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    • 2. 发明授权
    • 하프늄카르복실기를 함유한 굴절율이 향상된 아크릴계 UV 경화형 투명 점착제의 제조 및 방법
    • 使用丙烯酸羟基乙酯改善光学清漆丙烯酸压敏胶粘剂的折射率指标的方法
    • KR101379449B1
    • 2014-03-31
    • KR1020120123466
    • 2012-11-02
    • 서울대학교산학협력단
    • 김현중이승우박지원박초희
    • C09J133/04C09J4/02C09J7/00
    • C09J11/06C09J9/00C09J133/064
    • The present invention relates to a manufacturing method for an ultraviolet (UV) curing optically clear acrylic adhesive with an improved refractive index including a hafnium carboxyl group and, more specifically, to a manufacturing method for a UV curing optically clear acrylic adhesive with an improved refractive index including a hafnium carboxyl group that copolymerizes 2-ethylhexyl acrylate, 2-phenoxyethyl acrylate and acrylic acid, and hardens ingredients with UV by mixing the ingredients with hafnium carboxyl ethyl acrylate. The manufacturing method for a UV curing optically clear acrylic adhesive comprises: a step of copolymerizing 2-ethylhexyl acrylate, 2-phenoxyethyl acrylate and acrylic acid with ethyl acetate, which is a solvent, under a presence of catalysts; a step of manufacturing a mixture by mixing the copolymers with hafnium carboxyl ethyl acrylate; and a step of irradiating the mixture with UV. [Reference numerals] (AA) Weight reduction rate (%); (BB) Temperature (°C)
    • 本发明涉及一种具有改善的折射率(包括铪羧基)的紫外线(UV)固化的光学透明丙烯酸类粘合剂的制造方法,更具体地说,涉及具有改进的折射率的UV固化光学透明丙烯酸类粘合剂的制造方法 指标包括丙烯酸2-乙基己酯,丙烯酸2-苯氧基乙酯和丙烯酸共聚的铪羧基,并通过将成分与丙烯酸铪羧基乙酯混合,将具有UV的成分硬化。 UV固化光学透明丙烯酸类粘合剂的制造方法包括:在催化剂存在下,将丙烯酸2-乙基己酯,丙烯酸2-苯氧基乙酯和丙烯酸与作为溶剂的乙酸乙酯共聚的步骤; 通过将共聚物与丙烯酸铪羧基乙酯混合制备混合物的步骤; 以及用UV照射混合物的步骤。 (附图标记)(AA)重量减少率(%); (BB)温度(℃)