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1. 发明授权

US07704468B1 Method for forming an extraction agent for the separation of actinides from lanthanides 失效
标题翻译：形成用于从镧系元素分离锕系元素的萃取剂的方法
公开(公告)号：US07704468B1
公开(公告)日：2010-04-27
申请号：US11232541
申请日：2005-09-21
申请人： John R. Klaehn , Mason K. Harrup , Jack D. Law , Dean R. Peterman
发明人： John R. Klaehn , Mason K. Harrup , Jack D. Law , Dean R. Peterman
IPC分类号： C01G56/00
CPC分类号： G21F9/12 , C07F9/304 , C22B3/0052 , C22B3/007 , G21F9/125 , Y02P10/234
摘要： An extraction agent for the separation of trivalent actinides from lanthanides in an acidic media and a method for forming same are described, and wherein the methodology produces a stable regiospecific and/or stereospecific dithiophosphinic acid that can operate in an acidic media having a pH of less than about 7.
摘要翻译：描述了一种用于在酸性介质中从镧系元素分离三价锕系元素的提取剂及其形成方法，其中所述方法产生稳定的区域特异性和/或立体特异性二硫代次膦酸，其可在pH较小的酸性介质中操作比约7。

2. 发明授权

US07799293B2 Actinide extraction methods 失效
标题翻译：锕系提取方法
公开(公告)号：US07799293B2
公开(公告)日：2010-09-21
申请号：US11530508
申请日：2006-09-11
申请人： Dean R. Peterman , John R. Klaehn , Mason K. Harrup , Richard D. Tillotson , Jack D. Law
发明人： Dean R. Peterman , John R. Klaehn , Mason K. Harrup , Richard D. Tillotson , Jack D. Law
IPC分类号： B01D11/04 , C01G56/00 , C22B60/00
CPC分类号： C01G56/001 , C01F17/0006 , C07F9/304 , C22B3/007 , C22B59/00 , Y02P10/234
摘要： Methods of separating actinides from lanthanides are disclosed. A regio-specific/stereo-specific dithiophosphinic acid having organic moieties is provided in an organic solvent that is then contacted with an acidic medium containing an actinide and a lanthanide. The method can extend to separating actinides from one another. Actinides are extracted as a complex with the dithiophosphinic acid. Separation compositions include an aqueous phase, an organic phase, dithiophosphinic acid, and at least one actinide. The compositions may include additional actinides and/or lanthanides. A method of producing a dithiophosphinic acid comprising at least two organic moieties selected from aromatics and alkyls, each moiety having at least one functional group is also disclosed. A source of sulfur is reacted with a halophosphine. An ammonium salt of the dithiophosphinic acid product is precipitated out of the reaction mixture. The precipitated salt is dissolved in ether. The ether is removed to yield the dithiophosphinic acid.
摘要翻译：公开了从镧系元素分离锕系元素的方法。在有机溶剂中提供具有有机部分的区域特异性/立体特异性二硫代次膦酸，然后与含有锕系元素和镧系元素的酸性介质接触。该方法可以延伸到彼此分离锕系元素。提取锕系元素作为与二硫代次膦酸的络合物。分离组合物包括水相，有机相，二硫代次膦酸和至少一种锕系元素。组合物可以包括另外的锕系元素和/或镧系元素。还公开了包含至少两个选自芳族化合物和烷基的有机部分的二硫代次膦酸的方法，每个部分具有至少一个官能团。硫源与卤代膦反应。二硫代次膦酸产物的铵盐从反应混合物中沉淀出来。将沉淀的盐溶于乙醚中。除去乙醚，得到二硫代次膦酸。

3. 发明申请

US20100094042A1 METHOD FOR FORMING AN EXTRACTION AGENT FOR THE SEPARATION OF ACTINIDES FROM LANTHANIDES 失效
标题翻译：用于形成从土壤中分离丙酸酯的提取剂的方法
公开(公告)号：US20100094042A1
公开(公告)日：2010-04-15
申请号：US11232541
申请日：2005-09-21
申请人： John R. Klaehn , Mason K. Harrup , Jack D. Law , Dean R. Peterman
发明人： John R. Klaehn , Mason K. Harrup , Jack D. Law , Dean R. Peterman
IPC分类号： C07F9/30
CPC分类号： G21F9/12 , C07F9/304 , C22B3/0052 , C22B3/007 , G21F9/125 , Y02P10/234
摘要： An extraction agent for the separation of trivalent actinides from lanthanides in an acidic media and a method for forming same are described, and wherein the methodology produces a stable regiospecific and/or stereospecific dithiophosphinic acid that can operate in an acidic media having a pH of less than about 7.
摘要翻译：描述了一种用于在酸性介质中从镧系元素分离三价锕系元素的提取剂及其形成方法，其中所述方法产生稳定的区域特异性和/或立体特异性二硫代次膦酸，其可在pH较小的酸性介质中操作比约7。

4. 发明授权

US08158088B2 Extractant compositions for co-extracting cesium and strontium, a method of separating cesium and strontium from an aqueous feed, and calixarene compounds 失效
标题翻译：共萃取铯和锶的萃取剂组合物，从含水原料中分离铯和锶的方法和杯芳烃化合物
公开(公告)号：US08158088B2
公开(公告)日：2012-04-17
申请号：US12268189
申请日：2008-11-10
申请人： Dean R. Peterman , David H. Meikrantz , Jack D. Law , Catherine L. Riddle , Terry A. Todd , Mitchell R. Greenhalgh , Richard D. Tillotson , Richard A. Bartsch , Bruce A. Moyer , Laetitia H. Delmau , Peter V. Bonnesen
发明人： Dean R. Peterman , David H. Meikrantz , Jack D. Law , Catherine L. Riddle , Terry A. Todd , Mitchell R. Greenhalgh , Richard D. Tillotson , Richard A. Bartsch , Bruce A. Moyer , Laetitia H. Delmau , Peter V. Bonnesen
IPC分类号： B01D11/00
CPC分类号： C07D323/00 , C07C43/23
摘要： A mixed extractant solvent that includes at least one dialkyloxycalix[4]arenebenzocrown-6 compound, 4′,4′,(5′)-di-(t-butyldicyclohexano)-18-crown-6, at least one modifier, and, optionally, a diluent. The dialkyloxycalix[4]arenebenzocrown-6 compound is 1,3-alternate-25,27-di(octyloxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(decyloxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(dodecyloxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(2-ethylhexyl-1-oxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(3,7-dimethyloctyl-1-oxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(4-butyloctyl-1-oxy)calix[4]arenebenzocrown-6, or combinations thereof. The modifier is a primary alcohol. A method of separating cesium and strontium from an aqueous feed is also disclosed, as are dialkyloxycalix[4]arenebenzocrown-6 compounds and an alcohol modifier.
摘要翻译：包含至少一种二烷氧基钙[4]芳基苯并呋喃-6化合物，4'，4'，（5'） - 二 - （叔丁基二环己基）-18-冠-6的混合萃取剂溶剂，至少一种改性剂，任选地，稀释剂。二烷氧基钙[4]芳烃基苯并呋喃-6化合物是1,3-交替的25,27-二（辛氧基）杯[4]芳烃基苯并噻唑-6，1,3-交替的25,27-二（癸氧基）杯[4] 芳族苯并茂-6，1,3-交替的25,27-二（十二烷氧基）杯[4]芳烃基苯并茂-6，1,3-交替的25,27-二（2-乙基己基-1-氧）杯[4] （3,7-二甲基辛基-1-氧基）杯[4]芳烃基苯并呋喃-6,1,3交替的25,27-二（4-丁基辛基 - 1-氧基）杯[4]芳烃基苯并呋喃-6或其组合。改性剂是伯醇。还公开了一种从含水原料中分离铯和锶的方法，二烷基氧基钙[4]芳烃基苯并呋喃-6化合物和醇改性剂也是如此。

5. 发明授权

US07915472B2 Surface decontamination compositions and methods 有权
标题翻译：表面去污组合物和方法
公开(公告)号：US07915472B2
公开(公告)日：2011-03-29
申请号：US11350351
申请日：2006-02-07
申请人： Karen E. Wright , David C. Cooper , Dean R. Peterman , Ricky L. Demmer , Julia L. Tripp , Laurence C. Hull
发明人： Karen E. Wright , David C. Cooper , Dean R. Peterman , Ricky L. Demmer , Julia L. Tripp , Laurence C. Hull
IPC分类号： G21F9/00
CPC分类号： B08B7/0014 , Y10S588/901
摘要： Clay-based compositions capable of absorbing contaminants from surfaces or objects having surface faces may be applied to a surface and later removed, the removed clay-based compositions absorbing at least a portion of the contaminant from the surface or object to which it was applied.
摘要翻译：能够从具有表面的表面或物体吸收污染物的基于粘土的组合物可以施加到表面并随后除去，所移除的粘土基组合物从其所施加的表面或物体吸收至少一部分污染物。

6. 发明申请

US20100150798A1 ACTINIDE EXTRACTION METHODS AND ACTINIDE SEPARATION COMPOSITIONS 失效
标题翻译： ACTINIDE提取方法和ACTINIDE分离组合物
公开(公告)号：US20100150798A1
公开(公告)日：2010-06-17
申请号：US11530508
申请日：2006-09-11
申请人： Dean R. Peterman , John R. Klaehn , Mason K. Harrup , Richard D. Tillotson , Jack D. Law
发明人： Dean R. Peterman , John R. Klaehn , Mason K. Harrup , Richard D. Tillotson , Jack D. Law
IPC分类号： C22B60/00
CPC分类号： C01G56/001 , C01F17/0006 , C07F9/304 , C22B3/007 , C22B59/00 , Y02P10/234
摘要： Methods of separating actinides from lanthanides are disclosed. A regio-specific/stereo-specific dithiophosphinic acid having organic moieties is provided in an organic solvent that is then contacted with an acidic medium containing an actinide and a lanthanide. The method can extend to separating actinides from one another. Actinides are extracted as a complex with the dithiophosphinic acid. Separation compositions include an aqueous phase, an organic phase, dithiophosphinic acid, and at least one actinide. The compositions may include additional actinides and/or lanthanides. A method of producing a dithiophosphinic acid comprising at least two organic moieties selected from aromatics and alkyls, each moiety having at least one functional group is also disclosed. A source of sulfur is reacted with a halophosphine. An ammonium salt of the dithiophosphinic acid product is precipitated out of the reaction mixture. The precipitated salt is dissolved in ether. The ether is removed to yield the dithiophosphinic acid.
摘要翻译：公开了从镧系元素分离锕系元素的方法。在有机溶剂中提供具有有机部分的区域特异性/立体特异性二硫代次膦酸，然后与含有锕系元素和镧系元素的酸性介质接触。该方法可以延伸到彼此分离锕系元素。提取锕系元素作为与二硫代次膦酸的络合物。分离组合物包括水相，有机相，二硫代次膦酸和至少一种锕系元素。组合物可以包括另外的锕系元素和/或镧系元素。还公开了包含至少两个选自芳族化合物和烷基的有机部分的二硫代次膦酸的方法，每个部分具有至少一个官能团。硫源与卤代膦反应。二硫代次膦酸产物的铵盐从反应混合物中沉淀出来。将沉淀的盐溶于乙醚中。除去乙醚，得到二硫代次膦酸。

7. 发明申请

US20100116749A1 EXTRACTANT COMPOSITIONS FOR CO EXTRACTING CESIUM AND STRONTIUM, A METHOD OF SEPARATING CESIUM AND STRONTIUM FROM AN AQUEOUS FEED, CALIXARENE COMPOUNDS, AND AN ALCOHOL MODIFIER 失效
标题翻译：用于提取锶和锶的萃取剂组合物，从水性进料，氯仿化合物和醇醇改性剂分离铯和锶的方法
公开(公告)号：US20100116749A1
公开(公告)日：2010-05-13
申请号：US12268189
申请日：2008-11-10
申请人： DEAN R. PETERMAN , DAVID H. MEIKRANTZ , JACK D. LAW , CATHERINE L. RIDDLE , TERRY A. TODD , MITCHELL R. GREENHALGH , RICHARD D. TILLOTSON , RICHARD A. BARTSCH , BRUCE A. MOYER , LAETITIA H. DELMAU , PETER V. BONNESEN
发明人： DEAN R. PETERMAN , DAVID H. MEIKRANTZ , JACK D. LAW , CATHERINE L. RIDDLE , TERRY A. TODD , MITCHELL R. GREENHALGH , RICHARD D. TILLOTSON , RICHARD A. BARTSCH , BRUCE A. MOYER , LAETITIA H. DELMAU , PETER V. BONNESEN
IPC分类号： C07D323/00 , C09K3/00 , B01D17/00 , C07C43/205
CPC分类号： C07D323/00 , C07C43/23
摘要： A mixed extractant solvent that includes at least one dialkyloxycalix[4]arenebenzocrown-6 compound, 4′,4′,(5′)-di-(t-butyldicyclohexano)-18-crown-6, at least one modifier, and, optionally, a diluent. The dialkyloxycalix[4]arenebenzocrown-6 compound is 1,3-alternate-25,27-di(octyloxy)calix[4] arenebenzocrown-6, 1,3-alternate-25,27-di(decyloxy)calix[4]arene-benzocrown-6, 1,3-alternate-25,27-di(dodecyloxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(2-ethylhexyl-1-oxy)calix[4]arenebenzocrown-6, 1,3-alternate-25,27-di(3,7-dimethyloctyl-1-oxy)calix[4] arenebenzocrown-6, 1,3-alternate-25,27-di(4-butyloctyl-1-oxy)calix[4]arenebenzocrown-6, or combinations thereof. The modifier is a primary alcohol. A method of separating cesium and strontium from an aqueous feed is also disclosed, as are dialkyloxycalix[4]arenebenzocrown-6 compounds and an alcohol modifier.
摘要翻译：包含至少一种二烷氧基钙[4]芳基苯并呋喃-6化合物，4'，4'，（5'） - 二 - （叔丁基二环己基）-18-冠-6，至少一种改性剂的混合萃取剂溶剂，任选地，稀释剂。二烷氧基钙[4]芳烃基苯并呋喃-6化合物是1,3-交替的25,27-二（辛氧基）杯[4]芳烃基苯并噻唑-6，1,3-交替的25,27-二（癸氧基）杯[4] 芳基 - 苯并环己基-6,1,3-交替的25,27-二（十二烷氧基）杯[4]芳烃基苯并卡那-6，1,3-交替的25,27-二（2-乙基己基-1-氧）杯[ 4]芳基苯并卡隆-6,1,3-交替的25,27-二（3,7-二甲基辛基-1-氧基）杯[4]芳烃基苯并卡那-6，1,3-交替的25,27-二（4- 丁基辛-1-氧）杯[4]芳烃基苯甲酰基-6或其组合。改性剂是伯醇。还公开了一种从含水原料中分离铯和锶的方法，二烷基氧基钙[4]芳烃基苯并呋喃-6化合物和醇改性剂也是如此。

8. 发明申请

US20080179568A1 EXTRACTANT COMPOSITION INCLUDING CROWN ETHER AND CALIXARENE EXTRACTANTS 失效
标题翻译：提取物组合物，包括胡椒醚和加利福尼亚提取物
公开(公告)号：US20080179568A1
公开(公告)日：2008-07-31
申请号：US11859453
申请日：2007-09-21
申请人： David H. Meikrantz , Terry A. Todd , Catherine L. Riddle , Jack D. Law , Dean R. Peterman , Bruce J. Mincher , Christopher A. McGrath , John D. Baker
发明人： David H. Meikrantz , Terry A. Todd , Catherine L. Riddle , Jack D. Law , Dean R. Peterman , Bruce J. Mincher , Christopher A. McGrath , John D. Baker
IPC分类号： B01F1/00
CPC分类号： C22B3/002 , C22B26/00 , Y02P10/234
摘要： An extractant composition comprising a mixed extractant solvent consisting of calix[4] arene-bis-(tert-octylbenzo)-crown-6 (“BOBCalixC6”), 4′,4′,(5′)-di-(t-butyldicyclo-hexano)-18-crown-6 (“DtBu18C6”), and at least one modifier dissolved in a diluent. The DtBu18C6 may be present at from approximately 0.01M to approximately 0.4M, such as at from approximately 0.086 M to approximately 0.108 M. The modifier may be 1-(2,2,3,3-tetrafluoropropoxy)-3-(4-sec-butylphenoxy)-2-propanol (“Cs-7SB”) and may be present at from approximately 0.01M to approximately 0.8M. In one embodiment, the mixed extractant solvent includes approximately 0.15M DtBu18C6, approximately 0.007M BOBCalixC6, and approximately 0.75M Cs-7SB modifier dissolved in an isoparaffinic hydrocarbon diluent. The extractant composition further comprises an aqueous phase. The mixed extractant solvent may be used to remove cesium and strontium from the aqueous phase.
摘要翻译：一种萃取剂组合物，其包含由杯[4]芳烃 - 双 - （叔辛基苯并） - 起始-6（“BOBCalixC6”），4'，4'，（5'） - 二 - （叔丁基二环己烷）-18-冠-6（“DtBu18C6”）和溶解在稀释剂中的至少一种改性剂。 DtBu18C6可以以约0.01M至约0.4M，例如约0.086M至约0.108M存在。改性剂可以是1-（2,2,3,3-四氟丙氧基）-3-（4- 仲丁基苯氧基）-2-丙醇（“Cs-7SB”），并且可以以约0.01M至约0.8M存在。在一个实施方案中，混合萃取剂溶剂包括溶解在异链烷烃稀释剂中的约0.15M DtBu18C6，约0.007M BOBCalixC6和约0.75M Cs-7SB改性剂。萃取剂组合物还包含水相。混合的萃取剂溶剂可用于从水相中除去铯和锶。

9. 发明授权

US07291316B2 Cesium and strontium extraction using a mixed extractant solvent including crown ether and calixarene extractants 失效
标题翻译：使用包括冠醚和杯芳烃萃取剂的混合萃取剂溶剂进行铯和锶萃取
公开(公告)号：US07291316B2
公开(公告)日：2007-11-06
申请号：US10808039
申请日：2004-03-23
申请人： David H. Meikrantz , Terry A. Todd , Catherine L. Riddle , Jack D. Law , Dean R. Peterman , Bruce J. Mincher , Christopher A. McGrath , John D. Baker
发明人： David H. Meikrantz , Terry A. Todd , Catherine L. Riddle , Jack D. Law , Dean R. Peterman , Bruce J. Mincher , Christopher A. McGrath , John D. Baker
IPC分类号： C02F1/26 , C02F1/68 , G21F9/06
CPC分类号： C22B3/002 , C22B26/00 , Y02P10/234
摘要： A mixed extractant solvent including calix[4]arene-bis-(tert-octylbenzo)-crown-6 (“BOBCalixC6”), 4′,4′,(5′)-di-(t-butyldicyclo-hexano)-18-crown-6 (“DtBu18C6”), and at least one modifier dissolved in a diluent. The mixed extractant solvent may be used to remove cesium and strontium from an acidic solution. The DtBu18C6 may be present from approximately 0.01 M to approximately 0.4M, such as from approximately 0.086 M to approximately 0.108 M. The modifier may be 1-(2,2,3,3-tetrafluoropropoxy)-3-(4-sec-butylphenoxy)-2-propanol (“Cs-7SB”) and may be present from approximately 0.01M to approximately 0.8M. In one embodiment, the mixed extractant solvent includes approximately 0.15M DtBu18C6, approximately 0.007M BOBCalixC6, and approximately 0.75M Cs-7SB modifier dissolved in an isoparaffinic hydrocarbon diluent. The mixed extractant solvent may form an organic phase in an extraction system that also includes an aqueous phase. Methods of extracting cesium and strontium as well as strontium alone are also disclosed.
摘要翻译：混合萃取剂溶剂包括杯[4]芳烃双 - （叔辛基苯并） - 起始-6（“BOBCalixC6”），4'，4'，（5'） - 二 - （叔丁基二环己基） -crown-6（“DtBu18C6”）和溶解在稀释剂中的至少一种改性剂。混合的萃取剂溶剂可用于从酸性溶液中除去铯和锶。 DtBu18C6可以为约0.01M至约0.4M，例如约0.086M至约0.108M。改性剂可为1-（2,2,3,3-四氟丙氧基）-3-（4-仲 - 丁基苯氧基）-2-丙醇（“Cs-7SB”），并且可以以约0.01M至约0.8M存在。在一个实施方案中，混合萃取剂溶剂包括溶解在异链烷烃稀释剂中的约0.15M DtBu18C6，约0.007M BOBCalixC6和约0.75M Cs-7SB改性剂。混合的萃取剂溶剂可以在还包含水相的萃取系统中形成有机相。还公开了提取铯和锶以及单独的锶的方法。

10. 发明授权

US07846888B2 Long lasting decontamination foam 有权
标题翻译：持久的去污泡沫
公开(公告)号：US07846888B2
公开(公告)日：2010-12-07
申请号：US11349815
申请日：2006-02-07
申请人： Ricky L. Demmer , Dean R. Peterman , Julia L. Tripp , David C. Cooper , Karen E. Wright
发明人： Ricky L. Demmer , Dean R. Peterman , Julia L. Tripp , David C. Cooper , Karen E. Wright
IPC分类号： A62D3/00 , A61Q5/02 , C11D17/00
CPC分类号： A61L2/22 , A62D3/30 , A62D2101/02
摘要： Compositions and methods for decontaminating surfaces are disclosed. More specifically, compositions and methods for decontamination using a composition capable of generating a long lasting foam are disclosed. Compositions may include a surfactant and gelatin and have a pH of less than about 6. Such compositions may further include affinity-shifting chemicals. Methods may include decontaminating a contaminated surface with a composition or a foam that may include a surfactant and gelatin and have a pH of less than about 6.
摘要翻译：公开了用于去污表面的组合物和方法。更具体地，公开了使用能够产生持久的泡沫的组合物去污的组合物和方法。组合物可以包括表面活性剂和明胶，并且具有小于约6的pH。这样的组合物还可以包括亲和力化学药剂。方法可以包括用可包含表面活性剂和明胶并具有小于约6的pH的组合物或泡沫来净化污染的表面。

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