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1. 发明公开

KR1020010016730A 중성자방사화 분석법을 이용한 표준용액의 제조방법 无效
标题翻译：使用中子活动分析制备标准溶液的方法
公开(公告)号：KR1020010016730A
公开(公告)日：2001-03-05
申请号：KR1019990031783
申请日：1999-08-03
申请人： 이계호 , 정래석
发明人： 이계호 , 정래석
IPC分类号： G01N23/00
CPC分类号： G01N23/025 , G01N2223/106 , G01N2223/652
摘要： PURPOSE: A standard solution preparing method is provided to enhance the reliability of a standard solution by metering the trace elements of a primer through the neutron active analysis. CONSTITUTION: In the neutron active analysis, an artificial radioactive nuclide is generated from a stable element for the qualitative and quantitative analysis. A radioactive nuclide is generated by irradiating a neutron beam causing nuclear reaction with an atomic nucleus to a sample. The radioactive nuclide is changed to a novel stable nucleus by passing through a decay process corresponding to the inherent half period of respective nuclides while emitting a gamma ray of a specific energy. The qualitative analysis is possible according to the detection of a half period through repeated measurement of the energy of the gamma rays. Therefore, the neutron active analysis is proper to the analysis of the trace elements of a primer. Further, an absolute quantization without need of a standard material is possible.
摘要翻译：目的：提供标准溶液制备方法，以通过中子活性分析计量底漆的微量元素来提高标准溶液的可靠性。构成：在中子活性分析中，人造放射性核素由稳定元素产生，用于定性和定量分析。通过照射产生与原子核的核反应的中子束对样品产生放射性核素。通过在发射比能量的γ射线的同时通过对应于各个核素的固有半周期的衰变过程，将放射性核素改变成新的稳定核。根据伽马射线能量的重复测量，可以根据半周期的检测进行定性分析。因此，中子活性分析适用于底漆微量元素的分析。此外，无需标准材料的绝对量化是可能的。

2. 发明授权

KR100357317B1 시료주입장치 및 시료분석방법 失效
标题翻译：样品注射系统和样品分析方法
公开(公告)号：KR100357317B1
公开(公告)日：2002-10-19
申请号：KR1020000000972
申请日：2000-01-10
申请人： 이계호
发明人： 이계호 , 정래석 , 신동근
IPC分类号： B05D1/02
摘要： 본 발명은 시료주입장치 및 시료분석방법에 관한 것으로써, 좀더 자세히는 시료용액 자체를 곧바로 가열하여 증기화시킴으로써 시료용액을 작은 물방울로 분사시킨 후 가열하는 종래의 시료주입장치보다 효율이 우수하고, 시료의 종류와 점도에 관계 없이 폭넓게 적용할 수 있는 새로운 시료주입장치 및 시료분석방법에 관한 것이다.

3. 发明公开

KR1020010029548A 시료주입장치 및 시료분석방법 失效
标题翻译：采样系统和分析方法
公开(公告)号：KR1020010029548A
公开(公告)日：2001-04-06
申请号：KR1020000000972
申请日：2000-01-10
申请人： 이계호
发明人： 이계호 , 정래석 , 신동근
IPC分类号： B05D1/02
摘要： PURPOSE: Provided are a sampling system and a method for analyzing samples. In particular, the system heats directly and evaporates a sample prior to nebulizing, and can be applied widely to various samples without regarding their kind or viscosity. CONSTITUTION: The sampling system is characterized in that: it has a microwave nebulizer to make the sample nebulized after evaporating the same, using microwave. The method for analyzing the sample is characterized by comprising the steps of: evaporating the sample; nebulizing the same; cooling a solvent included the nebulized sample to lower than the boiling point; discharging the cooled solvent; and transporting desolvated sample to the sample analyzer.
摘要翻译：目的：提供样品系统和分析样品的方法。特别地，系统在雾化之前直接加热并蒸发样品，并且可以广泛应用于各种样品而不考虑其种类或粘度。构成：采样系统的特征在于：它具有微波雾化器，使其在蒸发之后使用微波进行雾化。分析样品的方法的特征在于包括以下步骤：蒸发样品; 雾化相同; 冷却溶剂包括雾化样品低于沸点; 排出冷却的溶剂; 并将脱溶样品运送到样品分析仪。

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