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1. 发明申请

US20080071117A1 Method for the Continuous Production of Dmc Catalysts 审中-公开
标题翻译：连续生产Dmc催化剂的方法
公开(公告)号：US20080071117A1
公开(公告)日：2008-03-20
申请号：US11576105
申请日：2005-09-28
申请人： Edward Bohres , Michael Triller , Bernd Bechtloff , Raimund Ruppel
发明人： Edward Bohres , Michael Triller , Bernd Bechtloff , Raimund Ruppel
IPC分类号： C07C41/01
CPC分类号： C08G65/2663 , B01J19/18 , B01J19/26 , B01J27/26 , B01J35/002 , B01J2219/00033 , B01J2219/00182
摘要： The invention provides a continuous process for preparing DMC catalysts, which comprises continuously feeding the solutions of a metal salt and of a hexacyanometallate compound and, if appropriate, organic ligands and/or organic additives into a continuous reactor, and continuously withdrawing the resulting suspension of the DMC compound from the reactor.
摘要翻译：本发明提供了一种用于制备DMC催化剂的连续方法，其包括将金属盐和六氰基金属酸盐化合物以及如果合适的有机配体和/或有机添加剂的溶液连续地供入到连续反应器中，并连续地将所得悬浮液来自反应器的DMC化合物。

2. 发明授权

US07811958B2 Method for producing an DMC catalyst 失效
标题翻译： DMC催化剂的制造方法
公开(公告)号：US07811958B2
公开(公告)日：2010-10-12
申请号：US11908145
申请日：2006-03-07
申请人： Edward Bohres , Michael Triller , Raimund Ruppel
发明人： Edward Bohres , Michael Triller , Raimund Ruppel
IPC分类号： B01J27/26
CPC分类号： B01J27/26 , C08G65/2663
摘要： The invention relates to a process for preparing DMC catalysts by reacting cyanometalate compounds, preferably cyanometalate salts, in particular alkali metal or alkaline earth metal salts, with metal salts, wherein the reaction is carried out in the presence of a Brönsted acid.
摘要翻译：本发明涉及一种制备DMC催化剂的方法，该方法通过氰化金属盐化合物，优选氰酸金属盐，特别是碱金属或碱土金属盐与金属盐反应，其中反应在布朗斯台德酸存在下进行。

3. 发明申请

US20080167502A1 Method For Producing an Dmc Catalyst 失效
标题翻译：生产Dmc催化剂的方法
公开(公告)号：US20080167502A1
公开(公告)日：2008-07-10
申请号：US11908145
申请日：2006-03-07
申请人： Edward Bohres , Michael Triller , Raimund Ruppel
发明人： Edward Bohres , Michael Triller , Raimund Ruppel
IPC分类号： C07C41/26 , C07F3/06
CPC分类号： B01J27/26 , C08G65/2663
摘要： The invention relates to a process for preparing DMC catalysts by reacting cyano-metalate compounds, preferably cyanometalate salts, in particular alkali metal or alkaline earth metal salts, with metal salts, wherein the reaction is carried out in the presence of a Brönsted acid.
摘要翻译：本发明涉及通过氰基金属化合物，优选氰基金属盐，特别是碱金属或碱土金属盐与金属盐反应制备DMC催化剂的方法，其中反应在布朗斯台德酸存在下进行。

4. 发明申请

US20120129685A1 PROCESS FOR PREPARING MULTIMETAL CYANIDE COMPOUNDS 审中-公开
标题翻译：制备多种氰基化合物的方法
公开(公告)号：US20120129685A1
公开(公告)日：2012-05-24
申请号：US13388406
申请日：2010-08-11
申请人： Jochen Mezger , Burkhard Walther , Helmut Mack , Simone Klapdohr , Zhizhong Cai , Silke Flakus , Tobias Austermann , Bernhard Hoffner , Wolfgang Rohde , Bernd Bechtloff , Michael Triller , Sirus Zarbakhsh
发明人： Jochen Mezger , Burkhard Walther , Helmut Mack , Simone Klapdohr , Zhizhong Cai , Silke Flakus , Tobias Austermann , Bernhard Hoffner , Wolfgang Rohde , Bernd Bechtloff , Michael Triller , Sirus Zarbakhsh
IPC分类号： B01J27/26
CPC分类号： C01C3/11 , B01J27/26 , B01J35/023 , C08G65/2663
摘要： The invention relates to a process for preparing multimetal cyanide compounds by reacting the aqueous solution of a metal salt a) with the aqueous solution of a hexacyanometalate compound b), wherein the mixture of the solutions a) and b) flows over the surface of a rotating body A to an outer region of the surface of the rotating body A and is flung off from there.
摘要翻译：本发明涉及通过使金属盐a）的水溶液与六氰基金属酸盐化合物b）的水溶液反应制备多金属氰化合物的方法，其中溶液a）和b）的混合物在将旋转体A旋转到旋转体A的表面的外部区域，并从那里脱落。

5. 发明申请

US20080300376A1 Method for the Production of Multimetal Cyanide Compounds 失效
公开(公告)号：US20080300376A1
公开(公告)日：2008-12-04
申请号：US12095805
申请日：2006-11-23
申请人： Michael Triller , Raimund Ruppel
发明人： Michael Triller , Raimund Ruppel
IPC分类号： C08G18/22 , C07F15/06
CPC分类号： B01J27/26 , B01J27/02 , B01J37/0201 , B01J37/30 , C08G18/4866 , C08G65/2663
摘要： Process for preparing multimetal cyanide compounds, which comprises the stepsa) reaction of the aqueous solution of a metal salt of the general formula (I) M1gXn (I) with the aqueous solution of a cyanometalate compound of the general formula (II) M3r[M2(CN)b]d, , (II) if appropriate in the presence of organic ligands, organic additives and/or surface-active agents,to form a multimetal cyanide compound of the general formula (III) M1a[M2(CN)b]d.fM1jXk.h(H2O).eL.zP (III) b) reaction of the multimetal cyanide compound of the general formula (III) with a salt of the general formula (IV) M4sYt , (IV) which is different from (II) whereM1 is a metal ion selected from the group consisting of Zn2+, Fe2+, Fe3+, Co2+, Co3+, Ni2+, Mn2+, Sn2+, Sn4+, Pb2+, Al3+, Sr2+, Cr3+, Cd2+, Cu2+, La3+, Ce3+, Ce4+, Eu3+, Mg2+, Ti4+, Ag+, Rh2+, Ru2+, Ru3+, Pd2+M2 is a metal ion selected from the group consisting of Fe2+, Fe3+, Co2+, Co3+, Mn2+, Mn3+, Ni2+, Cr2+, Cr3+, Rh3+, Ru2+, Ir3+and M1 and M2 are identical or different,X is an anion, selected from the group consisting of halide, hydroxide, sulfate, hydrogensulfate, carbonate, hydrogencarbonate, cyanide, thiocyanate, isocyanate, cyanate, carboxylate, oxalate, nitrate and nitrite (NO2—) or a mixture of two or more of the abovementioned anions or a mixture of one or more of the abovementioned anions with an uncharged species selected from among CO, H2O and NO,Y is an anion which is different from X and is selected from the group consisting of halide, sulfate, hydrogensulfate, disulfate, sulfite, sulfonate, (═RSO3—where R═C1-C20-alkyl, aryl, C1-C2-alkylaryl), carbonate, hydrogencarbonate, cyanide, thiocyanate, isocyanate, isothiocyanate, cyanate, carboxylate, oxalate, nitrate, nitrite, phosphate, hydrogenphosphate, dihydrogenphosphate, diphosphate, borate, tetraborate, perchlorate, tetrafluoroborate, hexafluorophosphate, tetraphenylborate,L is a water-miscible ligand selected from the group consisting of alcohols, aldehydes, ketones, ethers, polyethers, esters, polyesters, polycarbonate, ureas, amides, nitriles, and sulfides and mixtures thereof,P is an organic additive, selected from the group consisting of polyethers, polyesters, polycarbonates, polyalkylene glycol sorbitan esters, polyalkylene glycol glycidyl ethers, polyacrylamide, poly(acrylamide-co-acrylic acid), polyacrylic acid, poly(acrylamide-co-maleic acid), polyacrylonitrile, polyalkyl acrylate, polyalkyl methacrylate, polyvinyl methyl ether, polyvinyl ethyl ether, polyvinyl acetate, polyvinyl alcohol, poly-N-vinylpyrrolidone, poly(N-vinylpyrrolidone-co-acrylic acid), polyvinyl methyl ketone, poly(4-vinylphenol), poly(acrylic acid-co-styrene), oxazoline polymers, polyalkylenimines, maleic acid and maleic anhydride copolymers, hydroxyethylcellulose, polyacetates, ionic surface- and interface-active compounds, bile acids, and their salts, esters and amides, carboxylic esters of polyhydric alcohols and glycosides,anda, b, d, g, n, r, s, j, k and t are integers or fractions greater than zero,e, f, h and z are integers or fractions greater than or equal to zerowherea, b, d, g, n, j, k and r and also s and t are selected so that the compound is electrically neutral,M3 is hydrogen or an alkali metal or alkaline earth metal, andM4 is an alkali metal ion or an ammonium ion (NH4+) or an alkylammonium ion (R4N+, R3NH+, R2NH2+, RNH3+ where R═C1-C20-alkyl).

6. 发明授权

US08119825B2 Method for the production of multimetal cyanide compounds 失效
标题翻译：生产多金属氰化物的方法
公开(公告)号：US08119825B2
公开(公告)日：2012-02-21
申请号：US12095805
申请日：2006-11-23
申请人： Michael Triller , Raimund Ruppel
发明人： Michael Triller , Raimund Ruppel
IPC分类号： C07F15/00 , C01B21/06 , C08G18/00
CPC分类号： B01J27/26 , B01J27/02 , B01J37/0201 , B01J37/30 , C08G18/4866 , C08G65/2663
摘要： Process for preparing multimetal cyanide compounds, which comprises the steps a) reaction of the aqueous solution of a metal salt of the general formula (I) M1gXn (I) With the aqueous solution of a cyanometalate compound of the general formula (II) M3r[M2(CN)b]d, (II), If appropriate in the presence of organic ligands, organic additives and/or surface-active agents, to form a multimetal cyanide compound of the general formula (III) M1a[M2(CN)b]d.fM1jXk.h(H2O).eL.zP (III) b) reaction of the multimetal cyanide compound of the general formula (III) with a salt of the general formula (IV) M4sYt (IV) which is different from general formula (II) where M1, M2, M3, M4, X, L, P, Y, g, n, r, b, d, a, f, j, k, h, e, z, s, and t are defined in the specification.
摘要翻译：制备多金属氰化合物的方法，其包括步骤a）通式（I）的化合物M1gXn（I）的水溶液与通式（II）的氰基金属化合物的水溶液反应， M2（CN）b] d，（II）如果在有机配体，有机添加剂和/或表面活性剂存在下适当，形成通式（III）的多金属氰化物M1a [M2（CN） b）d.fM1jXk.h（H2O）.eL.zP（III）b）通式（III）的多金属氰化合物与通式（IV）的盐与M4sYt（IV）不同的反应通式（II）其中M1，M2，M3，M4，X，L，P，Y，g，n，r，b，d，a，f，j，k，h，e，z，s和t 在规范中定义。

7. 发明授权

US07807615B2 Production of (co)surfactants by reacting polyols with olefins 有权
标题翻译：通过使多元醇与烯烃反应制备（共）表面活性剂
公开(公告)号：US07807615B2
公开(公告)日：2010-10-05
申请号：US11911028
申请日：2006-04-05
申请人： Juergen Stephan , Michael Roeper , Thomas Heidemann , Michael Triller , Juergen Tropsch
发明人： Juergen Stephan , Michael Roeper , Thomas Heidemann , Michael Triller , Juergen Tropsch
IPC分类号： C11D1/66
CPC分类号： C07C41/06 , C07C43/135 , C08G65/329 , C11D1/72 , C11D1/721 , C11D3/3707 , Y02P20/582
摘要： The present invention relates to a process for preparing polyol alkyl ethers by reacting compounds comprising at least three hydroxyl functionalities with olefins in the presence of acidic catalysts at temperatures of from 20 to 250° C. and pressures of from 0.5 to 10 bar, wherein the olefins correspond to the general formula (I) in which R1 is hydrogen and R2 is a linear or branched carbon radical having from 7 to 28 carbon atoms, or R1 and R2 are each linear or branched carbon radicals having from 1 to 27 carbon atoms, the sum of the carbon number of R1 and R2 being at most 28, to polyol alkyl ethers derived from compounds having at least three hydroxyl functionalities, not more than all but one hydroxyl functionality being replaced by a moiety of the general formula (VIII) to the use of these polyol alkyl ethers as surfactants and to laundry detergents and cleaning compositions comprising these polyol alkyl ethers.
摘要翻译：本发明涉及一种制备多元醇烷基醚的方法，该方法是在20至250℃的温度和0.5至10巴的压力下，在酸性催化剂存在下，使包含至少三个羟基官能团的化合物与烯烃反应，烯烃对应于其中R 1为氢且R 2为具有7至28个碳原子的直链或支链碳原子的通式（I），或R 1和R 2为具有1至27个碳原子的直链或支链碳原子， R 1和R 2的碳数最多为28的多元醇烷基醚衍生自具有至少三个羟基官能团的化合物的多元醇烷基醚，不超过一个羟基官能团，除了一个羟基官能团被通式（Ⅷ）的部分替代为使用这些多元醇烷基醚作为表面活性剂和洗衣洗涤剂以及包含这些多元醇烷基醚的清洁组合物。

8. 发明申请

US20080281116A1 Acid-Functionalized Organometallic Framework Materials 有权
标题翻译：酸官能化有机金属框架材料
公开(公告)号：US20080281116A1
公开(公告)日：2008-11-13
申请号：US12096619
申请日：2006-12-12
申请人： Markus Schubert , Ulrich Muller , Marco Bosch , Michael Triller , Stephan Hatscher
发明人： Markus Schubert , Ulrich Muller , Marco Bosch , Michael Triller , Stephan Hatscher
IPC分类号： C07F5/06
CPC分类号： B01J31/1691 , B01J20/226 , B01J39/26 , B01J45/00 , B01J2231/49 , C07C51/418 , C07F5/069 , C07C63/28
摘要： The present invention relates to porous metal organic frameworks comprising at least one at least bidentate organic compound L coordinated to at least one metal ion M, wherein L has at least one functional group G which bonds noncoordinatively to M and is selected from the group consisting of —SO3H and —PO3H2 and their analogues. The invention further provides processes for their preparation and also their use.
摘要翻译：本发明涉及包含至少一种与至少一种金属离子M配位的至少二齿有机化合物L的多孔金属有机骨架，其中L具有至少一个官能团G，其与M非键合键合并选自 -SO 3 H和-PO 3 H 2 H 2和它们的类似物。本发明进一步提供了它们的制备方法及其应用。

9. 发明申请

US20100029961A1 DMC CATALYSTS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF 失效
标题翻译： DMC催化剂，其生产方法及其用途
公开(公告)号：US20100029961A1
公开(公告)日：2010-02-04
申请号：US12525828
申请日：2008-01-31
申请人： Michael Triller , Matthias Schopohl , Veit Stegmann , Thomas Ostrowski
发明人： Michael Triller , Matthias Schopohl , Veit Stegmann , Thomas Ostrowski
IPC分类号： C07C41/02 , B01J27/26 , B01J31/26 , C07D301/00
CPC分类号： B01J27/26 , B01J31/0278 , B01J37/031 , C08G65/2606 , C08G65/2663 , Y02P20/542
摘要： The invention relates to a process for preparing DMC catalysts by reaction of cyanometalate compounds with metal salts, wherein the reaction is carried out in ionic liquids as solvents or suspension media.
摘要翻译：本发明涉及一种通过氰化金属化合物与金属盐反应制备DMC催化剂的方法，其中反应在离子液体中作为溶剂或悬浮介质进行。

10. 发明申请

US20080176782A1 Production of (Co)Surfactants by Reacting Polyols With Olefins 有权
标题翻译：通过与烯烃反应多元醇制备（Co）表面活性剂
公开(公告)号：US20080176782A1
公开(公告)日：2008-07-24
申请号：US11911028
申请日：2006-04-05
申请人： Jurgen Stephan , Michael Roper , Thomas Heidemann , Michael Triller , Jurgen Tropsch
发明人： Jurgen Stephan , Michael Roper , Thomas Heidemann , Michael Triller , Jurgen Tropsch
IPC分类号： C11D1/66 , C07C41/06 , C07C43/13
CPC分类号： C07C41/06 , C07C43/135 , C08G65/329 , C11D1/72 , C11D1/721 , C11D3/3707 , Y02P20/582
摘要： The present invention relates to a process for preparing polyol alkyl ethers by reacting compounds comprising at least three hydroxyl functionalities with olefins in the presence of acidic catalysts at temperatures of from 20 to 250° C. and pressures of from 0.5 to 10 bar, wherein the olefins correspond to the general formula (I) in which R1 is hydrogen and R2 is a linear or branched carbon radical having from 7 to 28 carbon atoms, or R1 and R2 are each linear or branched carbon radicals having from 1 to 27 carbon atoms, the sum of the carbon number of R1 and R2 being at most 28, to polyol alkyl ethers derived from compounds having at least three hydroxyl functionalities, not more than all but one hydroxyl functionality being replaced by a moiety of the general formula (VIII) to the use of these polyol alkyl ethers as surfactants and to laundry detergents and cleaning compositions comprising these polyol alkyl ethers.
摘要翻译：本发明涉及一种制备多元醇烷基醚的方法，该方法是在20至250℃的温度和0.5至10巴的压力下，在酸性催化剂存在下，使包含至少三个羟基官能团的化合物与烯烃反应，烯烃对应于其中R 1为氢且R 2为具有7至28个碳原子的直链或支链碳基团的通式（I），或R' SUP 1和R 2各自为具有1至27个碳原子的直链或支链碳原子，R 1和R 2的碳数之和至少28个的多元醇烷基醚衍生自具有至少三个羟基官能团的化合物，不超过一个羟基官能团，除了一个羟基官能团被通式（VIII）的部分替代为使用的这些多元醇烷基醚作为表面活性剂和洗涤剂和包含这些多元醇烷基醚的清洁组合物。

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