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1. 发明授权

KR100355569B1 고순도 칼슘이 포함된 게르마늄용질액 제조방법 및 그용질액 失效
标题翻译：锗溶质液体产生包含高纯度钙和溶液的方法
公开(公告)号：KR100355569B1
公开(公告)日：2002-10-12
申请号：KR1019990055932
申请日：1999-12-08
申请人： 주식회사 지투케이
发明人： 백영숙
IPC分类号： C01G23/04 , B82B3/00 , B01J21/06
摘要： 본발명은화학원소기호Ge-32이며, 입자크기가약0.2㎛∼0.3㎛인순도 99.999%의이산화게르마늄(Germauim oxide)을엄선한다음이를각종공정을거쳐서고농축게르마늄(Germanium)의용질액을제조하고, 이와는별도로입자크기가약0.2㎛∼0.3㎛인순도 99%이상의고분말파우더타입으로된 칼슘을엄선한다음이또한각종공정을거쳐서고순도칼슘(Calsium)용질액을제조한다음상기각각제조된고농축게르마늄(Germanium)의용질액과고순도칼슘(Calsium)용질액을순수물과적정량섞어서고순도칼슘이포함된게르마늄용질액을제조하는것으로, 이와같이얻어진본 발명의얻어진고순도칼슘이포함된게르마늄용질액은각종의약품및 각종음료수, 식물성장용유기질비료, 세제류등에사용할수 있으며특히불치병으로알려진각종암세포를멸균시키는기능이매우탁월하며장시간복용해도인체에는전혀해가없고체질개선의 효과가있으며또한고엽제또는기타각종인체유독성분으로피부가손상이된 환자에게피부에발라주거나혹은묽게희석하여목욕을시키거나하는방법으로서치료효과를얻을수 있다. 그리고과음으로인한숙취에도탁월한효과가있다. 또한나이가들어가면서우리인간은칼슘의결핍현상이나타나게되는데본 발명품에칼슘이같이포함되어있어골다공증예방에도커다란효과가있는것이다.

2. 发明公开

KR1020010054936A 고순도 칼슘이 포함된 게르마늄용질액 제조방법 및 그용질액 失效
标题翻译：含有高纯度钙及其溶液的锗溶液的生产
公开(公告)号：KR1020010054936A
公开(公告)日：2001-07-02
申请号：KR1019990055932
申请日：1999-12-08
申请人： 주식회사 지투케이
发明人： 백영숙
IPC分类号： C01G23/04 , B82B3/00 , B01J21/06
CPC分类号： A61K33/06 , C01F11/00 , C01G17/02
摘要： PURPOSE: A process for preparing a high purity calcium-containing germanium solution by dissolving germanium oxide powder in pure water and adding a calcium solution to the obtained sol solution is provided. Therefore, the obtained titled compound can be used for various medicines, beverages, organic fertilizers for plant growth, detergents or the like. CONSTITUTION: Germanium having a particle size of about 0.2 to 0.3 micrometer and a purity of 99.999% is added to a mixture of 20% by weight of germanium oxide and 80% by weight of pure water in a high temperature vacuum mixer under nitrogen atmosphere and agitated at about 70deg.C at a speed of about 3,000 rpm for 30 min to give a highly concentrated germanium solution. Calcium powder having a particle size of about 0.2 to 0.3 micrometer and a purity of 99% or more is mixed with pure water in a ratio of 1:1 in a high speed mixer under nitrogen atmosphere and grinded at a speed of about 3,000 rpm or more for 48 hr to give a high purity calcium solution. The obtained germanium solution and calcium solution are mixed with water in a ratio of germanium/calcium/water of 20 to 50:50:10 at about 100deg.C or less to produce the subject solution.
摘要翻译：目的：提供通过将氧化锗粉末溶解在纯水中并向所得溶胶溶液中加入钙溶液来制备高纯度含钙锗溶液的方法。因此，所得标题化合物可用于各种药物，饮料，植物生长用有机肥料，洗涤剂等。构成：在氮气气氛下，在高温真空混合机中，将20〜20重量％的氧化锗和80重量％纯水的混合物加入粒径为0.2〜0.3微米，纯度为99.999％的锗，以约3,000rpm的速度在约70℃下搅拌30分钟，得到高度浓缩的锗溶液。将粒径为约0.2至0.3微米，纯度为99％或更高的钙粉在氮气氛下，在高速混合器中以1:1的比例与纯水混合并以约3,000rpm的速度研磨，或更多48小时，得到高纯度的钙溶液。将得到的锗溶液和钙溶液与水以比例的锗/钙/水为20〜50:50:10，以约100℃以下的比例混合，得到目标溶液。

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