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91. 发明授权

US07446151B2 Process for production of high-isoprene butyl rubber 有权
标题翻译：生产高异戊二烯丁基橡胶的方法
公开(公告)号：US07446151B2
公开(公告)日：2008-11-04
申请号：US11897828
申请日：2007-08-31
申请人： Rui Resendes , Gabor Kaszas , Mark J. Drewitt , Stephan Glander , Gerhard Langstein , Martin Bohnenpoll
发明人： Rui Resendes , Gabor Kaszas , Mark J. Drewitt , Stephan Glander , Gerhard Langstein , Martin Bohnenpoll
IPC分类号： C08F8/20 , C08F8/46 , C08F236/20 , C08F236/08
CPC分类号： C08F210/12 , C08F4/06 , C08F4/005 , C08F236/08 , C08F212/36 , C08F2500/17 , C08F2500/03 , C08F2500/06
摘要： The present invention relates to a continuous process for producing polymers at conversions ranging from 50% to 95% having a Mooney viscosity of at least 25 Mooney-units and a gel content of less than 15 wt. % containing repeating units derived from at least one isoolefin monomer, more than 4.1 mol % of repeating units derived from at least one multiolefin monomer and optionally further copolymerizable monomers in the presence of AlCl3 and a suitable proton source (e.g. water) or cationogen and at least one multiolefin cross-linking agent wherein the process is conducted in the absence of transition metal compounds and organic nitro compounds.
摘要翻译：本发明涉及以50至95％的转化率生产聚合物的连续方法，门尼粘度至少为25门尼单元，凝胶含量小于15wt。含有衍生自至少一种异烯烃单体的重复单元的％，大于4.1摩尔％的衍生自至少一种多烯烃单体的重复单元和任选的其它可共聚单体，在AlCl 3存在下和合适的质子源（例如水）或阳离子原子和至少一种多烯烃交联剂，其中该方法在不存在过渡金属化合物和有机硝基化合物的情况下进行。

92. 发明申请

US20080045682A1 Metal-Containing Compositions 有权
标题翻译：含金属组合物
公开(公告)号：US20080045682A1
公开(公告)日：2008-02-21
申请号：US11792738
申请日：2005-12-09
申请人： Joseph Schwab
发明人： Joseph Schwab
IPC分类号： C08F30/04
CPC分类号： C08F4/12 , C08F4/06 , C08F4/16
摘要： The present invention relates to metal-containing compositions comprising a metal-containing precursor unit (MU), a prepolymer unit (PU), and a catalyst or an initiator capable of inducing a combining reaction of ethylenically unsaturated groups of the metal-containing precursor unit and the prepolymer unit. In another embodiment, the composition comprises MU and a catalyst or initiator capable of inducing a combining reaction of the metal-containing precursor units. Both MU and PU contain additional functional groups, which may be selected to impart compatibility with each other and to produce optically clear films. The metal-containing compositions can be used to produce films or articles having a transmittance of at least 90% and index of refraction in the range of 1.4 to 1.8 in the 400-700 nm range of light and 1.4 to 2.4 in the 150-400 nm range of light.
摘要翻译：本发明涉及包含含金属的前体单元（MU），预聚物单元（PU）和催化剂或引发剂的含金属组合物，所述催化剂或引发剂能够诱导含金属前体单元的烯属不饱和基团的组合反应和预聚物单元。在另一个实施方案中，组合物包含MU和能够诱导含金属的前体单元的组合反应的催化剂或引发剂。 MU和PU都包含另外的官能团，其可以被选择以赋予彼此的相容性并产生光学透明的膜。含金属的组合物可用于生产透光率至少为90％的膜或制品，在400-700nm光线范围内的折射率为1.4至1.8，在150-400nm范围内为1.4至2.4 nm范围的光。

93. 发明申请

US20070238841A1 Polymerization processes 有权
公开(公告)号：US20070238841A1
公开(公告)日：2007-10-11
申请号：US11805063
申请日：2007-05-22
申请人： Timothy Shaffer , Scott Milner , Michael Matturro , David Chung , Michael McDonald , Robert Webb
发明人： Timothy Shaffer , Scott Milner , Michael Matturro , David Chung , Michael McDonald , Robert Webb
IPC分类号： C08F2/00
CPC分类号： C08F210/12 , C08F2/06 , C08F10/00 , C08F4/06 , C08F4/52 , C08F2/002 , C08F4/00 , C08F4/12 , C08F2/14 , C08F236/08 , C08F2500/04 , C08F2500/03
摘要： The invention provides for a process to produce polymers utilizing a hydrofluorocarbon diluent.

94. 发明授权

US07232872B2 Polymerization processes 有权
标题翻译：聚合工艺
公开(公告)号：US07232872B2
公开(公告)日：2007-06-19
申请号：US10538984
申请日：2003-12-19
申请人： Timothy Daniel Shaffer , Scott Thomas Milner , Michael Gerard Matturro , David Yen-Lung Chung , Michael Francis McDonald , Robert Norman Webb
发明人： Timothy Daniel Shaffer , Scott Thomas Milner , Michael Gerard Matturro , David Yen-Lung Chung , Michael Francis McDonald , Robert Norman Webb
IPC分类号： C08F2/14 , C08F4/20 , C08F10/10
CPC分类号： C08F210/12 , C08F2/06 , C08F10/00 , C08F4/06 , C08F4/52 , C08F2/002 , C08F4/00 , C08F4/12 , C08F2/14 , C08F236/08 , C08F2500/04 , C08F2500/03
摘要： The invention provides for a process to produce polymers utilizing a hydrofluorocarbon diluent.
摘要翻译：本发明提供了使用氢氟烃稀释剂制备聚合物的方法。

95. 发明授权

US07214750B2 Polymerization processes 有权
标题翻译：聚合工艺
公开(公告)号：US07214750B2
公开(公告)日：2007-05-08
申请号：US10539015
申请日：2003-12-19
申请人： Michael Francis McDonald , Scott Thomas Milner , Timothy Daniel Shaffer , Robert Norman Webb
发明人： Michael Francis McDonald , Scott Thomas Milner , Timothy Daniel Shaffer , Robert Norman Webb
IPC分类号： G08F2/14 , G08F10/10
CPC分类号： C08F210/12 , C08F2/06 , C08F10/00 , C08F4/06 , C08F4/52 , C08F4/12 , C08F2/14 , C08F2/002 , C08F4/00 , C08F236/08 , C08F2500/04 , C08F2500/03
摘要： The invention relates to new processes to produce polymers utilizing bayonette cooled slurry reactor systems and diluents including hydrofluorocarbons.
摘要翻译：本发明涉及使用卡口冷却的浆料反应器系统和包括氢氟烃的稀释剂来生产聚合物的新方法。

96. 发明申请

US20050288468A1 Silicon compound 有权
标题翻译：硅化合物
公开(公告)号：US20050288468A1
公开(公告)日：2005-12-29
申请号：US10523702
申请日：2003-08-07
申请人： Kohji Ohno , Yoshinobu Tsujii , Takeshi Fukuda
发明人： Kohji Ohno , Yoshinobu Tsujii , Takeshi Fukuda
IPC分类号： C07F7/21 , C08F4/06 , C08F4/42 , C08G77/04 , C08G77/28 , C08F20/06 , C07F7/04
CPC分类号： C08F4/42 , C07F7/21 , C08F4/06 , C08G77/04 , C08G77/045 , C08G77/28
摘要： A silicon compound represented by Formula (1). In Formula (1), R1 is a group independently selected respectively from the group consisting of a hydrogen atom, alkyl, substituted or non-substituted aryl and substituted or non-substituted arylalkyl, and A1 is an organic group substituted with a halogenated sulfonyl group and is preferably a group represented by Formula (2). In Formula (2), X is halogen; R2 is alkyl; a is an integer of 0 to 2; and Z1 is a single bond or alkylene having a carbon number of 1 to 10. The silicon compound provided by the present invention is a silsesquioxane derivative having an excellent living polymerizable radical polymerization initiating function. For example, it is possible to commence polymerization by allowing an acryl base monomer to coexist to form an acryl base polymer making use of one point of the structure of the silsesquioxane in the present invention as a starting point. Because a halogenated sulfonyl group has a strong electrophilicity, it is possible to synthesize various silsesquioxane derivatives by reacting the silicon compound provided by the present invention with various nucleophilic reagents, and it can actively be used as an intermediate useful for organic synthesis.
摘要翻译：由式（1）表示的硅化合物。在式（1）中，R 1是分别独立地选自氢原子，烷基，取代或未取代的芳基和取代或未取代的芳基烷基的基团，和A ^{1是被卤代磺酰基取代的有机基团，优选为式（2）表示的基团。在式（2）中，X是卤素; R 2是烷基; a为0〜2的整数; Z 1是碳数为1〜10的单键或亚烷基。本发明提供的硅化合物是具有优异的活性聚合自由基聚合引发功能的倍半硅氧烷衍生物。例如，可以通过使丙烯酰基单体共存，以本发明中的倍半硅氧烷的结构的一个点为起点，共聚形成丙烯酸基聚合物，进行聚合。由于卤代磺酰基具有很强的亲电性，所以可以通过使本发明提供的硅化合物与各种亲核试剂反应来合成各种倍半硅氧烷衍生物，并且可以有效地用作有机合成中间体。}

97. 发明授权

US06949613B2 Polymerization initiator and use 失效
标题翻译：聚合引发剂及用途
公开(公告)号：US06949613B2
公开(公告)日：2005-09-27
申请号：US10276266
申请日：2001-06-08
申请人： David Mark Haddleton
发明人： David Mark Haddleton
IPC分类号： C08F4/00 , C08F4/02 , C08F4/06 , C08F4/10 , C08F4/42 , C08F4/44 , C08F4/50 , C08F293/00
CPC分类号： C08F4/00 , C08F4/027 , C08F4/06 , C08F4/10 , C08F4/44 , C08F4/50 , C08F293/005 , C08F2438/01
摘要： The application discloses supported initiators for transition metal mediated living free radical and/or atom transfer polymerisation comprising an initiator moiety attached to a support via a selectively cleavable link, and their use to produce polymers.
摘要翻译：本申请公开了用于过渡金属介导的活性自由基和/或原子转移聚合的负载引发剂，其包含通过可选择性切割链接连接到载体上的引发剂部分及其用于产生聚合物的用途。

98. 发明授权

US06939933B2 Process for polymerizing cationically polymerizable monomers 有权
标题翻译：聚合阳离子聚合单体的方法
公开(公告)号：US06939933B2
公开(公告)日：2005-09-06
申请号：US10433444
申请日：2001-02-14
申请人： Robert N. Webb , David Y. Chung , Andrew B. Donnalley , Michael F. McDonald , Kenneth W. Powers , Ralph Howard Schatz
发明人： Robert N. Webb , David Y. Chung , Andrew B. Donnalley , Michael F. McDonald , Kenneth W. Powers , Ralph Howard Schatz
IPC分类号： C08F2/04 , C08F4/00 , C08F4/06 , C08F4/12 , C08F4/14 , C08F110/10 , C08F210/10 , C08F210/12 , C08F236/04 , C08F2/00
CPC分类号： C08F110/10 , C08F210/10 , C08F210/12 , C08F236/04 , C08F2/38 , C08F4/12 , C08F4/16 , C08F4/00 , C08F4/06 , C08F2/14 , C08F4/52 , C08F4/14 , C08F236/06
摘要： The invention relates to a new catalyst system that improves the heat transfer capability of a butyl reactor slurry process system in the production of random copolymers of one or more isoolefin monomers and one or more conjugated diene monomers in continuous slurry polymerization processes. The process is carried out in an anhydrous polymerization system containing a mixture of the monomers in a polar diluent along with a Lewis acid and a C5 or greater initiator having a tertiary halide.
摘要翻译：本发明涉及一种新的催化剂体系，其改进丁基反应器浆料工艺系统在连续淤浆聚合方法中生产一种或多种异构烯烃单体和一种或多种共轭二烯单体的无规共聚物的传热能力。该方法在含有极性稀释剂中的单体与路易斯酸和具有叔卤酸酯的C 5或更多引发剂的混合物的无水聚合体系中进行。

99. 发明申请

US20050107536A1 Polymers with new sequence distributions 有权
标题翻译：具有新序列分布的聚合物
公开(公告)号：US20050107536A1
公开(公告)日：2005-05-19
申请号：US11010092
申请日：2004-12-10
申请人： Timothy Shaffer , David Chung
发明人： Timothy Shaffer , David Chung
IPC分类号： C08F2/00 , C08F2/06 , C08F4/32 , C08F4/44 , C08F4/64 , C08F4/68 , C08F8/00 , C08F10/00 , C08F210/12
CPC分类号： C08F210/12 , C08F2/06 , C08F10/00 , C08F4/06 , C08F4/52 , C08F4/12 , C08F2/14 , C08F2/002 , C08F4/00 , C08F236/08 , C08F2500/04 , C08F2500/03
摘要： The invention relates to new polymerization processes including diluents including hydrofluorocarbons and their use to produce novel polymers with new sequence distributions. In particular, the invention relates to copolymers of an isoolefin, preferably isobutylene, and a multiolefin, preferably a conjugated diene, more preferably isoprene, with new sequence distributions.
摘要翻译：本发明涉及新的聚合方法，包括包括氢氟烃在内的稀释剂，以及它们用于产生具有新的序列分布的新型聚合物的用途。特别地，本发明涉及异构烯烃，优选异丁烯和多烯烃，优选共轭二烯，更优选异戊二烯与新的序列分布的共聚物。

100. 发明申请

US20040059076A1 Process for polymerizing cationically polymerizable monomers 失效
标题翻译：聚合阳离子聚合单体的方法
公开(公告)号：US20040059076A1
公开(公告)日：2004-03-25
申请号：US10627005
申请日：2003-07-25
发明人： Robert Norman Webb , Michael Francis McDonald , David Yen-Lung Chung , Yuan-Ju Chen , Richard Dwight Hembree , John Patrick Soisson
IPC分类号： C08F002/14
CPC分类号： C08F236/04 , C08F4/005 , C08F4/14 , C08F4/16 , C08F4/54 , C08F110/10 , C08F210/10 , C08F210/12 , C08F4/00 , C08F4/12 , C08F4/06 , C08F2/14 , C08F2/38 , C08F4/52 , C08F212/06 , C08F236/06 , C08F236/08
摘要： The invention relates to a new catalyst system that improves the heat transfer capability of a butyl reactor slurry process system in the production of isobutylene-based polymers in continuous slurry polymerization processes. The process is carried out in an anhydrous polymerization system containing a mixture of the monomers in a polar diluent along with a Lewis acid and a C5 or greater initiator having a tertiary halide.
摘要翻译：本发明涉及一种新的催化剂体系，其改进丁基反应器浆料工艺系统在连续淤浆聚合方法中制备异丁烯基聚合物时的传热能力。该方法在包含极性稀释剂中的单体与路易斯酸和具有叔卤化物的C5或更多的引发剂的混合物的无水聚合体系中进行。

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