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1. 发明申请

US20090234140A1 METHOD FOR SEPARATING OF OPTICALLY PURE THIOPHENE COMPOUNDS USING SIMULATED MOVING BED CHROMATOGRAPHY 有权
标题翻译：使用模拟移动色谱仪分离光学纯净化合物的方法
公开(公告)号：US20090234140A1
公开(公告)日：2009-09-17
申请号：US11721366
申请日：2004-12-20
申请人： Jae Suk Koh , Chun Young Kim , Byoung In Lee , Sang Soo Lee , Seong Jun Lee , Jong Ho Lim , Seon Yeong Jeon , Jun Bae Hong
发明人： Jae Suk Koh , Chun Young Kim , Byoung In Lee , Sang Soo Lee , Seong Jun Lee , Jong Ho Lim , Seon Yeong Jeon , Jun Bae Hong
IPC分类号： C07D495/04
CPC分类号： C07D495/04 , C07B57/00
摘要： Disclosed herein is a method of producing an optically active thiophene-based compound using a simulated moving bed adsorption separation process, and more specifically, a method of continuously separating a racemic thiophene-based compound into its optically active thiophene-based compounds having high purity, through optical resolution using the simulated moving bed process. According to the method of the current invention, a racemic mixture of a thiophene-based compound can be continuously separated into its optically active thiophene-based compounds having high purity, which is an intermediate of optically active dorzolamide acting as a topical therapeutic agent for glaucoma, using a simulated moving bed adsorption separation technique, thereby increasing industrial usability.
摘要翻译：本文公开了使用模拟移动床吸附分离方法制造光学活性噻吩类化合物的方法，更具体地说，是将外消旋噻吩类化合物连续分离成其高纯度的光学活性噻吩类化合物的方法，通过使用模拟移动床过程的光学分辨率。根据本发明的方法，可以将噻吩类化合物的外消旋混合物连续分离成其高纯度的光学活性噻吩类化合物，其是用作青光眼的局部治疗剂的光学活性多吡咯酰胺的中间体，使用模拟移动床吸附分离技术，从而提高工业可用性。

2. 发明授权

US07767832B2 Method for separating of optically pure thiophene compounds using simulated moving bed chromatography 有权
标题翻译：使用模拟移动床层析分离光学纯噻吩化合物的方法
公开(公告)号：US07767832B2
公开(公告)日：2010-08-03
申请号：US11721366
申请日：2004-12-20
申请人： Jae Suk Koh , Chun Young Kim , Byoung In Lee , Sang Soo Lee , Seong Jun Lee , Jong Ho Lim , Seon Yeong Jeon , Jun Bae Hong
发明人： Jae Suk Koh , Chun Young Kim , Byoung In Lee , Sang Soo Lee , Seong Jun Lee , Jong Ho Lim , Seon Yeong Jeon , Jun Bae Hong
IPC分类号： C07D495/06
CPC分类号： C07D495/04 , C07B57/00
摘要： Disclosed herein is a method of producing an optically active thiophene-based compound using a simulated moving bed adsorption separation process, and more specifically, a method of continuously separating a racemic thiophene-based compound into its optically active thiophene-based compounds having high purity, through optical resolution using the simulated moving bed process. According to the method of the current invention, a racemic mixture of a thiophene-based compound can be continuously separated into its optically active thiophene-based compounds having high purity, which is an intermediate of optically active dorzolamide acting as a topical therapeutic agent for glaucoma, using a simulated moving bed adsorption separation technique, thereby increasing industrial usability.
摘要翻译：本文公开了使用模拟移动床吸附分离方法制造光学活性噻吩类化合物的方法，更具体地说，是将外消旋噻吩类化合物连续分离成其高纯度的光学活性噻吩类化合物的方法，通过使用模拟移动床过程的光学分辨率。根据本发明的方法，可以将噻吩类化合物的外消旋混合物连续分离成其高纯度的光学活性噻吩类化合物，其是用作青光眼的局部治疗剂的光学活性多吡咯酰胺的中间体，使用模拟移动床吸附分离技术，从而提高工业可用性。

3. 发明授权

US09376354B2 Displacement desorption process for light olefin separation 有权
标题翻译：轻烯烃分离的位移解吸过程
公开(公告)号：US09376354B2
公开(公告)日：2016-06-28
申请号：US13819007
申请日：2011-08-26
申请人： Jong Nam Kim , Jong Ho Park , Hee Tae Beum , Seong Jun Lee , Jang Jae Lee , Dong Wook Kim , Chang Hyun Ko , Sang Sup Han , Soon Haeng Cho
发明人： Jong Nam Kim , Jong Ho Park , Hee Tae Beum , Seong Jun Lee , Jang Jae Lee , Dong Wook Kim , Chang Hyun Ko , Sang Sup Han , Soon Haeng Cho
IPC分类号： B01D53/04 , C07C7/04 , C07C7/13 , C07C7/00
CPC分类号： C07C7/005 , B01D53/04 , B01D2253/108 , B01D2256/24 , B01D2257/7022 , B01D2259/40086 , B01D2259/404 , C07C7/04 , C07C7/13 , Y02P30/464 , C07C11/02 , C07C11/04 , C07C11/06
摘要： A process and apparatus for separating an olefin from mixed gases containing light olefins is provided. The process includes adsorbing the olefin of an olefin-containing mixed gas in an adsorption column packed with an adsorbent selectively adsorbing the olefin; discharging gases other than the olefin through the outlet of the adsorption column; desorbing the adsorbed olefin by displacement using a desorbent, and separating the olefin from the desorbent, thereby producing a high-purity olefin. The apparatus includes adsorption columns packed with an adsorbent selectively adsorbing an olefin, and at least two distillation columns for separating an olefin/desorbent mixture and an olefin poor stream/desorbent into their components. If the olefin concentration of the off-gas from an olefin rinse step is higher than that of a raw material gas, recovering the olefin from the off-gas is carried out before or after the adsorption step.
摘要翻译：提供了一种用于从含有轻质烯烃的混合气体中分离烯烃的方法和装置。该方法包括在填充有选择性吸附烯烃的吸附剂的吸附塔中吸附含烯烃混合气体的烯烃; 通过吸附塔的出口排出除烯烃以外的气体; 使用解吸剂通过置换解吸吸附的烯烃，并从解吸剂中分离烯烃，从而产生高纯度烯烃。该装置包括填充有选择性吸附烯烃的吸附剂的吸附塔和用于将烯烃/脱附剂混合物和烯烃不良物流/解吸剂分离成其组分的至少两个蒸馏塔。如果来自烯烃漂洗步骤的废气的烯烃浓度高于原料气体的烯烃浓度，则在吸附步骤之前或之后进行从废气中回收烯烃。

4. 发明授权

US08367885B2 Method of preparing multicomponent bismuth molybdate catalysts with controlling pH and a method of preparing 1,3-butadiene using thereof 失效
标题翻译：制备控制pH的多组分钼酸铋催化剂的方法和使用其制备1,3-丁二烯的方法
公开(公告)号：US08367885B2
公开(公告)日：2013-02-05
申请号：US12451437
申请日：2008-05-08
申请人： Young Min Chung , Seong Jun Lee , Tae Jin Kim , Seung Hoon Oh , Yong Seung Kim , In Kyu Song , Hee Soo Kim , Ji Chul Jung , Ho Won Lee
发明人： Young Min Chung , Seong Jun Lee , Tae Jin Kim , Seung Hoon Oh , Yong Seung Kim , In Kyu Song , Hee Soo Kim , Ji Chul Jung , Ho Won Lee
IPC分类号： C07C5/48
CPC分类号： H04N21/4126 , B01J23/002 , B01J23/31 , B01J23/8876 , B01J37/031 , B01J2523/00 , C07C5/48 , C07C2523/18 , C07C2523/28 , C07C2523/745 , C07C2523/755 , C07C2523/883 , H04N21/4334 , H04N21/43615 , H04N21/43637 , H04N21/440263 , H04N21/64322 , C07C11/167 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/847
摘要： This invention relates to a method of preparing a multicomponent bismuth molybdate catalyst by changing the pH of a coprecipitation solution upon coprecipitation and a method of preparing 1,3-butadiene using the catalyst. The multicomponent bismuth molybdate catalyst, coprecipitated using a solution having an adjusted pH, the preparation method thereof, and the method of preparing 1,3-butadiene through oxidative dehydrogenation using a C4 mixture including n-butene and n-butane as a reactant are provided. The C4 raffinate, containing many impurities, is directly used as a reactant without an additional process for separating n-butane or extracting n-butene, thus obtaining 1,3-butadiene at high yield. The activity of the multicomponent bismuth molybdate catalyst can be simply increased through precise pH adjustment upon coprecipitation, which is not disclosed in the conventional techniques. This method can be applied to the increase in the activity of multicomponent bismuth molybdate catalysts reported in the art.
摘要翻译：本发明涉及通过在共沉淀时改变共沉淀溶液的pH值和使用该催化剂制备1,3-丁二烯的方法制备多组分钼酸铋催化剂的方法。提供了使用调节pH的溶液共沉淀的多组分钼酸铋催化剂及其制备方法以及使用包含正丁烯和正丁烷作为反应物的C4混合物通过氧化脱氢制备1,3-丁二烯的方法。含有许多杂质的C4萃余液直接用作反应物，而不需要另外的分离正丁烷或提取正丁烯的方法，从而以高产率获得1,3-丁二烯。多组分钼酸铋催化剂的活性可以通过共沉淀下的精确pH调节简单地增加，这在传统技术中没有公开。该方法可以应用于本领域中报道的多组分钼酸铋催化剂的活性的提高。

5. 发明申请

US20100137664A1 PROCESS FOR 1,3-BUTADIENE SEPARATION FROM A CRUDE C4 STREAM WITH ACETYLENE CONVERTER 有权
标题翻译：用乙炔转化器从C4原料中分离1,3-丁二烯的方法
公开(公告)号：US20100137664A1
公开(公告)日：2010-06-03
申请号：US12452715
申请日：2008-07-18
申请人： Hee Du Lee , Kyung Jong Oh , Min Su Ko , Min Gyoo Park , Seong Jun Lee , Yoon Jae Yim , Seung Hoon Oh , Tae Jin Kim , Yong Seung Kim , Deuk Soo Park , Hong Chan Kim
发明人： Hee Du Lee , Kyung Jong Oh , Min Su Ko , Min Gyoo Park , Seong Jun Lee , Yoon Jae Yim , Seung Hoon Oh , Tae Jin Kim , Yong Seung Kim , Deuk Soo Park , Hong Chan Kim
IPC分类号： C07C2/38 , B01J10/00
CPC分类号： C10G67/04 , C07C7/08 , C07C11/107 , C10G21/00 , C10G21/28 , C10G45/32 , C10G2300/44 , C10G2400/20 , C07C11/167
摘要： Disclosed is a method of recovering 1,3-butadiene from a C4 stream containing butane, isobutane, 2-butene, 1-butene, isobutene, butadiene and acetylene. The process of recovering highly pure 1,3-butadiene includes acetylene conversion for selectively converting acetylene through liquid-phase hydrogenation, so that the acetylene content is decreased to 70 wt ppm or less, and 1,3-butadiene extraction using an extractive distillation column, a pre-separator, a solvent stripping column, a solvent recovery column, and a purification column. Through the acetylene conversion, the concentration of vinylacetylene is decreased to 70 wt ppm or less, after which 1,3-butadiene is recovered using only one extractive distillation column, thereby considerably decreasing the degree of utility and the loss of streams in the course of extraction. The number of units necessary for the process is decreased, thus remarkably reducing the time during which impurities can accumulate in a processing unit.
摘要翻译：公开了从含有丁烷，异丁烷，2-丁烯，1-丁烯，异丁烯，丁二烯和乙炔的C4流中回收1,3-丁二烯的方法。回收高纯度1,3-丁二烯的方法包括乙炔转化，用于通过液相氢化选择性地转化乙炔，使得乙炔含量降低至70重量ppm以下，使用萃取蒸馏塔进行1,3-丁二烯萃取，预分离器，溶剂汽提塔，溶剂回收塔和纯化塔。通过乙炔转化，乙烯基乙炔的浓度降低至70重量ppm以下，此后仅使用一个萃取蒸馏塔回收1,3-丁二烯，从而大大降低了在过程中的效用和流失萃取。该方法所需的单元数量减少，从而显着地减少了杂质在处理单元中积累的时间。

6. 发明申请

US20090302912A1 DUTY CYCLE CORRECTION CIRCUIT OF SEMICONDUCTOR MEMORY APPARATUS 有权
标题翻译：半导体存储器的占空比校正电路
公开(公告)号：US20090302912A1
公开(公告)日：2009-12-10
申请号：US12346683
申请日：2008-12-30
申请人： Seong Jun Lee
发明人： Seong Jun Lee
IPC分类号： H03K3/017
CPC分类号： H03K5/1565 , G11C7/22 , G11C7/222
摘要： A duty cycle correction circuit of a semiconductor memory apparatus includes a duty ratio correcting unit configured to correct a duty ratio of a clock signal according to levels of a first reference voltage and a second reference voltage, and to output the clock signal as a correction clock signal, a duty ratio detecting unit configured to count first and second counting signals in response to a duty ratio of the correction clock signal when a pump enable signal is enabled, a pump enable signal generating unit configured to generate the pump enable signal in response to the duty ratio of the correction clock signal, and a reference voltage generating unit configured to generate the first and second reference voltages in response to the first and second counting signals.
摘要翻译：半导体存储装置的占空比校正电路包括占空比校正单元，其被配置为根据第一参考电压和第二参考电压的电平来校正时钟信号的占空比，并将时钟信号作为校正时钟输出信号，占空比检测单元，被配置为当启用泵使能信号时响应于所述校正时钟信号的占空比来对第一和第二计数信号进行计数;泵使能信号生成单元，被配置为响应于校正时钟信号的占空比，以及被配置为响应于第一和第二计数信号而产生第一和第二参考电压的参考电压产生单元。

7. 发明申请

US20090088594A1 BISMUTH MOLYBDATE-BASED CATALYSTS, METHOD OF PREPARING THEREOF AND METHOD OF PREPARING 1,3-BUTADIENE USING THEREOF 有权
标题翻译： BISMUTH MOLYBAST基催化剂及其制备方法及其制备1,3-丁二烯的方法
公开(公告)号：US20090088594A1
公开(公告)日：2009-04-02
申请号：US12297352
申请日：2007-03-16
申请人： Seung Hoon Oh , Seong Jun Lee , Tae Jin Kim , Ahn Seop Choi , Young Min Chung , In Kyu Song , Ji Chul Jung , Hee Soo Kim
发明人： Seung Hoon Oh , Seong Jun Lee , Tae Jin Kim , Ahn Seop Choi , Young Min Chung , In Kyu Song , Ji Chul Jung , Hee Soo Kim
IPC分类号： C07C5/333 , B01J23/31
CPC分类号： B01J35/0006 , B01J23/31 , B01J35/002 , B01J37/03 , C07C5/3335 , C07C2523/644 , C07C11/167
摘要： This invention relates to a bismuth molybdate catalyst, a preparation method thereof, and a method of preparing 1,3-butadiene using the same, and to a bismuth molybdate catalyst, a preparation method thereof, and a method of preparing 1,3-butadiene using the same, in which 1,3-butadiene can be prepared through oxidative dehydrogenation directly using a C4 mixture including n-butene and n-butane as a reactant in the presence of a mixed-phase bismuth molybdate catalyst including α-bismuth molybdate (Bi2Mo3On) and γ-bismuth molybdate (Bi2MoO6). According to this invention, the C4 raffinate, containing many impurities, is used as a reactant, without an additional n-butane separation process, thus obtaining 1,3-butadiene at high yield. Unlike complicated multicomponent-based metal oxides, the catalyst of the invention has simple constituents and synthesis routes, and can be easily formed through physical mixing, and thus is very advantageous in assuring reproducibility and can be directly applied to commercial processes.
摘要翻译：本发明涉及钼酸铋催化剂及其制备方法，以及使用其制备1,3-丁二烯的方法，以及钼酸铋催化剂及其制备方法以及制备1,3-丁二烯的方法使用相同的方法，其中可以通过氧化脱氢制备1,3-丁二烯，其中包括在包括α-钼酸铋的混合钼酸铋催化剂存在下，使用包含正丁烯和正丁烷的C4混合物作为反应物 Bi2Mo3On）和γ-钼酸铋（Bi2MoO6）。根据本发明，不含额外的正丁烷分离方法，将含有许多杂质的C4萃余液用作反应物，从而以高产率获得1,3-丁二烯。不同于复合多组分金属氧化物，本发明的催化剂具有简单的组成和合成路线，并且可以通过物理混合容易地形成，因此在确保再现性方面是非常有利的，并且可以直接应用于商业过程。

8. 发明授权

US11294202B2 Contact lens for presbyopia 有权
公开(公告)号：US11294202B2
公开(公告)日：2022-04-05
申请号：US16302048
申请日：2017-06-28
申请人： Seong Jun Lee , Hyun Seung Lee , Hyun Jeong Lee
发明人： Seong Jun Lee , Hyun Seung Lee , Hyun Jeong Lee
IPC分类号： G02C7/06 , G02C7/02 , G02C7/04
摘要： The present invention relates to a contact lens for presbyopia and, more specifically, to a contact lens for presbyopia, providing both a far-distance vision area and a near-distance vision area in one contact lens, and continuously forming a lens magnification of the far-distance vision area and the near-distance vision area of the dominant eye and the non-dominant eye while changing the sizes of the far-distance vision area and the near-distance vision area of two eyes according to the dominant eye and the non-dominant eye, such that an intermediate-distance area is partially overlapped, thereby continuously providing a near-distance vision area at a far distance by a neural summation phenomenon that selects a clearly visible image in both eyes.

9. 发明授权

US08410328B2 Method of preparing multicomponent bismuth molybdate catalysts comprising four metal components and method of preparing 1,3-butadiene using said catalysts 有权
标题翻译：制备包含四种金属组分的多组分钼酸铋催化剂的方法和使用所述催化剂制备1,3-丁二烯的方法
公开(公告)号：US08410328B2
公开(公告)日：2013-04-02
申请号：US12733865
申请日：2008-08-24
申请人： Young Min Chung , Tae Jin Kim , Seong Jun Lee , Yong Seung Kim , Seung Hoon Oh , In Kyu Song , Hee Soo Kim , Ji Chul Jung , Ho Won Lee
发明人： Young Min Chung , Tae Jin Kim , Seong Jun Lee , Yong Seung Kim , Seung Hoon Oh , In Kyu Song , Hee Soo Kim , Ji Chul Jung , Ho Won Lee
IPC分类号： C07C5/48 , B01J23/31
CPC分类号： B01J23/8876 , B01J23/002 , B01J23/8898 , B01J37/03 , B01J2523/00 , C07C5/48 , C07C2523/887 , C07C11/167 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/847 , B01J2523/27 , B01J2523/72 , B01J2523/845 , B01J2523/22 , B01J2523/17
摘要： A method of preparing multicomponent bismuth molybdate catalysts composed of four metal components and a method of preparing 1,3-butadiene using the catalyst, and particularly, to multicomponent bismuth molybdate catalysts composed of a divalent cationic metal, a trivalent cationic metal, bismuth and molybdenum, a preparation method thereof, and a method of preparing 1,3-butadiene from a C4 mixture including n-butene and n-butane using oxidative dehydrogenation are described.
摘要翻译：制备由四种金属组分组成的多组分钼酸铋催化剂的方法和使用该催化剂制备1,3-丁二烯的方法，特别是由二价阳离子金属，三价阳离子金属，铋和钼组成的多组分钼酸铋催化剂，其制备方法以及使用氧化脱氢从包含正丁烯和正丁烷的C4混合物制备1,3-丁二烯的方法。

10. 发明授权

US09090522B2 Method and apparatus for recovering ethylene from fluidized catalytic cracking (FCC) off-gas 有权
标题翻译：从流化催化裂化（FCC）废气中回收乙烯的方法和装置
公开(公告)号：US09090522B2
公开(公告)日：2015-07-28
申请号：US13819021
申请日：2011-08-26
申请人： Jong Ho Park , Jong Nam Kim , Hee Tae Beum , Seong Jun Lee , Jang Jae Lee , Dong Wook Kim , Chang Hyun Ko , Sang Sup Han , Soon Haeng Cho
发明人： Jong Ho Park , Jong Nam Kim , Hee Tae Beum , Seong Jun Lee , Jang Jae Lee , Dong Wook Kim , Chang Hyun Ko , Sang Sup Han , Soon Haeng Cho
IPC分类号： C07C7/12 , B01D53/047 , C07C7/13 , C10G70/04
CPC分类号： C07C7/12 , B01D53/047 , B01D2253/108 , B01D2256/24 , B01D2257/7022 , B01D2259/40073 , B01D2259/4063 , C07C7/13 , C10G70/046 , C10G2300/107 , C10G2300/4081 , C10G2400/20 , Y02C20/20 , Y02P30/464 , C07C11/04
摘要： A method and apparatus for concentrating and recovering ethylene from the off-gas from an apparatus which produces gasoline, propylene and the like by fluidized catalytic cracking (FCC) of heavy oils such as atmospheric residue, generated in a crude oil refining process, is provided. The method and apparatus can reduce the amount of ethylene rinse in the subsequent ethylene displacement desorption process by increasing the ethylene purity of a raw material gas and reducing the concentration of weakly adsorbing components in the raw material gas and can reduce the loss of a desorbent during a distillation process for separating the desorbent from the weakly adsorbing components. Thus, ethylene can be recovered from the off-gas from fluidized catalytic cracking of heavy oils at high concentration and low cost.
摘要翻译：提供了一种从废气中浓缩和回收乙烯的方法和装置，该装置通过在原油精炼过程中产生的重质油如大气残留物的流化催化裂化（FCC）产生汽油，丙烯等。该方法和装置可以通过提高原料气体的乙烯纯度和降低原料气体中弱吸附组分的浓度来减少后续乙烯取代脱附过程中的乙烯冲洗量，并可以减少脱附剂在用于将解吸剂与弱吸附组分分离的蒸馏方法。因此，可以从废气中以高浓度和低成本从重油的流化催化裂化中回收乙烯。

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