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91. 发明授权

US4271229A Sizing composition to yield sized glass fibers with improved UV stability 失效
标题翻译：定型组合物以获得具有改进的UV稳定性的尺寸的玻璃纤维
公开(公告)号：US4271229A
公开(公告)日：1981-06-02
申请号：US72392
申请日：1979-09-04
申请人： Chester S. Temple
发明人： Chester S. Temple
IPC分类号： C03C25/26 , C03C25/32 , C08J5/08 , D06M13/513 , D06M15/564 , D06M15/643 , D04H1/58
CPC分类号： D06M15/6436 , C03C25/26 , C03C25/326 , C08J5/08 , D06M13/513 , D06M15/564 , Y10T428/2962 , Y10T428/2964 , Y10T428/31551 , Y10T428/31612 , Y10T428/31663 , Y10T442/2402 , Y10T442/259
摘要： Sizing compositions, sized glass fiber strands are used to produce reinforced polymeric materials that have improved UV stability while maintaining good physical properties. The sizing composition, sized glass fiber strands and reinforced polymeric materials having sized glass fiber strands involve the use of materials in the sizing composition, such as polyurethane polymers, ureidofunctional silanes, aminofunctional silanes, lubricants and processing aids.One particular aspect of the present invention has materials associated with the sizing composition, sized glass fiber strands and reinforced polymers such as polyamides, polyethyleneterephthlate, polybutyleneterephthlate, polystyrenics, thermosetting esters, and chemically coupled polypropylene that are thermoplastic, aliphatic, polyurethane polymer dispersions, ureidofunctional silane, gamma-aminopropyltriethoxysilane, a lubricant modified gamma-aminopropyltriethoxysilane, dibutyphthalate, polyalkylene polyol lubricant, and a polyester film former.
摘要翻译：上胶组合物尺寸的玻璃纤维股线用于生产具有改善的UV稳定性同时保持良好物理性能的增强聚合材料。具有尺寸的玻璃纤维线的施胶组合物，尺寸的玻璃纤维束和增强的聚合物材料涉及使用上浆组合物中的材料，例如聚氨酯聚合物，脲基官能硅烷，氨基官能硅烷，润滑剂和加工助剂。本发明的一个特定方面具有与上胶组合物，大小的玻璃纤维丝束和增强聚合物如聚酰胺，聚对苯二甲酸乙二酯，聚对苯二甲酸丁二酯，聚苯乙烯，热固性酯和化学偶合聚丙烯相关联的材料，它们是热塑性，脂肪族，聚氨酯聚合物分散体，脲基官能团硅烷，γ-氨丙基三乙氧基硅烷，润滑剂改性γ-氨基丙基三乙氧基硅烷，二邻苯二甲酸酯，聚亚烷基多元醇润滑剂和聚酯成膜剂。

92. 发明授权

US4221602A Size for forming glass fibers having a reduced tendency to give gumming deposits 失效
标题翻译：用于形成具有降低趋向于涂胶沉积物的玻璃纤维的尺寸
公开(公告)号：US4221602A
公开(公告)日：1980-09-09
申请号：US39472
申请日：1979-05-16
申请人： Douglas M. Walser
发明人： Douglas M. Walser
IPC分类号： C03C25/26 , C03C25/32 , C03C25/02
CPC分类号： C03C25/321 , C03C25/26 , Y10T428/2938
摘要： A method and composition are provided for producing an improved sized glass fiber strand that has a reduced tendency to form gummy deposits on fabrication machinery under high relative humidity conditions. The glass fiber strand is treated with a starch based forming size comprising about 50 to about 65 weight percent of the non-aqueous components of the composition being a starch containing cross-links that has been partially cooked along with a hydrogenated vegetable oil, or fatty triglyceride, cationic wetting agent, emulsifying agent, and water. The forming size composition can also contain a salt of a polyamino functional polyamide resin and a carboxylic acid and a wax and a coupling agent.
摘要翻译：提供了一种制备改进尺寸的玻璃纤维股线的方法和组合物，其在高相对湿度条件下在制造机械上形成粘性沉积物的倾向降低。用基于淀粉的成型尺寸处理玻璃纤维束，其中所述淀粉基成型尺寸包含约50％至约65％重量百分数的组合物的非水性组分，其是含有与氢化植物油一起部分煮熟的交联物的淀粉或脂肪甘油三酯，阳离子润湿剂，乳化剂和水。成型粒度组合物还可以含有聚氨基官能聚酰胺树脂和羧酸以及蜡和偶联剂的盐。

93. 发明授权

US4065417A Reversible shear thinning gel forming coating composition for glass fibers 失效
标题翻译：用于玻璃纤维的可逆剪切变薄凝胶形成涂料组合物
公开(公告)号：US4065417A
公开(公告)日：1977-12-27
申请号：US593601
申请日：1975-07-07
申请人： Robert Wong , Homer G. Hill
发明人： Robert Wong , Homer G. Hill
IPC分类号： C03C25/26 , C08L1/00 , C08L31/04 , C08L63/02 , C08L77/00
CPC分类号： C03C25/26
摘要： An improved method of coating fibers and particularly glass fibers with a solution of materials containing a reversible shear thinning gel producing agent which causes the coating to be transformed into a shear thinning gel under predetermined conditions. The predetermined conditions may be brought about after the coated fibers are brought together into touching engagement in a package, or may be caused to occur before the coated fibers are brought together in touching engagement in the package. The fibers can be removed from the package and still retain a coating on the fibers, since the shearing action of the fibers through the gel converts the gel to a liquid which adheres to the fibers as they are being pulled through the gel. The predetermined conditions may involve a change in temperature, or a change in concentration of solids. The change in temperature will usually be a cooling of the coating materials to a temperature below the gelation point, and the change in concentration will usually be an evaporation of solvent to form at least a skin of gel on the surface of the coating materials. The change in temperature technique can be used to increase the amount of solids that is applied to the fibers. The uncoated fibers, however, are preferably drawn through the gel to subject the reversible shear thinning gel to shear which causes the materials to flow around and adhere to the fibers, following which the coating reverts to a gel.
摘要翻译：一种用包含可逆剪切稀化凝胶产生剂的材料溶液涂覆纤维，特别是玻璃纤维的改进方法，其使得涂层在预定条件下转变成剪切稀化凝胶。在将涂覆的纤维聚集在包装中的接触接合之后，可能会导致预定条件，或者可能在涂覆的纤维在包装中接触接合在一起之前发生。纤维可以从包装中移除并且仍然保留在纤维上的涂层，因为通过凝胶的纤维的剪切作用将凝胶转化成当被拉动通过凝胶时粘附到纤维上的液体。预定条件可能涉及温度的变化或固体浓度的变化。温度的变化通常是将涂层材料冷却到低于凝胶化点的温度，并且浓度的变化通常是溶剂的蒸发，以在涂层表面上形成至少一层凝胶。温度技术的变化可用于增加施加到纤维上的固体的量。然而，未涂布的纤维优选通过凝胶拉伸以使可逆剪切稀化凝胶经受剪切，这导致材料流动并粘附到纤维上，随后涂层还原成凝胶。

94. 发明授权

US4056651A Moisture and heat resistant coating for glass fibers 失效
标题翻译：用于玻璃纤维的防潮和耐热涂层
公开(公告)号：US4056651A
公开(公告)日：1977-11-01
申请号：US706025
申请日：1976-07-16
申请人： Daniel A. Scola
发明人： Daniel A. Scola
IPC分类号： C03C25/26 , C08J5/06 , C09D179/00 , B32B17/04 , B32B17/10 , B32B27/26
CPC分类号： C08J5/06 , C03C25/26 , C08K5/0016 , C08K5/54 , C09D179/00 , Y10T428/265 , Y10T428/2933 , Y10T428/2938 , Y10T428/2962 , Y10T428/2964 , Y10T428/2969 , Y10T428/31612 , Y10T428/31623
摘要： A moisture and heat resistant finish coating for materials having a hydroxylated surface such as glass fibers embeddable in a resin matrix composite consisting essentially of approximately, by weight, 40-98 percent of a polyimide film former, 2-60 percent of a silane coupling agent and up to 30 percent of a wetting and lubricating agent.
摘要翻译：具有羟基化表面的材料的防潮和耐热表面涂层，其可嵌入树脂基质复合材料中的玻璃纤维，所述树脂基质复合物基本上由约占重量百分比的40-98％的聚酰亚胺成膜剂，2-60％的硅烷偶联剂和高达30％的润湿和润滑剂。

95. 发明授权

US4052182A Process for producing air blown glass fiber strand mat 失效
标题翻译：生产空气玻璃纤维条纹的方法
公开(公告)号：US4052182A
公开(公告)日：1977-10-04
申请号：US459135
申请日：1974-04-08
申请人： Joseph P. Stalego , William H. Rigby, Jr.
发明人： Joseph P. Stalego , William H. Rigby, Jr.
IPC分类号： C03C25/26 , D04H3/03 , C03C25/02
CPC分类号： D04H3/03 , C03C25/26
摘要： A process of making a mat of glass fibers wherein a strand of glass fibers frictionally engages the surface of a revolving cylinder from which the strand is tangentially discharged onto a moving conveyor. The strand is caused to be randomly looped upon the conveyor by alternate blasts of air which laterally impinge upon the strand to throw the strand in a looped fashion from side to side across the conveyor. More efficient and sustained operation in the processing of glass fiber mat is obtained by wetting the individual filaments of glass with a water solution comprising organosilane, nonionic lubricants, and acidic salt, which water solution eliminates wheel wrap of the glass fiber strand around the revolving cylinder without adversely affecting other desirable properties of the strand and the mat.

96. 发明授权

US3997306A Glass fiber sizing composition for the reinforcement of resin matrices and method of using same 失效
标题翻译：用于增强树脂基体的玻璃纤维施胶组合物及其使用方法
公开(公告)号：US3997306A
公开(公告)日：1976-12-14
申请号：US565986
申请日：1975-03-31
申请人： Jerry C. Hedden
发明人： Jerry C. Hedden
IPC分类号： C03C25/26 , C03C25/02
CPC分类号： C03C25/26
摘要： A glass fiber size is provided which contains a phenolic epoxy resin, the reaction product of the partial ester of a polycarboxylic acid containing one or more unesterified carboxyl groups with a compound containing more than one epoxy group, an amino silane coupling agent, a methacryloxy alkyl trialkoxy silane, and a non-ionic surface active agent. A method of sizing glass fibers and glass fibers sized with the aforementioned composition are also provided.
摘要翻译：提供玻璃纤维尺寸，其包含酚醛环氧树脂，含有一个或多个未酯化羧基的多元羧酸的部分酯与含有多于一个环氧基的化合物的反应产物，氨基硅烷偶联剂，甲基丙烯酰氧基烷基三烷氧基硅烷和非离子表面活性剂。还提供了用上述组合物调整玻璃纤维和玻璃纤维尺寸的方法。

97. 发明授权

US3933711A Forming size of aqueous polyvinylacetate 失效
标题翻译：聚乙酸乙烯酯水溶液的成型尺寸
公开(公告)号：US3933711A
公开(公告)日：1976-01-20
申请号：US491730
申请日：1974-07-23
申请人： Donald L. Motsinger , Charles E. Nalley , Joe B. Lovelace
发明人： Donald L. Motsinger , Charles E. Nalley , Joe B. Lovelace
IPC分类号： C03C25/26 , C03C25/28 , C08L31/04
CPC分类号： C08L31/04 , C03C25/26 , C03C25/28 , Y10T428/2964
摘要： A glass fiber forming size utilized to produce glass fiber strands is described in which the forming size is an aqueous mixture of polyvinyl acetate, fatty acid lubricant, methacrylato chromic chloride and gamma (ethylene diamine) propyl trimethoxy silane, the mixture being adjusted to pH between 6.1 and 6.5. The size composition is applied to glass fibers during forming. The strands produced utilizing this forming size find particular utility when formed into roving and produce a particularly effective gun roving product.
摘要翻译：描述了用于生产玻璃纤维线的玻璃纤维形成尺寸，其中成型尺寸是聚乙酸乙烯酯，脂肪酸润滑剂，甲基丙烯酰氯和丙烯三甲氧基硅烷的水性混合物，将该混合物调节至 6.1和6.5。成型时应用玻璃纤维的大小组成。使用该成形尺寸产生的股线在形成粗纱时产生特别的效用，并产生特别有效的枪粗纱产品。

98. 发明授权

US3900584A Method for analysis of treated glass fibers 失效
标题翻译：处理玻璃纤维分析方法
公开(公告)号：US3900584A
公开(公告)日：1975-08-19
申请号：US30626772
申请日：1972-11-13
申请人： OWENS CORNING FIBERGLASS CORP
发明人： ROSINSKI KLAUS D , SCHROER JOHN W
IPC分类号： C03C25/26 , G01N25/14 , G01N33/38 , C03C25/02 , G01N31/12
CPC分类号： G01N25/14 , C03C25/26 , G01N33/38
摘要： A method for determining the degree of cure of glass fibers coated with a heat-cured polymeric material wherein the coated glass fibers are contacted with water at an elevated temperature for a time sufficient to extract water-soluble carbon material from the heat-cured polymeric material, and the resulting extract is subjected to analysis to determine the carbon content of the extract. It has been found that the carbon content of the aqueous extract is inversely proportional to the degree of cure of the polymeric material.

99. 发明授权

US3666740A Method of producing high molecular polyallyl alcohol 失效
标题翻译：生产高分子量聚乙醇的方法
公开(公告)号：US3666740A
公开(公告)日：1972-05-30
申请号：US3666740D
申请日：1969-08-14
申请人： VALENTIN ALEXEEVICH KARGIN , LEV SOLOMONOVICH POLAK , VIKTOR ALEXANDROVICH KABANOV , VITALY PAVLOVICH ZUBOV , VALENTINA FEDOROVNA PANKOVA
发明人： KARGIN VALENTIN ALEXEEVICH , POLAK LEV SOLOMONOVICH , KABANOV VIKTOR ALEXANDROVICH , ZUBOV VITALY PAVLOVICH , PANKOVA VALENTINA FEDOROVNA
IPC分类号： B26D1/24 , C03C25/26 , C08F2/38 , C08F16/00 , C08J5/22 , C08F1/80 , C08F3/36
CPC分类号： C08J5/2243 , B26D1/245 , C03C25/26 , C08F16/00 , C08J2329/06
摘要： A method of producing high-molecular weight polyallyl alcohol by polymerizing allyl alcohol in the presence of an inorganic complexing agent that forms a coordination bond with the functional group of the monomer under the effect of a radical initiator. Suitable complexing agents include salts of metals of Groups I and II of the Periodic Table or acids, e.g., HCl HNO3, H2SO4, etc.
摘要翻译：在与自由基引发剂的作用下与单体的官能团形成配位键的无机络合剂的存在下，使烯丙醇聚合而制造高分子量聚烯丙醇的方法。合适的络合剂包括周期表第I和II族金属的盐或酸，例如HCl HNO 3，H 2 SO 4等。

100. 发明授权

US3617353A Soil release chemicals and method of application to glass fabric or fiber 失效
标题翻译：土壤释放化学品及其应用于玻璃纤维或纤维的方法
公开(公告)号：US3617353A
公开(公告)日：1971-11-02
申请号：US3617353D
申请日：1968-06-03
申请人： TANNER CO CHAS S
发明人： COONEY WILLIAM J
IPC分类号： C03C25/10 , C03C25/26 , C03C25/02 , B32B17/04
CPC分类号： C03C25/26 , C03C25/475 , Y10T428/2962 , Y10T428/2964 , Y10T428/31612 , Y10T428/31649 , Y10T428/31663 , Y10T442/2107 , Y10T442/2295 , Y10T442/2631 , Y10T442/2934
摘要： Soil release for application to glass fibers and fabrics which have been treated with acrylic resin, or acrylic resins, and dyes to give the fibers a base coat, which soil release comprises an aqueous emulsion of copolymers of acrylic or methacrylic acids with ester of acrylic or methacrylic acid, wherein the proportion of acid is high, ranging from about 25 to 80 percent acid, by weight, in combination with an aqueous solution of a nonyl or octyl phenol, reacted with from 9 to about 50 moles of ethylene oxide, and aqueous solution of a fatty alcohol or acid, which also has been reacted with 5 to 50 percent of ethylene oxide, the composition thus prepared being used as a finish bath treatment for glass fibers which have already been dyed or had a base color coating applied thereto, thereby to apply over the base color layer on a glass fiber or fabric a second molecular or semimolecular layer of this resinous material, which functions as a soil release and, also, by controlling the base dye system and amount of soil release obtain a fabric which is flame retardant.

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