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91. 发明授权

US4612388A Process for producing N-acylphenylalanines 失效
标题翻译： N-酰基苯丙氨酸的制备方法
公开(公告)号：US4612388A
公开(公告)日：1986-09-16
申请号：US719300
申请日：1985-04-03
申请人： Ryuichi Mita , Toshio Katoh , Chojiro Higuchi , Akihiro Yamaguchi
发明人： Ryuichi Mita , Toshio Katoh , Chojiro Higuchi , Akihiro Yamaguchi
IPC分类号： C07C231/10 , C07C67/00 , C07C231/00 , C07C231/12 , C07C233/46 , C07C233/47 , C07C233/82 , C07C233/83 , C07C99/06
CPC分类号： C07C233/46
摘要： Disclosed herein is a process for producing an N-acyl-substituted or unsubstituted phenylalanine comprising hydrolyzing a 2-substituted-4-substituted or unsubstituted benzylidene-5-oxazolone with alkali, adjusting pH of the reaction solution containing its hydrolysis product with acid at 5-9 and reducing the resultant reaction solution catalytically in the presence of a palladium or platinum reducing catalyst.In accordance with the process of the present invention, time duration required for effecting the reduction can be shortened markedly in comparison with the reduction in an aqueous strong alkaline solution. Moreover, the catalyst recovered after completion of the reduction can be used repeatedly without any additional treatment and without any observed lowering in its activity. Accordingly, the reduction using the recovered catalyst may proceed in practically the same time as in the case of using a fresh catalyst.In the process of the present invention, the reduction is carried out continuously without isolating the alkaline hydrolysis product, i.e., a substituted or unsubstituted N-acylaminocinnamic acid from the reaction mixture, so that the process is featured advantageously by simplified process and improved overall yield.
摘要翻译：本文公开了N-酰基取代或未取代的苯丙氨酸的制备方法，其包括用碱水解2-取代-4-取代或未取代的亚苄基-5-恶唑酮，调节含有其水解产物的反应溶液的pH为5 -9并在钯或铂还原催化剂的存在下催化还原所得的反应溶液。根据本发明的方法，与强碱性水溶液的降低相比，可以显着缩短实现还原所需的时间。此外，还原后还原反应的催化剂可以重复使用，无需任何额外的处理，并且没有观察到其活性降低。因此，使用回收的催化剂的还原可以与使用新鲜催化剂的情况几乎相同的时间进行。在本发明的方法中，还原是从反应混合物中分离碱性水解产物，即取代或未取代的N-酰氨基肉桂酸，连续进行，使得该方法有利地通过简化的方法和改进的总产率。

92. 发明授权

US4275240A Process for the preparation of 2,2'-bisphenol sulfoxides 失效
标题翻译：制备2,2'-双酚亚砜的方法
公开(公告)号：US4275240A
公开(公告)日：1981-06-23
申请号：US126980
申请日：1980-03-03
申请人： Akihiro Yamaguchi , Keizaburo Yamaguchi , Hisamichi Murakami , Tadashi Kobayashi
发明人： Akihiro Yamaguchi , Keizaburo Yamaguchi , Hisamichi Murakami , Tadashi Kobayashi
IPC分类号： C07C317/00
CPC分类号： C07C317/00
摘要： 2,2'-Bisphenol sulfoxides are prepared by oxidizing 2,2'-bisphenol sulfides with hydrogen peroxide in the presence of such an organic solvent as not to form any organic peracids under reaction conditions.
摘要翻译： 2,2'-双酚亚砜通过在这种有机溶剂的存在下用过氧化氢氧化2,2'-双酚硫化物制备，在反应条件下不形成任何有机过酸。

93. 发明授权

US4248804A Process for the preparation of 2,2'-bis[4-(1,1,3,3-tetramethylbutyl)phenol]sulfide 失效
标题翻译：制备2,2'-双[4-（1,1,3,3-四甲基丁基）苯酚]硫化物的方法
公开(公告)号：US4248804A
公开(公告)日：1981-02-03
申请号：US70614
申请日：1979-08-29
申请人： Akihiro Yamaguchi , Tadashi Kobayashi , Keisaburo Yamaguchi , Hisamichi Murakami
发明人： Akihiro Yamaguchi , Tadashi Kobayashi , Keisaburo Yamaguchi , Hisamichi Murakami
IPC分类号： C07C319/14 , C07C321/30 , C07C149/36
CPC分类号： C07C323/00
摘要： 2,2'-bis[4-(1,1,3,3-tetramethylbutyl)phenol]sulfide is prepared by suspending 4-(1,1,3,3-tetramethylbutyl)phenol in an organic solvent, reacting it with sulfur dichloride or sulfur monochloride at a temperature of from -10.degree. to 40.degree. C., and isolating the precipitate so formed.
摘要翻译：通过将4-（1,1,3,3-四甲基丁基）苯酚在有机溶剂中悬浮，使其与硫反应制备2,2'-双[4-（1,1,3,3-四甲基丁基）苯酚]硫醚二氯化物或一氯化硫，在-10℃至40℃的温度下，分离形成的沉淀物。

94. 发明授权

US4192677A 1,3,4-Oxadiazole derivatives and use thereof 失效
标题翻译： 1,3,4-恶二唑衍生物及其用途
公开(公告)号：US4192677A
公开(公告)日：1980-03-11
申请号：US958190
申请日：1978-11-06
申请人： Mitsuo Okazaki , Akihiro Yamaguchi , Masaomi Sasaki
发明人： Mitsuo Okazaki , Akihiro Yamaguchi , Masaomi Sasaki
IPC分类号： G03G5/06
CPC分类号： G03G5/0661
摘要： 1,3,4-oxadiazole derivative expressed by the general formula ##STR1## wherein R represents alkyl having 1-4 carbon atoms, dialkylamino having 1-4 carbon atoms, diarylamino, phenyl, styryl, halogenophenyl, nitrophenyl, alkylphenyl having 1-4 carbon atoms, alkoxyphenyl having 1-4 carbon atoms, cyanophenyl, carboxylic ester substituted phenyl, dialkylaminophenyl having 1-4 carbon atoms, naphthyl, anthryl, or heterocyclic radical, is a photoconductive substance with high sensitivity and is a compound useful as a constituent of electrophotographic plate.
摘要翻译：其中R代表具有1-4个碳原子的烷基，具有1-4个碳原子的二烷基氨基，二芳基氨基，苯基，苯乙烯基，卤代苯基，硝基苯基，具有1-4个碳原子的烷基苯基的1,3,4-恶二唑衍生物碳原子，具有1-4个碳原子的烷氧基苯基，氰基苯基，羧酸酯取代的苯基，具有1-4个碳原子的二烷基氨基苯基，萘基，蒽基或杂环基，是具有高灵敏度的光电导物质，并且是用作电子照相平板。

95. 发明授权

US4157913A Derivatives of 1,3,4-oxadiazole and electrophotographic elements containing same 失效
标题翻译： 1,3,4-恶二唑的衍生物和含有它们的电子照相元件
公开(公告)号：US4157913A
公开(公告)日：1979-06-12
申请号：US863130
申请日：1977-12-22
申请人： Mitsuo Okazaki , Akihiro Yamaguchi , Masaomi Sasaki
发明人： Mitsuo Okazaki , Akihiro Yamaguchi , Masaomi Sasaki
IPC分类号： C07D271/10 , C07D455/04 , C07F17/02 , G03G5/06 , C07D413/14 , G03G5/04
CPC分类号： C07D271/10 , C07D455/04 , C07F17/02 , G03G5/0674
摘要： 1,3,4-OXADIAZOLE DERIVATIVES EXPRESSED BY THE GENERAL FORMULA ##STR1## , wherein R represents cyanophenyl, nitrophenyl, dialkylaminophenyl (wherein alkyl has 1-4 carbon atoms), julolidyl, N-alkylcarbazolyl (wherein alkyl has 1-4 carbon atoms) or ferrocenyl radical, are photoconductive substances possessing high sensitivity and are compounds useful as a constituent of electrophotographic plates.
摘要翻译：其中R代表氰基苯基，硝基苯基，二烷基氨基苯基（其中烷基具有1-4个碳原子），高碘基，N-烷基咔唑基（其中烷基具有1-4个碳原子））或二茂铁基是具有高灵敏度的光电导物质，并且是可用作电子照相平板的组成的化合物。

96. 发明授权

US08714136B2 Direct fuel-injection engine 失效
标题翻译：直接燃油喷射发动机
公开(公告)号：US08714136B2
公开(公告)日：2014-05-06
申请号：US12745814
申请日：2008-12-12
申请人： Kenichiro Ikeya , Nobuhiko Sasaki , Hiroshi Sono , Yukihisa Yamaya , Akihiro Yamaguchi , Yoshimasa Kaneko , Goichi Katayama , Yutaka Tajima
发明人： Kenichiro Ikeya , Nobuhiko Sasaki , Hiroshi Sono , Yukihisa Yamaya , Akihiro Yamaguchi , Yoshimasa Kaneko , Goichi Katayama , Yutaka Tajima
IPC分类号： F02B3/00
CPC分类号： F02B23/0669 , F02B3/06 , F02B23/0621 , F02B23/0651 , F02B23/0657 , F02B23/0696 , F02B2275/14 , Y02T10/123 , Y02T10/125
摘要： In a direct fuel-injection engine equipped with a pentroof-shaped piston, cross-sectional shapes containing a piston central axis (Lp) of a cavity recessed in a central part of the piston having a top face with the height varying in the circumferential direction are set so as to be basically identical at each position in the circumferential direction (see broken line). Since the sizes of the cross-sectional shapes of the cavity thereby become different in a region further on the piston central axis (Lp) side than intersection points (e1, d1) in the vicinity of a fuel injection point (Oinj), in order to compensate for this, by correcting in a cross section that is away from the piston pin direction the cross-sectional shape of the broken line into the cross-sectional shape of a solid line so that it enlarges, the size of the cross-sectional shape at each position of the circumferential direction of the cavity is thereby made more uniform, thus making the conditions in which fuel and air are mixed uniform and improving the engine output and reducing harmful exhaust materials.
摘要翻译：在配备有五角柱形活塞的直接燃料喷射发动机中，包含在活塞的中心部分凹陷的空腔的活塞中心轴线（Lp）的横截面形状具有顶面，其高度在圆周方向上变化被设定为在圆周方向上的每个位置基本相同（参见虚线）。由于空腔的横截面形状的大小因此在活塞中心轴线（Lp）侧的区域比在燃料喷射点（Oinj）附近的交点（e1，d1）变得不同，按顺序为了补偿这一点，通过将离开活塞销方向的横截面中的虚线的横截面形状校正为实线的横截面形状，使其扩大，横截面的尺寸因此，空腔的圆周方向的每个位置的形状更均匀，从而使得燃料和空气混合的条件均匀，并且改善发动机输出并减少有害排气材料。

97. 发明申请

US20050151732A1 Method for drawing object having rough model and detailed model 有权
标题翻译：具有粗糙模型和详细模型的绘制对象的方法
公开(公告)号：US20050151732A1
公开(公告)日：2005-07-14
申请号：US11011158
申请日：2004-12-15
申请人： Akihiro Yamaguchi , Akihiko Yoshida
发明人： Akihiro Yamaguchi , Akihiko Yoshida
IPC分类号： A63F13/00 , G06T15/00 , G06T15/40
CPC分类号： G06T15/10 , G06T2210/36
摘要： Detailed model data having numerous polygons and rough model data having fewer polygons are prepared for one object. A rectangular parallelepiped including the entire object is defined as a bounding box. A virtual three-dimensional space is perspective-transformed to divide an image-drawing field, which is an image drawing range, into a far image-drawing field and a near image-drawing field according to a distance from a viewpoint of virtual camera. When at least a part of the bounding box is included in the far image-drawing field, polygons of rough model data included in the far image-drawing field are drawn in a frame buffer. When at least a part of the bounding box is included in the near image-drawing field, polygons of detailed model data included in the near image-drawing field are drawn in a frame buffer.
摘要翻译：为一个对象准备具有多个多边形的详细模型数据和具有较少多边形的粗略模型数据。包括整个对象的长方体被定义为边界框。透视变换虚拟三维空间，根据与虚拟摄像机的视点的距离，将作为图像绘制范围的图像绘制区域划分为远的图像绘制场和近图像绘制场。当边界框的至少一部分被包括在远图像绘制区域中时，包括在远图像绘制区域中的粗略模型数据的多边形被绘制在帧缓冲器中。当边界框的至少一部分被包括在近图像绘制区域中时，包括在近图像绘制区域中的详细模型数据的多边形被绘制在帧缓冲器中。

98. 发明授权

US6010386A Method for removing black film from skirt of CRT front panel 失效
标题翻译：从CRT前面板裙部去除黑色薄膜的方法
公开(公告)号：US6010386A
公开(公告)日：2000-01-04
申请号：US203316
申请日：1998-12-01
申请人： Masahisa Okamoto , Akihiro Yamaguchi
发明人： Masahisa Okamoto , Akihiro Yamaguchi
IPC分类号： H01J9/227 , H01J9/38 , H01J9/00
CPC分类号： H01J9/2278 , H01J9/38 , H01J2209/017
摘要： A method for manufacturing a cathode ray tube includes the steps of applying a black substance to the inner surface of a glass panel, immersing the skirt inner wall and the sealing surface of the glass panel in a glass dissolving liquid for etching, and removing the black substance adhered to the skirt inner wall and the sealing surface by a removing means while spraying a cleaning liquid on the inner surface of the glass panel, thereby forming the desired black matrix film on the front inner wall of the glass panel. Therefore, the excess black substance coating film adhered to the skirt inner wall and the sealing surface of the skirt portion of the glass panel can be removed effectively, and the occurrence of minute flaws that adversely affect the production and life of the cathode ray tube is prevented.
摘要翻译：阴极射线管的制造方法包括以下步骤：将黑色物质施加到玻璃面板的内表面，将玻璃面板的裙部内壁和密封面浸渍在用于蚀刻的玻璃溶解液中，除去黑色物质在玻璃面板的内表面上喷洒清洗液体时，通过除去装置粘附在裙部内壁和密封面上，从而在玻璃面板的前内壁上形成所需的黑色矩阵膜。因此，可以有效地除去附着在玻璃面板的裙部内壁和裙部的密封面上的过量的黑色物质涂膜，并且对阴极射线管的生产和使用寿命产生不利影响的微小缺陷的发生是防止了

99. 发明授权

US5710334A Aromatic dinitro and diamino intermediates 失效
标题翻译：芳香二硝基和二氨基中间体
公开(公告)号：US5710334A
公开(公告)日：1998-01-20
申请号：US453073
申请日：1995-05-26
申请人： Yuko Ishihara , Mitsunori Matsuo , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Yuko Ishihara , Mitsunori Matsuo , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： C07C201/12 , C07C205/45 , C07C221/00 , C07C225/22 , C08G73/10 , C08G73/12 , C08J5/18 , C08L79/08 , C07C217/84 , C07C217/90
CPC分类号： C08G73/10 , C08G73/1007 , C08G73/1014 , C08G73/1017 , C08G73/1067 , Y10T428/31504 , Y10T428/31721
摘要： This invention relates to a novel thermoplastic and amorphous polyimide which is readily soluble in organic solvent, a novel aromatic diamino compound used for the polyimide, a preparation process thereof, a polyimide-based resin composition comprising the thermoplastic polyimide and a fibrous reinforcement, a process for preparing the resin composition, an injection molded article of the resin composition, a polyimide-based composite obtained by molding the above soluble and thermoplastic polyimide in combination with a fibrous reinforcement, and a fibrous reinforcement having a surface modified with the above polyimide. The polyimide comprise a requisite structural unit having one or more recurring structural units of the formula: ##STR1## wherein m and n are individually an integer of 0 or 1, and R is ##STR2## The polyimide of the invention is essentially amorphous, excellent in melt flow stability in the decreased temperature as compared with conventionally known polyimide and has greatly improved processability. The polyimide of the invention obtained by using a novel aromatic diamino compound as a monomer can control various properties such as melt flow ability and solubility in solvents by side chains and not by principal chain of polyimide. Thus, excellent melt flow property and solubility in solvents can be obtained while maintaining high heat resistance and adhesive property which are derived from benzophenone structure of the diamino compound of the the invention.
摘要翻译：本发明涉及易溶于有机溶剂的新型热塑性和无定形聚酰亚胺，用于聚酰亚胺的新型芳族二氨基化合物及其制备方法，包含热塑性聚酰亚胺和纤维增强剂的聚酰亚胺基树脂组合物，用于制备树脂组合物的树脂组合物的注塑制品，通过将上述可溶性和热塑性聚酰亚胺与纤维增强剂组合成型而获得的聚酰亚胺类复合材料和具有用上述聚酰亚胺改性的表面的纤维增强剂。聚酰亚胺包含必需的结构单元，其具有一个或多个下式的重复结构单元：其中m和n分别为0或1的整数，且R为“无定形”，优异的与传统已知的聚酰亚胺相比在降低的温度下的熔体流动稳定性，并且具有极大的改进的加工性能。通过使用新颖的芳族二氨基化合物作为单体获得的本发明的聚酰亚胺可以通过侧链而不是聚酰亚胺的主链来控制各种性能如熔体流动性和在溶剂中的溶解度。因此，在保持由本发明的二氨基化合物的二苯甲酮结构得到的高耐热性和粘合性的同时，可以获得优异的熔体流动性和溶剂中的溶解性。

100. 发明授权

US5708128A Linear polyamic acid, linear polyimide and thermoset polyimide 失效
标题翻译：线性聚酰胺酸，线性聚酰亚胺和热固性聚酰亚胺
公开(公告)号：US5708128A
公开(公告)日：1998-01-13
申请号：US668836
申请日：1996-06-24
申请人： Hideaki Oikawa , Shoji Tamai , Masahiro Ohta , Akihiro Yamaguchi
发明人： Hideaki Oikawa , Shoji Tamai , Masahiro Ohta , Akihiro Yamaguchi
IPC分类号： C08G73/10 , C08G69/26
CPC分类号： C08G73/101 , C08G73/1071 , Y10T428/31504
摘要： Novel thermoset polyimide and composite materials comprising the thermoset polyimides and a fibrous reinforcement are prepared according to this invention. The thermoset polyimides are obtained by heat-treating a linear polyamic acid or a linear polyimide prepared by using 4,4'-bis(3-aminophenoxy)biphenyl and pyromellitic dianhydride as essential monomers or by adding 4,4'-diaminodiphenyl ether or 3,3',4,4'-biphenyltetracarboxylic dianhydride to the essential monomers and by end-capping the molecular chain end with an aromatic dicarboxylic anhydride having a carbon-carbon triple bond. The thermoset polyimides have essential excellent properties of thermoplastic polyimide and additionally has enhanced heat resistance and improved mechanical properties. The thermoset polyimide can be used to provide various kinds of composite materials for aircraft matrices, electric and electronic appliances and others.
摘要翻译：根据本发明制备了新型热固性聚酰亚胺和包含热固性聚酰亚胺和纤维增强材料的复合材料。热固性聚酰亚胺通过热处理线性聚酰胺酸或通过使用4,4'-双（3-氨基苯氧基）联苯和均苯四酸二酐作为必需单体制备的线性聚酰亚胺或通过加入4,4'-二氨基二苯醚或3 ，3'，4,4'-联苯四羧酸二酐加入到基本单体中，并通过用具有碳 - 碳三键的芳族二羧酸酐封端分子链末端。热固性聚酰亚胺具有热塑性聚酰亚胺的基本优异性能，并且还具有增强的耐热性和改善的机械性能。热固性聚酰亚胺可用于为飞机基体，电气和电子设备等提供各种复合材料。

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