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91. 发明授权

US3142614A Polyvalent organo-lead fungicide 失效
标题翻译：多价有机铅杀菌剂
公开(公告)号：US3142614A
公开(公告)日：1964-07-28
申请号：US12266061
申请日：1961-07-10
申请人： ETHYL CORP
发明人： LIGETT WALDO B
IPC分类号： A01N55/02 , C07F7/24
CPC分类号： A01N55/02 , C07F7/24

92. 发明授权

US3133100A Stable lead alkyl compositions and a method for preparing the same 失效
公开(公告)号：US3133100A
公开(公告)日：1964-05-12
申请号：US20093862
申请日：1962-06-08
申请人： ETHYL CORP
发明人： THOMAS WILFORD H , COOK SHIRL E
IPC分类号： C07F7/24 , C10L1/10
CPC分类号： C07F7/24 , C10L1/103

93. 发明授权

US3133095A Stable lead alkyl compositions and a method for preparing the same 失效
公开(公告)号：US3133095A
公开(公告)日：1964-05-12
申请号：US20092762
申请日：1962-06-08
申请人： ETHYL CORP
发明人： THOMAS WILFORD H , COOK SHIRL E
IPC分类号： C07F7/24 , C10L1/10
CPC分类号： C10L1/103 , C07F7/24

94. 发明授权

US3113955A Process for making tetramethyl lead 失效
公开(公告)号：US3113955A
公开(公告)日：1963-12-10
申请号：US13199361
申请日：1961-08-17
申请人： DU PONT
发明人： SANDY CHARLES A
IPC分类号： C07F7/24
CPC分类号： C07F7/24

95. 发明授权

US3085069A Process for purifying tetraethyllead compositions 失效
标题翻译：纯化四乙基铅组合物的方法
公开(公告)号：US3085069A
公开(公告)日：1963-04-09
申请号：US78489159
申请日：1959-01-05
申请人： DU PONT
发明人： MATTISON EDWIN L
IPC分类号： C07F7/24
CPC分类号： C07F7/24

96. 发明授权

US3073853A Trimethyl lead methyl sulfide 失效
标题翻译：三甲基铅甲硫醚
公开(公告)号：US3073853A
公开(公告)日：1963-01-15
申请号：US5951960
申请日：1960-09-30
申请人： CALIFORNIA RESEARCH CORP
发明人： PETER BALLINGER
IPC分类号： C07F7/24 , C10L1/30
CPC分类号： C07F7/24 , C10L1/306

97. 发明授权

US3072695A Process for making tetramethyl lead 失效
标题翻译：制造四甲基铅的方法
公开(公告)号：US3072695A
公开(公告)日：1963-01-08
申请号：US7140460
申请日：1960-11-25
申请人： DU PONT
发明人： VICTOR TULLIO
IPC分类号： C07F7/24
CPC分类号： C07F7/24

98. 发明授权

US3057897A Preparation of organolead compounds 失效
标题翻译：有机物化合物的制备
公开(公告)号：US3057897A
公开(公告)日：1962-10-09
申请号：US78486059
申请日：1959-01-05
申请人： ETHYL CORP
发明人： ROBINSON GENE C
IPC分类号： C07F3/00 , C07F3/02 , C07F3/06 , C07F5/02 , C07F5/06 , C07F7/00 , C07F7/08 , C07F7/22 , C07F7/24 , C07F9/90 , C07F9/92 , C07F17/00 , C08J9/00
CPC分类号： C08J9/0061 , C07F3/00 , C07F3/02 , C07F3/06 , C07F5/027 , C07F5/062 , C07F7/00 , C07F7/0827 , C07F7/2212 , C07F7/24 , C07F9/90 , C07F9/92 , C07F17/00 , C08J2375/04 , C08J2483/00
摘要： A polyvalent metal (which term includes arsenic, boron and silicon) is reacted with an organic ester of an inorganic acid and a bimetallic organic compound in which one metal is a Group Ia or IIa metal (Doming) and the other is a Group IIb or IIIa metal (including boron). The organic ester of an inorganic acid is of formula where either R or R1 is an organic radical (preferably alkyl and the other is hydrogen or an organic radical, a is 1 or 2 and Z is an anion, preferably sulphate, phosphate or halide. Specified polyvalent metal include beryllium, magnesium, calcium, mercury, zinc, boron, aluminium, gallium, silicon, lead, tin, arsenic and antimony. It is preferred to use these metals in a finely divided state. The bimetallic organic compound is of formula M(M1YaY1b)c where M is a Group Ia or IIa metal, M1 is a Group IIb or IIIa metal, Y is an organic radical preferably a hydrocarbon radical having up to 18 carbon atoms, Y1 is an electron donating ligand such as halogen, an organic radical (especially C1-C18 hydrocarbyl), an alcohol residue or hydrogen. a is 1 to 4 inclusive, b is 0-3 inclusive and c is the valency of M. Typical such compounds are sodium tetraethyl aluminium, sodium tetraoctyl aluminium, sodium triethylaluminium hydride, sodium diethyl aluminium dichloride; a list is given. The reaction is usually carried out at a temperature between -20 DEG C. and 200 DEG C. at a pressure not above 1000 psi. Diluents or solvents are not essential but may be used when the bimetallic organic compound is a solid. Specified solvents include hydrocarbons, ethers and amines, particularly tertiary amines. If desired, the process may be modified by using a hydride of a Group Ia or IIa metal and an olefin in the presence of a compound of a metal capable of forming a complex with said metal hydride, thus producing the bimetallic organic compound in situ.

99. 发明授权

US3045035A Process for the production of tetraethyl lead 失效
公开(公告)号：US3045035A
公开(公告)日：1962-07-17
申请号：US69020657
申请日：1957-10-15
申请人： MONTEDISON SPA
发明人： ALBERTO MALATESTA
IPC分类号： C07F7/24
CPC分类号： C07F7/24

100. 发明授权

US3038916A Thermal stabilization of alkyllead compounds 失效
标题翻译：烷基化合物的热稳定性
公开(公告)号：US3038916A
公开(公告)日：1962-06-12
申请号：US2001060
申请日：1960-04-05
申请人： ETHYL CORP
发明人： COOK SHIRL E , HYMIN SHAPIRO
IPC分类号： C07F7/24 , C10L1/10 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/20 , C10L1/22 , C10L1/26 , C10L1/30
CPC分类号： C10L1/14 , C07F7/24 , C10L1/103 , C10L1/1608 , C10L1/18 , C10L1/20 , C10L1/22 , C10L1/2641 , C10L1/306
摘要： An alkyl lead compound may be stabilized by addition thereto of (1) a plurality of different fused ring aromatic hydrocarbons in amount of from 2 to 30% by weight, said hydrocarbons having boiling points of at least 180 degrees at atmospheric pressure and containing up to 20 carbon atoms in the molecule, and (2) a saturated aliphatic monohydric alcohol containing from 1 to 6 carbon atoms in the molecule, there being present 1 to 25% of said alcohol, the total amount of alcohol plus hydrocarbon being from 3 to 45%. Hydrocarbons specified include methyl naphthalene, dimethyl naphthalene, 1,2,3,4-tetrahydronaphthalene, anthracene, ethyl naphthalene, 1,4-dihydropnaphthalene, 1,4-dihydronaphthalene and fluorene. Specification 670,526 is referred to.

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