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    • 2. 发明授权
    • 기상성장 탄소나노섬유가 함유된 에폭시 나노복합재료의 제조방법 및 그로 제조된 나노복합재료
    • 含有蒸气碳纳米纤维及其制品的环氧纳米复合材料的制备方法
    • KR100665130B1
    • 2007-01-04
    • KR1020050086854
    • 2005-09-16
    • 한국화학연구원
    • 박수진이재락이은정서민강
    • C08J5/06C08J3/20B82Y30/00
    • Provided is a method for manufacturing an epoxy nanocomposite material, which allows vapor phase-grown carbon nanofibers to be dispersed well in a matrix resin while not using solvent, and thus enables production of a nanocomposite material having excellent mechanical strength and friction and wear characteristics. The method for manufacturing an epoxy nanocomposite material comprises the steps of: physically mixing 100 parts by weight of an epoxy matrix resin with 0.1-2.5 parts by weight of vapor phase-grown carbon nanofibers as a reinforcing agent to obtain the dispersion; and adding a curing agent to the dispersion to cure it. In the method, the curing step comprises the steps of: curing at 70-100 deg,C for 20-30 minutes under a heating rate of 5 deg.C/min.; and curing at 140-160 deg.C for 90-120 minutes; and curing at 180-200 deg.C for 40-60 minutes.
    • 提供一种制造环氧纳米复合材料的方法,其允许气相生长的碳纳米纤维在不使用溶剂的情况下良好地分散在基质树脂中,从而能够制备具有优异的机械强度和摩擦和磨损特性的纳米复合材料。 制造环氧纳米复合材料的方法包括以下步骤:将100重量份的环氧基体树脂与0.1-2.5重量份气相生长碳纳米纤维作为增强剂物理混合以获得分散体; 并向分散体中加入固化剂以使其固化。 在该方法中,固化步骤包括以5℃/ min的加热速率在70-100℃下固化20-30分钟的步骤。 并在140-160℃固化90-120分钟; 并在180-200℃固化40-60分钟。