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91. 发明授权

US08007652B2 Method for collection of valuable metal from ITO scrap 有权
标题翻译：从ITO废料中收集贵重金属的方法
公开(公告)号：US08007652B2
公开(公告)日：2011-08-30
申请号：US12445776
申请日：2007-06-27
申请人： Yuichiro Shindo , Kouichi Takemoto
发明人： Yuichiro Shindo , Kouichi Takemoto
IPC分类号： C25C1/00 , C25C1/14 , C25C1/22 , C25C5/02 , C01G19/00 , C01G15/00 , C22B25/00 , C22B58/00 , C25B11/04
CPC分类号： C25C1/24 , C22B3/045 , C22B7/006 , C22B25/06 , C22B58/00 , Y02P10/228 , Y02P10/234
摘要： Proposed is a method for collecting valuable metal from an ITO scrap including the steps of subjecting the ITO scrap to electrolysis and collecting the result as indium-tin alloy. Additionally provided is a method for collecting valuable metal from an ITO scrap including the steps of providing an ITO electrolytic bath and an indium-tin alloy collecting bath, dissolving the ITO in the electrolytic bath, and thereafter collecting indium-tin alloy in the indium-tin alloy collecting bath. These methods enable the efficient collection of indium-tin alloy from an ITO scrap of an indium-tin oxide (ITO) sputtering target or an ITO scrap such as ITO mill ends arisen during the manufacture of such ITO sputtering target.
摘要翻译：提出了从ITO废料中收集有价金属的方法，包括以下步骤：对ITO废料进行电解处理，并将结果作为铟锡合金进行收集。另外提供了一种从ITO废料中收集有价金属的方法，包括以下步骤：提供ITO电解槽和铟 - 锡合金收集槽，将ITO溶解在电解槽中，然后在铟 - 锡合金收集浴。这些方法使得能够在ITO溅射靶的制造期间从铟锡氧化物（ITO）溅射靶的ITO废料或诸如ITO研磨端的ITO废料有效收集铟锡合金。

92. 发明授权

US07601247B2 Falling bed cathode cell for metal electrowinning 失效
标题翻译：用于金属电解沉积的倒床阴极电池
公开(公告)号：US07601247B2
公开(公告)日：2009-10-13
申请号：US10561560
申请日：2004-06-23
申请人： Douglas J. Robinson , Stacey A. MacDonald , Davide Scotti , Francesco Todaro
发明人： Douglas J. Robinson , Stacey A. MacDonald , Davide Scotti , Francesco Todaro
IPC分类号： C25C7/02 , C25C7/00 , C25C1/12 , C25C1/08 , C25C1/14 , C25C1/16 , C25C1/10
CPC分类号： C25C7/002 , C25C5/02
摘要： A cell (100) for metal electrowinning from metal ion solutions is described, wherein the cathode (1) consists of a falling bed of growing beads; the beads, withdrawn from the lower part of the bed, are recycled to the top section of the cathodic compartment by means of an external vertical duct (3).
摘要翻译：描述了用于从金属离子溶液进行金属电解提取的电池（100），其中阴极（1）由生长珠的落下床组成; 从床的下部排出的珠粒通过外部垂直管道（3）再循环到阴极室的顶部。

93. 发明授权

US6120673A Method and device for regenerating tin-plating solutions 失效
标题翻译：镀锡溶液再生方法及装置
公开(公告)号：US6120673A
公开(公告)日：2000-09-19
申请号：US74725
申请日：1998-05-07
申请人： Ulrich Reiter , Werner Harnischmacher , Klaus Fischwasser , Hans-Wilhelm Lieber , Ralph Blittersdorf , Annette Heuss
发明人： Ulrich Reiter , Werner Harnischmacher , Klaus Fischwasser , Hans-Wilhelm Lieber , Ralph Blittersdorf , Annette Heuss
IPC分类号： B01D61/44 , C02F1/461 , C02F1/469 , C23C18/16 , C25D21/22 , C25C1/14
CPC分类号： C23C18/1617 , C25D21/22 , Y10S204/13
摘要： The invention relates to a method and a device for regenerating exhausted tin-plating solutions which contain tin and copper ions, free complexing agent and complexing agent bound to the copper ions, as well as expended and unexpended reducing agent. By means of a suitable rinsing technique, the rinse water of the tin-plating process is concentrated to a 10 to 15 percent dilution of the process solution. The regenerating solution thus produced is fed to an electrolytic cell. The electrolytic cell comprises a cathode chamber, a middle chamber and an anode chamber. The cathode chamber is separated from the middle chamber by an anion-exchange membrane and the anode chamber is separated from the middle chamber by a cation-exchange membrane. The regenerating solution is initially provided in the cathode chamber. Here, the interfering copper component is cathodically deposited. After an appropriate residence time, the regenerating solution, depleted of copper, is transferred by pumping into the middle chamber where tin enrichment is effected by tin ions diffused from the anode chamber through the cation-exchange membrane. The regenerated solution is subsequently fed back into the tin-plating process.
摘要翻译：本发明涉及一种用于再生含有锡和铜离子的排出的镀锡溶液的方法和装置，与铜离子结合的游离络合剂和络合剂，以及消耗和未用的还原剂。通过合适的冲洗技术，将镀锡工艺的冲洗水浓缩至工艺溶液的10至15％稀释度。将这样制作的再生溶液送入电解槽。电解槽包括阴极室，中间室和阳极室。阴极室通过阴离子交换膜与中间室分离，阳极室通过阳离子交换膜与中间室分离。再生溶液最初设置在阴极室中。这里，干扰铜组分被阴极沉积。在适当的停留时间之后，通过泵送进入中间室来转移耗尽铜的再生溶液，其中通过阳离子交换膜从阳极室扩散的锡离子进行锡富集。再生的溶液随后被反馈到镀锡过程中。

94. 发明授权

US6110349A Method for recovering metallic tin from electroplating sludge 失效
标题翻译：从电镀污泥中回收金属锡的方法
公开(公告)号：US6110349A
公开(公告)日：2000-08-29
申请号：US170066
申请日：1998-10-13
申请人： Katsuhito Kawamura , Fuyuhiko Ishikawa , Kazumitsu Sambonchiku , Kei Yuki , Shinji Kawashima , Toshimichi Ukena
发明人： Katsuhito Kawamura , Fuyuhiko Ishikawa , Kazumitsu Sambonchiku , Kei Yuki , Shinji Kawashima , Toshimichi Ukena
IPC分类号： C25C1/14 , C25D21/18
CPC分类号： C25D21/18 , C25C1/14
摘要： Improved recovery of tin from sludge formed during a halogen-type electrolytic tinplating of steel sheet comprises leaching the sludge with water at a pH of 7 or less, separating an iron-containing sludge remaining after the leaching, alkalifying the filtrate obtained in the first separation step to deposit tin-containing sludge, separating and recovering the tin-containing sludge deposited in the first alkalifying step, redissolving the tin-containing sludge in an alkaline solution, and electrolytic reduction of the alkaline solution. High purity metallic tin is recovered from sludge, at a high yield. Other materials are also recovered for reuse from the filtrate and precipitation, which are formed during the process, without pollution of the operational environment.
摘要翻译：在钢板的卤素型电解镀锡过程中形成的污泥中锡的回收率提高包括用pH为7以下的水浸渍污泥，分离浸出后剩余的含铁污泥，碱化第一次分离中得到的滤液分离和回收沉积在第一碱化步骤中的含锡污泥，再次溶解在碱性溶液中的含锡污泥，以及碱性溶液的电解还原。高纯度金属锡以高产率从污泥中回收。还可以回收其他材料，以便在过程中形成的滤液和沉淀物再次使用，而不会污染操作环境。

95. 发明授权

US5620584A Electrochemical reduction of metal salts as a method of preparing highly dispersed metal colloids and substrate fixed metal clusters by electrochemical reduction of metal salts 失效
标题翻译：作为通过电化学还原金属盐制备高度分散的金属胶体和底物固定金属簇的方法的金属盐的电化学还原
公开(公告)号：US5620584A
公开(公告)日：1997-04-15
申请号：US401750
申请日：1995-03-09
申请人： Manfred T. Reetz , Wolfgang Helbig , Stefan A. Quaiser
发明人： Manfred T. Reetz , Wolfgang Helbig , Stefan A. Quaiser
IPC分类号： B01J13/00 , B01J23/44 , B01J23/46 , B01J35/00 , B01J37/16 , B22F9/00 , B22F9/24 , C25B1/00 , C25C5/02 , C25C1/00 , C25C1/06 , C25C1/12 , C25C1/14
CPC分类号： B01J37/16 , B01J23/44 , B01J23/462 , B01J35/0013 , C25C5/02 , Y10T428/256 , Y10T428/259 , Y10T428/2982 , Y10T428/2991
摘要： The object of the invention is a method for the electrochemical preparation of metal colloids with particle sizes of less than 30 nm, characterized in that one or more salts of one or more metals of groups Ib, IIb, III, IV, V, VI, VIIb, VIII, lanthanoides, and/or actinoides of the periodic table are cathodically reduced in the presence of a stabilizer, optionally with a supporting electrolyte being added, in organic solvents or in solvent mixtures of organic solvents and/or water within a temperature range of between -78.degree. C. and +120.degree. C. to form metal colloidal solutions or redispersible metal colloid powders, optionally in the presence of inert substrates and/or soluble metal salts of the respective metals. The invention further relates to soluble or redispersible colloids as well as application on substrates and immobilization thereof, in particular for the preparation of catalysts.
摘要翻译：本发明的目的是一种电化学制备粒径小于30nm的金属胶体的方法，其特征在于一种或多种Ib，IIb，III，IV，V，VI，在有机溶剂或有机溶剂和/或水的溶剂混合物的温度范围内，在稳定剂存在下，任选地加入支持电解质，将元素周期表的VIIb，VIII，镧系元素和/或锕系元素阴极还原在-78℃至+ 120℃之间，任选地在各自金属的惰性底物和/或可溶性金属盐的存在下形成金属胶体溶液或可再分散的金属胶体粉末。本发明还涉及可溶性或可再分散的胶体以及在底物上的应用和其固定，特别是用于制备催化剂。

96. 发明授权

US5578191A Process for extracting tin from organic solutions by electrolysis 失效
标题翻译：通过电解从有机溶液中提取锡的方法
公开(公告)号：US5578191A
公开(公告)日：1996-11-26
申请号：US508876
申请日：1995-07-28
申请人： Philippe G. Robert
发明人： Philippe G. Robert
IPC分类号： G03C5/00 , C02F1/461 , C02F1/467 , C25C1/14 , G03C5/395 , C25D5/02
CPC分类号： G03C5/3954 , C25C1/14 , C02F1/4678 , Y02P10/212
摘要： The present invention concerns a process for the electrolytic extraction of the tin found a quantity of less than 1 g/l and in a chelated form in organic solutions.The process consists of using an electrolysis unit comprising an anode compartment and cathode compartment separated by a physical barrier, introducing the organic solution into the cathode compartment and carrying out the electrolysis in galvanostatic or potentiostatic mode.This process can be applied to the recycling of photographic effluents containing tin, in particular to the processing of reversal products.
摘要翻译：本发明涉及一种电解提取锡的方法，其在有机溶液中发现少量1g / l的螯合形式。该方法包括使用包括由物理屏障隔开的阳极室和阴极室的电解单元，将有机溶液引入阴极室并以恒电流或恒电位模式进行电解。该方法可以应用于含有锡的照相流出物的再循环，特别是反转产物的加工。

97. 发明授权

US5411645A Hydrogen assisted reduced oxide soldering system 失效
标题翻译：氢辅助还原氧化物焊接系统
公开(公告)号：US5411645A
公开(公告)日：1995-05-02
申请号：US109136
申请日：1993-08-19
申请人： D. Morgan Tench
发明人： D. Morgan Tench
IPC分类号： C25C3/24 , B23K1/20 , B23K35/38 , C23C18/16 , C23G1/36 , C25C1/00 , C25C1/14 , C25C3/36 , C25D21/18 , C25F7/00
CPC分类号： B23K1/206 , B23K35/38 , C23C18/1617 , C23G1/36 , C25D21/18 , B23K2201/42
摘要： A system is provided for regenerating reducing agents used in ancillary chemical or electrochemical processes such as restoring solderability of electronic components to be soldered in a fluxless soldering process. The system includes a cathode, an anode, and an electrolyte system that is separated by a semipermeable ionic barrier into a catholyte and an anolyte. The catholyte includes the reduced member of a redox couple, which can be regenerated electrochemically. The redox couple of the electrolyte system is charged like a battery and discharged during the ancillary process. Regeneration of the reduced member of the redox couple is accomplished at the cathode, which may evolve hydrogen gas. Chemical balance is maintained by the semipermeable ionic barrier, which permits proton migration from the anolyte to the catholyte but acts as a barrier against diffusion and migration of cations from the catholyte to the anolyte. Ideally, the anodic reaction is breakdown of water to form oxygen, which is vented, and protons that migrate across the ionic barrier to the catholyte replacing protons consumed in the ancillary process. The overall reaction in a fluxless soldering system is reduction of metallic oxides to metal, electrochemical regeneration of reducing agents, release of oxygen, and evolution of hydrogen to produce a reducing atmosphere in an enclosed chamber containing the fluxless soldering system.
摘要翻译：提供了用于再生用于辅助化学或电化学过程中的还原剂的系统，例如在无焊剂焊接工艺中恢复要焊接的电子部件的可焊性。该系统包括阴极，阳极和电解质系统，其由半透性离子屏障分离成阴极电解液和阳极电解液。阴极电解质包括氧化还原对的还原成员，其可以电化学地再生。电解液系统的氧化还原电极像电池一样充电并在辅助过程中放电。在阴极处实现氧化还原对的还原成员的再生，这可能产生氢气。化学平衡通过半透性离子屏障保持，这允许质子从阳极电解液迁移到阴极电解液，但是作为阻止阳离子从阴极电解液到阳极电解液的扩散和迁移的屏障。理想地，阳极反应是水的分解以形成被排出的氧，以及迁移穿过离子屏障到阴极电解液的质子代替在辅助过程中消耗的质子。无助焊剂系统中的总体反应是将金属氧化物还原为金属，还原剂的电化学再生，氧的释放和氢的释放，以在包含无助焊剂系统的封闭室中产生还原气氛。

98. 发明授权

US5376239A Process for separating electrodeposited metal in electrolytic refining 失效
标题翻译：在电解精炼中分离电沉积金属的工艺
公开(公告)号：US5376239A
公开(公告)日：1994-12-27
申请号：US145190
申请日：1993-11-03
申请人： Hideomi Saito , Saburo Tanaka , Akiyoshi Tatsui , Akira Yoshioka
发明人： Hideomi Saito , Saburo Tanaka , Akiyoshi Tatsui , Akira Yoshioka
IPC分类号： C25C7/08 , C25C1/14 , C25C1/18 , C25C1/22
CPC分类号： C25C7/08 , Y10S266/901
摘要： A process for separating an electrodeposited metal from a cathode plate in electrolytic refining is disclosed. The cathode plate on which the metal is electrodeposited is first held. Then, heated air is blown toward the cathode plate and the electrodeposited metal thereon. As a result, the electrodeposited metal is separated from the cathode plate. An apparatus for carrying out the same process is also disclosed. The apparatus includes a separating furnace, a holding assembly, and a device for introducing heated air into the separating furnace. The holding assembly is attached to the separating furnace for holding the cathode plate in the furnace. The heated air-introducing device introduces heated air, blowing it against the cathode plate, whereby the electrodeposited metal is separated from the cathode plate.
摘要翻译：公开了一种在电解精炼中将电沉积金属与阴极板分离的方法。首先保持其上沉积有金属的阴极板。然后，将加热的空气吹向阴极板和其上的电沉积金属。结果，电沉积金属与阴极板分离。还公开了用于执行相同过程的装置。该装置包括分离炉，保持组件和用于将加热的空气引入分离炉的装置。保持组件附接到用于将阴极板保持在炉中的分离炉。加热的空气引入装置引入加热的空气，将其吹向阴极板，由此使电沉积金属与阴极板分离。

99. 发明授权

US5217585A Transition metal decontamination process 失效
标题翻译：过渡金属去除工艺
公开(公告)号：US5217585A
公开(公告)日：1993-06-08
申请号：US811474
申请日：1991-12-20
申请人： Thomas S. Snyder , William R. Gass , Gregory F. Boris , Laura J. Ayers
发明人： Thomas S. Snyder , William R. Gass , Gregory F. Boris , Laura J. Ayers
IPC分类号： G21F9/28 , C01G99/00 , C22B3/06 , C22B23/06 , C25C1/00 , C25C1/08 , C25C1/12 , C25C1/14 , C25C1/18 , C25C1/22 , G01F9/00 , G21F9/06 , G21F9/10 , G21F9/30
CPC分类号： C01G99/003 , C22B3/06 , C22B3/24 , C25C1/00 , C25C1/08 , G21F9/06 , G21F9/30 , Y02P10/234
摘要： Nickel (or other transition metal) contaminated with about 5 ppm technetium is decontaminated by dissolving the nickel and the technetium into an aqueous acid solution while introducing a graphite or activated carbon powder into the acid to immediately adsorb the dissolving technetium. The technetium-contaminated powder is separated from the aqueous acid solution and the nickel is then electrowon from the solution. The depleted acid solution is then recycled back to the dissolution step.

100. 发明授权

US4650553A Electrolytic recovery of lead from scrap 失效
标题翻译：从废料中电解回收铅
公开(公告)号：US4650553A
公开(公告)日：1987-03-17
申请号：US842578
申请日：1986-03-21
申请人： Alfred F. Felgendreger , Ashley D. Nevers , William J. Tuszynski
发明人： Alfred F. Felgendreger , Ashley D. Nevers , William J. Tuszynski
IPC分类号： C25C1/18 , H01M10/54 , C25C1/14
CPC分类号： C25C1/18 , H01M10/54 , Y02P10/212 , Y02W30/84
摘要： Lead is recovered from lead-containing scrap metal in an electrolytic process employing an aqueous solution of C.sub.1-4 alkanesulfonic acid as the electrolyte at a high concentration, scrap lead as the anode, and an electroconductive cathode, impressing an electromotive force across the solution between the electrodes to provide a specified steady-state concentration of lead salt in the electrolyte, and continuing the process to deplete the anode and collect lead at the cathode.
摘要翻译：铅是以含有高浓度的C 1-4烷基磺酸的水溶液，废铅作为阳极的电解方法从导电废金属中回收的，导电阴极在电解液之间施加电动势，电极在电解质中提供特定的稳态浓度的铅盐，并且继续消耗阳极并在阴极收集铅的过程。

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