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1. 发明申请

US20130317190A1 COPOLYMERIZABLE SURFACTANTS 审中-公开
标题翻译：可共聚表面活性剂
公开(公告)号：US20130317190A1
公开(公告)日：2013-11-28
申请号：US13979770
申请日：2011-10-08
申请人： Thomas Schliwka , Thomas Mausberg , Uwe Held , Ronald Klagge , Stefan Busch , Markus Scherer
发明人： Thomas Schliwka , Thomas Mausberg , Uwe Held , Ronald Klagge , Stefan Busch , Markus Scherer
IPC分类号： C07D303/48 , C08F224/00 , C07F9/655
CPC分类号： C07D303/48 , C07F9/65502 , C08F2/24 , C08F2/26 , C08F224/00
摘要： The invention relates to the use of compounds of the formula (I), R—CH(O—(AO)mX)—CH2—O—(AO)—CH2—CH═CH2, where: R denotes an alkyl radical which has 8 to 18 carbon atoms and can be saturated or unsaturated, straight-chain or branched; X denotes a sulfate or phosphate group or hydrogen; (AO) denotes an alkylene oxide unit, selected from the group consisting of ethylene oxide, propylene oxide or butylene oxide; n denotes a number in the range of 0 to 50; and m denotes zero or a number in the range of 1 to 30; as copolymerizable emulsifiers in the emulsion polymerization of olefinically unsaturated monomers.
摘要翻译：本发明涉及式（I），R-CH（O-（AO）m X）-CH 2 -O-（AO）-CH 2 -CH = CH 2的化合物的用途，其中：R表示具有 8至18个碳原子，可以是饱和或不饱和的，直链或支链的; X表示硫酸根或磷酸基或氢; （AO）表示选自环氧乙烷，环氧丙烷或环氧丁烷的环氧烷单元; n表示0〜50的范围的数; m表示0或1〜30的数; 作为烯属不饱和单体的乳液聚合中的可共聚的乳化剂。

2. 发明申请

US20100331486A1 COPOLYMERIZABLE SURFACTANTS (1) 有权
标题翻译：可共聚表面活性剂（1）
公开(公告)号：US20100331486A1
公开(公告)日：2010-12-30
申请号：US12824394
申请日：2010-06-28
申请人： Ronald Klagge , Uwe Held , Thomas Mausberg , Katharina Hömberg , Thomas Schliwka
发明人： Ronald Klagge , Uwe Held , Thomas Mausberg , Katharina Hömberg , Thomas Schliwka
IPC分类号： C08L33/14
CPC分类号： C08F2/24 , C08F222/20
摘要： The invention is directed to the use of maleic esters selected from compounds of formulae (I), (II) and (III), as copolymerizable emulsifiers in the emulsion polymerization of olefinically unsaturated monomers, in which A is a C3-C40 alkyl group; X, Y and Z independently are hydrogen or methyl; B and D independently are sulfate, phosphate or hydrogen; n and p independently are numbers in the range from 0 to 40; and m is a number in the range from 2 to 40.
摘要翻译：本发明涉及在烯属不饱和单体的乳液聚合中使用选自式（I），（II）和（III）的化合物的马来酸酯作为可共聚的乳化剂，其中A为C 3 -C 40烷基; X，Y和Z独立地是氢或甲基; B和D独立地是硫酸根，磷酸根或氢原子; n和p独立地为0至40的数字; m为2〜40的数。

3. 发明申请

US20090289220A1 Aqueous Surfactant Compositions With A Low Pour Point 有权
标题翻译：具有低倾点的水性表面活性剂组合物
公开(公告)号：US20090289220A1
公开(公告)日：2009-11-26
申请号：US12469117
申请日：2009-05-20
申请人： Ronald Klagge , Markus Scherer , Thomas Schliwka , Katharina Homberg , Uwe Held , Thomas Mausberg
发明人： Ronald Klagge , Markus Scherer , Thomas Schliwka , Katharina Homberg , Uwe Held , Thomas Mausberg
IPC分类号： C09K3/00
CPC分类号： B01F17/0021 , B01F17/0085 , C08F2/24
摘要： Surfactant compositions which comprise (i) 10 to 90% by weight of one or more compounds selected from the group (a) to (e), and (ii) 10 to 90% by weight of water, based on the composition, are disclosed, where the compounds (a) to (e) are defined as follows: (a) addition products of ethylene oxide and/or propylene oxide with allyl alcohol, (b) addition products of ethylene oxide and/or propylene oxide with allyl alcohol, terminally capped with C1-20 alkyl, (c) compounds of the formula R1—O—X—R2, where X is 1 to 40 ethylene oxide and/or propylene oxide units and where R1 and R2 independently are C1-20 alkyl, excluding allyl, (d) compounds of the formula R3—O—X—H, where X is 1 to 40 ethylene oxide and/or propylene oxide units and where R3 is C1-20 alkyl, excluding allyl, (e) compounds of the formula H—O—X—H, where X is 1 to 40 ethylene oxide and/or propylene oxide units. The surfactant compositions are liquid and pourable at 20° C., with a pour point below 0° C., and are useful as emulsifiers in emulsion polymerization.
摘要翻译：公开了表面活性剂组合物，其包含（i）10至90重量％的一种或多种选自组（a）至（e）的化合物和（ii）10至90重量％的水，基于组合物其中化合物（a）至（e）定义如下：（a）环氧乙烷和/或环氧丙烷与烯丙醇的加成产物，（b）环氧乙烷和/或环氧丙烷与烯丙醇的加成产物，末端用C 1-20烷基封端，（c）式R1-OX-R2的化合物，其中X是1至40个环氧乙烷和/或环氧丙烷单元，其中R 1和R 2独立地是C 1-20烷基，不包括烯丙基，（d）式R3-OXH的化合物，其中X为1至40个环氧乙烷和/或环氧丙烷单元，其中R3为C1-20烷基，不包括烯丙基，（e）式HOXH化合物，其中X为1 至40个环氧乙烷和/或环氧丙烷单元。表面活性剂组合物是液体并且在20℃下倾倒，倾点低于0℃，并且可用作乳液聚合中的乳化剂。

4. 发明申请

US20080139744A1 Fatty Alcohol Polyglycol Ether Sulfates as Emulsifiers for Emulsion Polymerization 审中-公开
标题翻译：脂肪醇聚乙二醇硫酸酯作乳化聚合乳化剂
公开(公告)号：US20080139744A1
公开(公告)日：2008-06-12
申请号：US11791563
申请日：2005-11-12
申请人： Uwe Held , Wolfgang Breuer , Thomas Mausberg
发明人： Uwe Held , Wolfgang Breuer , Thomas Mausberg
IPC分类号： C08F2/16 , C08G65/34
CPC分类号： C08F2/26
摘要： The invention is directed to an emulsifier for emulsion polymerization. The emulsifier is obtained by alkoxylating a mixture of (a) 20% to 80% by weight of a fatty alcohol containing 8 to 22 carbon atoms and (b) 20% to 80% by weight of a ring opening product of a 1,2-epoxyalkane containing 8 to 18 carbon atoms with ethylene glycol, with from 5 to 100 mol ethylene oxide per equivalent of free OH groups in the sums of (a) and (b) and sulfation of the intermediate product obtained to form the emulsifier. The emulsifier provides a polymer similar with low coagulum and high stability.
摘要翻译：本发明涉及一种用于乳液聚合的乳化剂。通过将（a）20重量％至80重量％的含有8-22个碳原子的脂肪醇和（b）20重量％至80重量％的1,2开环产物的混合物含有8至18个碳原子的环氧烷烃与乙二醇，以及（a）和（b）之和中的每当量游离OH基团为5-100摩尔环氧乙烷，以及获得的中间体产物的硫酸化形成乳化剂。乳化剂提供与低凝固物相似的聚合物和高稳定性。

5. 发明授权

US08183320B2 Copolymerizable surfactants (1) 有权
标题翻译：可共聚表面活性剂（1）
公开(公告)号：US08183320B2
公开(公告)日：2012-05-22
申请号：US12824394
申请日：2010-06-28
申请人： Ronald Klagge , Uwe Held , Thomas Mausberg , Katharina Hömberg , Thomas Schliwka
发明人： Ronald Klagge , Uwe Held , Thomas Mausberg , Katharina Hömberg , Thomas Schliwka
IPC分类号： C08L31/06
CPC分类号： C08F2/24 , C08F222/20
摘要： The invention is directed to the use of maleic esters selected from compounds of formulae (I), (II) and (III), as copolymerizable emulsifiers in the emulsion polymerization of olefinically unsaturated monomers, in which A is a C3-C40 alkyl group; X, Y and Z independently are hydrogen or methyl; B and D independently are sulfate, phosphate or hydrogen; n and p independently are numbers in the range from 0 to 40; and m is a number in the range from 2 to 40.
摘要翻译：本发明涉及在烯属不饱和单体的乳液聚合中使用选自式（I），（II）和（III）的化合物的马来酸酯作为可共聚的乳化剂，其中A为C 3 -C 40烷基; X，Y和Z独立地是氢或甲基; B和D独立地是硫酸根，磷酸根或氢原子; n和p独立地为0至40的数字; m为2〜40的数。

6. 发明申请

US20120029131A1 Use Of Nonionic Surfactants As Emulsifiers For Emulsion Polymerization (III) 失效
标题翻译：用作乳液聚合乳化剂的非离子表面活性剂（III）
公开(公告)号：US20120029131A1
公开(公告)日：2012-02-02
申请号：US13259846
申请日：2010-03-13
申请人： Markus Scherer , Thomas Schliwka , Katharina Hömberg , Uwe Held , Thomas Mausberg , Ronald Klagge
发明人： Markus Scherer , Thomas Schliwka , Katharina Hömberg , Uwe Held , Thomas Mausberg , Ronald Klagge
IPC分类号： C08K9/04 , C08L9/10 , C08L13/02 , C08L19/02
CPC分类号： C08F2/30
摘要： The invention relates to the use of aqueous solutions of nonionic surfactants as gel phase free emulator systems for the emulsion polymerization, wherein said nonionic surfactants are chosen from the group (a) of the addition products from 1 to 40 mol ethylene and/or propylene oxide per mol of allyl alcohol, and (b) of the addition products from 1 to 40 mol ethylene and/or propylene oxide per mol of allyl alcohol, wherein the OH-group of said addition products is end-capped in the sense that it is substituted by a group OR, wherein R is an alkyl group with 1 to 20 C-atoms, which can be saturated or unsaturated, straight chained or branched.
摘要翻译：本发明涉及非离子表面活性剂的水溶液用作乳液聚合的无凝胶相模拟器系统，其中所述非离子表面活性剂选自1-40mol乙烯和/或环氧丙烷加成产物（a）组每摩尔烯丙醇，和（b）每摩尔烯丙醇1至40摩尔乙烯和/或环氧丙烷的加成产物，其中所述加成产物的OH-基是在上述意义上被封端被OR取代，其中R是具有1-20个碳原子的烷基，其可以是饱和或不饱和的，直链或支链的。

7. 发明授权

US08779075B2 Use of nonionic surfactants as emulsifiers for emulsion polymerization (III) 失效
标题翻译：非离子表面活性剂用作乳液聚合乳化剂（III）
公开(公告)号：US08779075B2
公开(公告)日：2014-07-15
申请号：US13259846
申请日：2010-03-13
申请人： Markus Scherer , Thomas Schliwka , Katharina Hömberg , Uwe Held , Thomas Mausberg , Ronald Klagge
发明人： Markus Scherer , Thomas Schliwka , Katharina Hömberg , Uwe Held , Thomas Mausberg , Ronald Klagge
IPC分类号： C08F2/30
CPC分类号： C08F2/30
摘要： The invention relates to the use of aqueous solutions of nonionic surfactants as gel phase free emulsion systems for emulsion polymerization. The nonionic surfactants are chosen from the group (a) of the addition products from 1 to 40 mol ethylene and/or propylene oxide per mol of allyl alcohol, and (b) of the addition products from 1 to 40 mol ethylene and/or propylene oxide per mol of allyl alcohol, wherein the OH-group of said addition products is end-capped in the sense that it is substituted by a group OR, wherein R is an alkyl group with 1 to 20 C-atoms, which can be saturated or unsaturated, straight chained or branched.
摘要翻译：本发明涉及非离子表面活性剂的水溶液用作乳液聚合的无凝胶相乳液体系。非离子表面活性剂选自单体摩尔量为1至40mol乙烯和/或环氧丙烷/ mol烯丙醇的加成产物组（a），和（b）1-40mol乙烯和/或丙烯的加成产物氧化物/摩尔烯丙醇，其中所述加成产物的OH基在被基团OR取代的意义上被封端，其中R是具有1至20个C原子的烷基，其可以是饱和的或不饱和的，直链或支链的。

8. 发明授权

US08193281B2 Copolymerizable surfactants (2) 有权
标题翻译：可共聚表面活性剂（2）
公开(公告)号：US08193281B2
公开(公告)日：2012-06-05
申请号：US12824369
申请日：2010-06-28
申请人： Ronald Klagge , Uwe Held , Thomas Mausberg , Katharina Hömberg , Thomas Schliwka
发明人： Ronald Klagge , Uwe Held , Thomas Mausberg , Katharina Hömberg , Thomas Schliwka
IPC分类号： C08F2/16 , C08F220/18 , C08G18/62 , C08G73/10 , B32B21/08
CPC分类号： C08F2/24 , C08F222/20
摘要： The invention is directed to the use of maleic esters selected from compounds of formulae (I) and (II) as copolymerizable emulsifiers in the emulsion polymerization of olefinically unsaturated monomers, in which A is an alkyl group having 3 to 40 carbon atoms; X and Z independently are hydrogen or methyl; M is hydrogen, an alkali metal, alkaline earth metal, or an ammonium or other amine salt; and n and p independently are numbers in the range from 0 to 40.
摘要翻译：本发明涉及在烯属不饱和单体的乳液聚合中使用选自式（I）和（II）的化合物的马来酸酯作为可共聚的乳化剂，其中A是具有3-40个碳原子的烷基; X和Z独立地是氢或甲基; M是氢，碱金属，碱土金属或铵盐或其它胺盐; n和p分别为0〜40的数。

9. 发明申请

US20120130035A1 Low-Viscosity Aqueous Compositions 失效
标题翻译：低粘度水性组合物
公开(公告)号：US20120130035A1
公开(公告)日：2012-05-24
申请号：US13298468
申请日：2011-11-17
申请人： Thomas Schliwka , Ronald Klagge , Uwe Held , Thomas Mausberg
发明人： Thomas Schliwka , Ronald Klagge , Uwe Held , Thomas Mausberg
IPC分类号： C08F2/24 , C09K3/00
CPC分类号： C08F2/26 , C08F212/08 , C08F218/08 , C08F218/10 , C08F220/06 , C08F2220/1825 , C08F220/14
摘要： Provided are low-viscosity aqueous compositions comprising compounds of Formula (III) and (IV). These compositions are prepared by jointly ethoxylating a mixture of the compounds of the Formula (I) and (II) to give an intermediate which represents a mixture of compounds of Formulas (I*) and (II*). The intermediate is then converted by sulfation or phosphation and subsequent neutralization, into an aqueous composition comprising the compounds of Formula (III) and (IV). The aqueous compositions are notable for having, at 20° C., a Brookfield viscosity of 3000 mPas or less (measured at 20° C. with spindle 2 and 20 rpm), and are suitable as emulsifiers for emulsion polymerization.
摘要翻译：提供包含式（III）和（IV）的化合物的低粘度水性组合物。这些组合物通过将式（I）和（II）的化合物的混合物共聚乙氧基化以得到表示式（I *）和（II *）的化合物的混合物的中间体来制备。然后通过硫酸化或磷酸化并随后中和将中间体转化成包含式（III）和（IV）的化合物的水性组合物。含水组合物在20℃下的Brookfield粘度为3000mPa·s以下（在20℃下用纺锤2和20rpm测量）是显着的，并且适用于乳液聚合的乳化剂。

10. 发明授权

US08142681B2 Aqueous surfactant compositions with a low pour point 有权
标题翻译：具有低倾点的水性表面活性剂组合物
公开(公告)号：US08142681B2
公开(公告)日：2012-03-27
申请号：US12469117
申请日：2009-05-20
申请人： Ronald Klagge , Markus Scherer , Thomas Schliwka , Katharina Hömberg , Uwe Held , Thomas Mausberg
发明人： Ronald Klagge , Markus Scherer , Thomas Schliwka , Katharina Hömberg , Uwe Held , Thomas Mausberg
IPC分类号： C09K3/00 , C08F2/22
CPC分类号： B01F17/0021 , B01F17/0085 , C08F2/24
摘要： Surfactant compositions which comprise (i) 10 to 90% by weight of one or more compounds selected from the group (a) to (e), and (ii) 10 to 90% by weight of water, based on the composition, are disclosed, where the compounds (a) to (e) are defined as follows: (a) addition products of ethylene oxide and/or propylene oxide with allyl alcohol, (b) addition products of ethylene oxide and/or propylene oxide with allyl alcohol, terminally capped with C1-20 alkyl, (c) compounds of the formula R1—O—X—R2, where X is 1 to 40 ethylene oxide and/or propylene oxide units and where R1 and R2 independently are C1-20 alkyl, excluding allyl, (d) compounds of the formula R3—O—X—H, where X is 1 to 40 ethylene oxide and/or propylene oxide units and where R3 is C1-20 alkyl, excluding allyl, (e) compounds of the formula H—O—X—H, where X is 1 to 40 ethylene oxide and/or propylene oxide units. The surfactant compositions are liquid and pourable at 20° C., with a pour point below 0° C., and are useful as emulsifiers in emulsion polymerization.
摘要翻译：公开了表面活性剂组合物，其包含（i）10至90重量％的一种或多种选自组（a）至（e）的化合物和（ii）10至90重量％的水，基于组合物其中化合物（a）至（e）定义如下：（a）环氧乙烷和/或环氧丙烷与烯丙醇的加成产物，（b）环氧乙烷和/或环氧丙烷与烯丙醇的加成产物，末端用C 1-20烷基封端，（c）式R 1 -O-X-R 2化合物，其中X为1至40个环氧乙烷和/或环氧丙烷单元，并且其中R 1和R 2各自为C 1-20烷基，不包括烯丙基，（d）式R 3 -O-X-H的化合物，其中X为1至40个环氧乙烷和/或环氧丙烷单元，其中R 3为C 1-20烷基，不包括烯丙基，（e）式 H-O-X-H，其中X为1至40个环氧乙烷和/或环氧丙烷单元。表面活性剂组合物是液体并且在20℃下倾倒，倾点低于0℃，并且可用作乳液聚合中的乳化剂。

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