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    • 1. 发明授权
    • 저장 및 작업 안정성이 향상된 유무기 복합 하드 코팅제조성물과 그 제조방법
    • 저장및작업안정성이향상된유무기복합하드코팅제조성물과그제조방저
    • KR100732085B1
    • 2007-06-25
    • KR1020060050830
    • 2006-06-07
    • 한국산업기술평가원(관리부서:요업기술원)(주)테크랜드
    • 임형미이승호이동진김대성김도현전봉열김상목
    • C09D183/00C09D5/00
    • Provided are a method for preparing a transparent coating agent, a transparent coating agent composition, a method for preparing a colored coating agent, and a colored coating agent composition to improve working stability and storage stability by using colloidal silica sol and silane. The preparation method of a transparent coating agent comprises the steps of mixing a silica sol, a silane, an alcohol and a catalyst with stirring to prepare a solution A; mixing a silane and a catalyst with stirring to prepare a solution B; and mixing the solution A and the solution B with stirring and maturing the mixture at a room temperature for a certain time. The transparent coating agent composition comprises 10-60 parts by weight of colloidal silica; 10-50 parts by weight of a first silane; 10-40 parts by weight of an alcohol; and 0.5-5 parts by weight of an acid, wherein the first silane is represented by RSi(OR')3; R is CH3, CH2CH3, CH2CH2CH3, CH2CH2CH2CH3, C6H5 or CH2CH2CH2CH2CH2CH2CH2CH3; and the acid is hydrofluoric acid, hydrochloric acid, sulfuric acid, nitric acid, formic acid, propionic acid or acetic acid.
    • 本发明提供透明涂层剂,透明涂层剂组合物,着色涂层剂的制备方法以及着色涂层剂组合物的制备方法,其通过使用胶体二氧化硅溶胶和硅烷来提高工作稳定性和储存稳定性。 透明涂布剂的制备方法包括以下步骤:在搅拌下混合硅溶胶,硅烷,醇和催化剂制备溶液A; 在搅拌下混合硅烷和催化剂以制备溶液B; 并在搅拌下混合溶液A和溶液B,并在室温下将混合物熟化一段时间。 该透明涂层剂组合物包含10-60重量份的胶体二氧化硅; 10-50重量份的第一硅烷; 10-40重量份的醇; 和0.5-5重量份的酸,其中第一硅烷由RSi(OR')3表示; R为CH 3,CH 2 CH 3,CH 2 CH 2 CH 3,CH 2 CH 2 CH 2 CH 3,C 6 H 5或CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 2 CH 3; 酸为氢氟酸,盐酸,硫酸,硝酸,甲酸,丙酸或乙酸。