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101. 发明申请

US20090163681A1 Fast Activating Catalyst 有权
标题翻译：快速活化催化剂
公开(公告)号：US20090163681A1
公开(公告)日：2009-06-25
申请号：US11963530
申请日：2007-12-21
申请人： Max P. McDaniel , Elizabeth A. Benham , Ted Cymbaluk , George Neil
发明人： Max P. McDaniel , Elizabeth A. Benham , Ted Cymbaluk , George Neil
IPC分类号： C08F4/18
CPC分类号： C08F10/00 , B01J21/08 , B01J23/26 , B01J35/1019 , B01J35/1047 , B01J35/1061 , B01J37/0207 , B01J37/036 , B01J37/06 , C08F110/02 , C08F4/025 , C08F4/78 , C08F2500/09 , C08F2500/12 , C08F2500/17 , C08F2500/07
摘要： A method of preparing a catalyst comprising aging a silica support in an alkaline solution to produce an alkaline aged silica support, removing at least a portion of the alkaline solution from the alkaline aged silica support to produce a dried silica support, and activating the silica support to produce a catalyst composition, wherein alkaline aging lowers the surface area of the silica support to less than about 50% of the original value and wherein activation of the silica support is carried out in batches of equal to or greater than about 500 lbs for a time period of less than about 8 hours. A method of preparing a polymer comprising alkaline aging a silica support material, adding chromium to the silica support material prior to the alkaline aging, after the alkaline aging, or both to form a chromium-silica support, rapidly activating the chromium-silica support produce an activated olefin polymerization catalyst, contacting the activated olefin polymerization catalyst with at least one monomer in a reaction zone under conditions suitable to produce a polymer, and recovering the polymer.
摘要翻译：一种制备催化剂的方法，包括在碱性溶液中老化二氧化硅载体以产生碱性老化二氧化硅载体，从碱性老化二氧化硅载体除去至少一部分碱性溶液以产生干燥二氧化硅载体，并活化二氧化硅载体以产生催化剂组合物，其中碱性老化将二氧化硅载体的表面积降低到小于原始值的约50％，并且其中二氧化硅载体的活化以等于或大于约500lb的批次进行，用于时间段少于约8小时。一种制备聚合物的方法，其包括使二氧化硅载体材料碱性老化，在碱性老化之前，碱性老化之后向二氧化硅载体材料中加入铬，或者二者形成铬二氧化硅载体，快速活化铬 - 二氧化硅载体产物活化烯烃聚合催化剂，在适合于生产聚合物的条件下，在反应区中使活化烯烃聚合催化剂与至少一种单体接触，并回收聚合物。

102. 发明申请

US20080287287A1 METHODS OF PREPARING A POLYMERIZATION CATALYST 有权
标题翻译：制备聚合催化剂的方法
公开(公告)号：US20080287287A1
公开(公告)日：2008-11-20
申请号：US11749663
申请日：2007-05-16
申请人： Max P. McDaniel , Elizabeth A. Benham , Randall S. Muninger
发明人： Max P. McDaniel , Elizabeth A. Benham , Randall S. Muninger
IPC分类号： B01J31/14 , C01B17/96 , C01F7/02
CPC分类号： C08F10/00 , B01J21/04 , B01J27/053 , B01J35/1019 , B01J35/1047 , C08F4/65912 , C08F4/65916 , C08F4/65927 , C08F110/02 , Y10S526/943 , C08F4/65922 , C08F4/025 , C08F2500/12
摘要： A method of preparing a composition comprising dry mixing commercial grade alumina and a solid sulfating agent to form a mixture and calcining the mixture to form a sulfated alumina support.
摘要翻译：一种制备组合物的方法，其包括将市售级氧化铝和固体硫酸盐干混，以形成混合物并煅烧所述混合物以形成硫酸化氧化铝载体。

103. 发明授权

US07271124B2 Process to produce polymers 有权
标题翻译：生产聚合物的方法
公开(公告)号：US07271124B2
公开(公告)日：2007-09-18
申请号：US10877191
申请日：2004-06-25
申请人： Max P. McDaniel , Elizabeth A. Benham , Al R. Wolfe
发明人： Max P. McDaniel , Elizabeth A. Benham , Al R. Wolfe
IPC分类号： B01J27/132
CPC分类号： C08F10/00 , C08F10/02 , C08F210/16 , C08F2410/04 , C08F4/69 , C08F4/646 , C08F4/24 , C08F210/14 , C08F2500/12 , C08F2500/07
摘要： A process to produce ethylene polymers is provided.
摘要翻译：提供了生产乙烯聚合物的方法。

104. 发明授权

US07071276B2 Process to produce polymers 有权
公开(公告)号：US07071276B2
公开(公告)日：2006-07-04
申请号：US10319393
申请日：2002-12-13
申请人： Max P. McDaniel , Elizabeth A. Benham , Al R. Wolfe
发明人： Max P. McDaniel , Elizabeth A. Benham , Al R. Wolfe
IPC分类号： C08F110/02
CPC分类号： C08F10/00 , C08F10/02 , C08F210/16 , C08F2410/04 , C08F4/69 , C08F4/646 , C08F4/24 , C08F210/14 , C08F2500/12 , C08F2500/07
摘要： A process to produce ethylene polymers is provided.

105. 发明授权

US06855781B2 Process to produce polymers 有权
标题翻译：生产聚合物的方法
公开(公告)号：US06855781B2
公开(公告)日：2005-02-15
申请号：US10355560
申请日：2003-01-31
申请人： Joseph J. Bergmeister , Steven J. Secora , Elizabeth A. Benham , Max P. McDaniel
发明人： Joseph J. Bergmeister , Steven J. Secora , Elizabeth A. Benham , Max P. McDaniel
IPC分类号： C08F4/02 , C08F4/69 , C08F10/00 , C08F10/02 , C08F210/16 , C08F4/643
CPC分类号： C08F10/02 , C08F210/16 , Y10T428/1352 , C08F4/69 , C08F210/14 , C08F2500/12 , C08F2500/07 , C08F2500/04 , C08F2500/13 , C08F2500/14 , C08F4/025 , C08F4/24
摘要： A process to produce ethylene polymers is provided. Particularly, a process to produce ethylene polymers having a broad molecular weight distribution is provided. More particularly, a process to produce ethylene polymers that have low formation of smoke and odor during blow molding is provided.
摘要翻译：提供了生产乙烯聚合物的方法。特别地，提供了生产具有宽分子量分布的乙烯聚合物的方法。更具体地，提供了一种生产在吹塑过程中具有低烟雾和气味形成的乙烯聚合物的方法。

106. 发明授权

US06197899B1 Olefin polymerization 失效
标题翻译：烯烃聚合
公开(公告)号：US06197899B1
公开(公告)日：2001-03-06
申请号：US08395125
申请日：1995-02-27
申请人： Kent E. Mitchell , Max P. McDaniel , M. Bruce Welch , Elizabeth A. Benham , Grover W. Cone
发明人： Kent E. Mitchell , Max P. McDaniel , M. Bruce Welch , Elizabeth A. Benham , Grover W. Cone
IPC分类号： C08F206
CPC分类号： C08F10/00 , Y10S526/904 , C08F4/6492 , C08F4/6555 , C08F4/6583
摘要： A process is disclosed for the particle form polymerization of olefins. The process employs a titanium-containing having hydrocarbon soluble titanium components. The resulting catalyst is pretreated with an organometallic reducing agent prior to the introduction of the catalyst into the polymerization zone to give a catalyst which can be used satisfactorily in a loop reactor with lower levels of cocatalyst.
摘要翻译：公开了用于烯烃的颗粒形式聚合的方法。该方法采用含有可溶解钛组分的钛。在将催化剂引入聚合区之前，将所得催化剂用有机金属还原剂预处理，得到可在具有较低水平助催化剂的环管反应器中令人满意地使用的催化剂。

107. 发明授权

US5595953A Chromium catalyst compositions 失效
标题翻译：铬催化剂组合物
公开(公告)号：US5595953A
公开(公告)日：1997-01-21
申请号：US486872
申请日：1995-06-07
申请人： Max P. McDaniel , Elizabeth A. Benham , Rickey D. Badley
发明人： Max P. McDaniel , Elizabeth A. Benham , Rickey D. Badley
IPC分类号： C08F4/22 , C08F4/02 , C08F4/06 , C08F4/24 , C08F4/69 , C08F10/00 , C08F210/02 , B01J21/08
CPC分类号： C08F10/00
摘要： Chromium catalyst compositions are provided. Theses chromium catalyst compositions can be used to polymerized olefins. The resulting polymerization product can have improved properties.
摘要翻译：提供了铬催化剂组合物。这些铬催化剂组合物可用于聚合烯烃。所得聚合产物可具有改进的性能。

108. 发明授权

US5459203A Ethylene cone-shell polymer powders 失效
标题翻译：乙烯锥壳聚合物粉末
公开(公告)号：US5459203A
公开(公告)日：1995-10-17
申请号：US336037
申请日：1994-11-08
申请人： Rolf L. Geerts , Elizabeth A. Benham , Max P. McDaniel
发明人： Rolf L. Geerts , Elizabeth A. Benham , Max P. McDaniel
IPC分类号： C08F4/22 , C08F4/06 , C08F4/42 , C08F4/54 , C08F4/60 , C08F4/69 , C08F10/00 , C08F255/02 , C08F110/02
CPC分类号： C08F10/00 , Y10S525/902 , Y10S526/905
摘要： A catalyst system for the polymerization of alpha-olefins comprising a chromium-containing catalyst and an yttrium-containing catalyst wherein the yttrium-containing catalyst is represented by the formula (Cp.sub.2 YX.sub.x).sub.y .multidot.M.sub.z L.sub.n, wherein Cp is cyclopentadienyl or cyclopentadienyl substituted with an alkyl or alkyl silyl radical, X is a halogen, M is an alkali metal, L is a suitable electron donor ligand, x is 1 or 2, y is 1 or 2, z is 0 or 1, and n is a number corresponding to the value needed to form a stable complex, with the proviso that when y is 2, z and n are 0 is provided. Also disclosed is a polymerization process employing such a catalyst system, and novel olefin polymers. Polymers thus produced exhibit high bulk density and a broad molecular weight distribution.
摘要翻译：包含含铬催化剂和含钇催化剂的α-烯烃聚合催化剂体系，其中含钇催化剂由式（Cp2YXx）yxMzLn表示，其中Cp是环烷基或被烷基取代的环戊二烯基，烷基甲硅烷基，X是卤素，M是碱金属，L是合适的电子给体配体，x是1或2，y是1或2，z是0或1，并且n是对应于数值需要形成稳定的络合物，条件是当y为2时，z和n为0。还公开了使用这种催化剂体系的聚合方法和新的烯烃聚合物。如此制备的聚合物表现出高的堆积密度和宽的分子量分布。

109. 发明授权

US5364915A Ethylene polymerization process 失效
标题翻译：乙烯聚合工艺
公开(公告)号：US5364915A
公开(公告)日：1994-11-15
申请号：US950525
申请日：1992-09-25
申请人： Elizabeth A. Benham , Max P. McDaniel
发明人： Elizabeth A. Benham , Max P. McDaniel
IPC分类号： C08F4/69 , C08F4/60 , C08F10/00 , C08F10/02 , C08F4/78
CPC分类号： C08F10/02
摘要： A process to produce a polyethylene composition that has less than 2 weight percent fines, based on the weight of said polyethylene composition, and a fluff bulk density greater than 25 pounds per cubic foot, said process comprising polymerizing ethylene in the presence of a trialkylaluminum compound, and a diluent that is essentially saturated with ethylene under slurry polymerization conditions that comprise a polymerization temperature from 104.degree. C. to 116.degree. C., with an activated catalyst system comprising (a) a catalyst support that comprises a silica compound, wherein said catalyst support has a pore volume less than 2 cubic centimeters per gram, (b) a catalyst that comprises a chromium compound, wherein the amount of chromium in said catalyst system is from about 0.1 to about 20 weight percent, wherein said weight percent is based on the total weight of said catalyst and catalyst support, and (c) a fluorine compound, wherein the amount of fluorine used is from about 0.1 to about 20 weight percent, wherein said weight percent is based on the total weight of said catalyst support.
摘要翻译：一种制备基于所述聚乙烯组合物重量小于2重量％的细粉和大于25磅/立方英尺的绒毛体积密度的聚乙烯组合物的方法，所述方法包括在三烷基铝化合物存在下聚合乙烯和在包含聚合温度为104℃至116℃的淤浆聚合条件下基本上用乙烯饱和的稀释剂，其中活化催化剂体系包含（a）包含二氧化硅化合物的催化剂载体，其中所述催化剂载体具有小于2立方厘米/克的孔体积，（b）包含铬化合物的催化剂，其中所述催化剂体系中的铬的量为约0.1至约20重量％，其中所述重量百分比为基所述催化剂和催化剂载体的总重量，和（c）氟化合物，其中使用的氟的量为约0.1〜的20重量％，其中所述重量百分数是基于所述催化剂载体的总重量。

110. 发明授权

US4988657A Process for olefin polymerization 失效
标题翻译：烯烃聚合方法
公开(公告)号：US4988657A
公开(公告)日：1991-01-29
申请号：US417954
申请日：1989-10-06
申请人： Shirley J. Martin , Elizabeth A. Benham , Max P. McDaniel , Bruce W. Gerhold
发明人： Shirley J. Martin , Elizabeth A. Benham , Max P. McDaniel , Bruce W. Gerhold
IPC分类号： C08F4/24 , C08F4/623 , C08F10/00 , C08F110/02
CPC分类号： C08F10/00 , C08F110/02
摘要： Olefins are polymerized with a catalyst composition which forms on mixing a supported chromium oxide catalyst system and a silane compound. This composition allows the production of one or more comonomers in-situ. The resultant polymer has a lower density, a higher melt index, and a higher high load melt index than polymers produced with a similar catalyst system in the absence of a silane compound.

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