共轭并被存在于酸性反应介质中的亲核试剂捕获。然后可以以已知的方式修饰所得类固醇产物以产生已知的类固醇。

109. 发明授权

US4211870A Preparation of substituted 2-aminopyrazines 失效
标题翻译：取代的2-氨基吡嗪的制备
公开(公告)号：US4211870A
公开(公告)日：1980-07-08
申请号：US27630
申请日：1979-04-06
申请人： Charles J. Barnett , Thomas L. Emmick , Richard C. Hoying
发明人： Charles J. Barnett , Thomas L. Emmick , Richard C. Hoying
IPC分类号： C07D241/26 , C07C17/35 , C07C29/40 , C07C33/20 , C07D241/20
CPC分类号： C07C29/40 , C07C17/35 , C07C255/00 , C07C33/20 , C07D241/20 , C12C11/02
摘要： Preparation of substituted 2-aminopyrazines by reaction of an .alpha.-chloro or .alpha.-bromo oxime with an aminoacetonitrile in the presence of an acid-uptake agent, followed by separation of the intermediate novel hydroxyimino-substituted aminoacetonitrile, and cyclization thereof with acid.
摘要翻译：通过在酸吸收剂存在下，通过α-氯或α-溴肟与氨基乙腈的反应制备取代的2-氨基吡嗪，然后分离中间体新的羟基亚氨基取代的氨基乙腈，并用酸环化。

110. 发明授权

US4210767A 2,2,3-Trimethyl-3-cyclopenten-1-ylalkenyl and alkylidene secondary alkanols, alkanones, cycloalkanols and cycloalkanones, organoleptic uses thereof in perfume compositions, colognes and perfumed articles and process for producing same 失效
标题翻译： 2,2,3-三甲基-3-环戊烯-1-基烯基和亚烷基仲链烷醇，链烷酮，环烷醇和环烷酮，在香料组合物，古龙水和香料制品中的感官用途及其制备方法
公开(公告)号：US4210767A
公开(公告)日：1980-07-01
申请号：US23442
申请日：1979-03-23
申请人： Takao Yoshida , Braja D. Mookherjee , Venkatesh Kamath , John B. Hall , William I. Taylor , Frederick L. Schmitt
发明人： Takao Yoshida , Braja D. Mookherjee , Venkatesh Kamath , John B. Hall , William I. Taylor , Frederick L. Schmitt
IPC分类号： C07C29/143 , C07C29/17 , C07C29/40 , C07C35/21 , C07C45/74 , C07C49/653 , C11B9/00 , C07C45/00 , C07C29/00
CPC分类号： C11B9/0034 , C07C29/143 , C07C35/21 , C07C45/74 , C07C49/653 , C11B9/003 , C07B2200/09 , C07C2101/08 , C07C2101/10 , C07C2101/14
摘要： Described are perfume and fragrance compositions and perfumed articles including soaps, detergents, powders as well as colognes containing 2,2,3-trimethyl-3-cyclopenten-1-ylalkenyl and alkylidene secondary alkanols, alkanones, cycloalkanols and cycloalkanones having the generic structure: ##STR1## wherein one of the lines + + + + + is a carbon-carbon double bond and the other of the lines + + + + + is a carbon-carbon single bond; wherein X is carbinol having the structure: ##STR2## or carbonyl having the structure ##STR3## wherein A' is hydrogen, CH.sub.3, C.sub.2 H.sub.5 or --CH.sub.2 --; wherein B' is hydrogen,CH.sub.3, C.sub.2 H.sub.5 or --CH.sub.2 --; where n is 0, 1 or 2; wherein each of the dashed lines are the same and each represents a carbon-carbon single bond or no bond; wherein A' and B' are both --CH.sub.2 -- when n is 1 or 2 and the dashed line is a carbon-carbon single bond or A' is hydrogen and B' is C.sub.2 H.sub.5 or CH.sub.3 or both A' and B' are each CH.sub.3 or A' is C.sub.2 H.sub.5 and B' is CH.sub.3 when n is 0 and the dashed line represents no bond, which imparts thereto rich, musky, cedar woody, sandalwood, sweet, floral, ionone-like, soft-fruity (apricot), green and earthy aromas with resinous topnotes and nutty oily nuances. Also described is a process for preparing such compounds according to the reaction schemes: ##STR4## wherein the lines + + + + + A', B', the dashed lines and n are as defined above wherein M is alkaline metal.
摘要翻译：描述了香料和香料组合物和包含肥皂，洗涤剂，粉末以及含有具有以下通用结构的2,2,3-三甲基-3-环戊烯-1-基烯基和亚烷基仲链烷醇，链烷酮，环烷醇和环烷酮的香水制品，其中线+ + + + +之一是碳 - 碳双键，另一条线+ + + + + +是碳 - 碳单键; 其中X是具有以下结构的甲醇：具有结构的羰基，其中A'是氢，CH 3，C 2 H 5或-CH 2 - ; 其中B'是氢，CH 3，C 2 H 5或-CH 2 - ; 其中n为0,1或2; 其中每个虚线相同并且各自表示碳 - 碳单键或无键; 其中当n为1或2并且虚线为碳 - 碳单键或A'为氢且B'为C 2 H 5或CH 3时，A'和B'均为-CH 2 - ，或者A'和B'均为CH 3 或A'为C 2 H 5，B'为CH 3，n为0，虚线表示无键，赋予其丰富，麝香，雪松木香，檀香，甜，花，紫罗兰酮，软果（杏），绿和土质的香气与树脂的顶部和坚果油的细微差别。还描述了根据以下反应方案制备这些化合物的方法：其中线+ + + + + A'，B'，虚线和n如上所定义，其中 M是碱金属。

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