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1. 发明公开

KR1020130023149A 알킬렌 카보네이트 및/또는 알킬렌 글리콜 합성용 촉매의 재생 방법 및 알킬렌 카보네이트 및/또는 알킬렌 글리콜의 제조 방법 有权
标题翻译：用于生产碳酸亚烷基酯和/或烷基甘氨酸的催化剂的再生方法和碳酸亚烷基酯和/或烷基甘氨酸的制备方法
公开(公告)号：KR1020130023149A
公开(公告)日：2013-03-07
申请号：KR1020120092890
申请日：2012-08-24
申请人： 롯데케미칼 주식회사
发明人： 양홍주 , 이성훈 , 홍준택
IPC分类号： B01J38/54 , C07C67/62 , C07C29/94
CPC分类号： Y02P20/584 , B01J38/54 , B01J31/0268 , B01J31/40 , B01J38/02 , C07C29/00 , C07C67/00
摘要： PURPOSE: A method of reclaiming alkylene carbonate and/or a catalyst for synthesizing alkylene glycol and a method of manufacturing the alkylene carbonate and/or alkylene glycol are provided to remove ethylene glycol effectively in a short period of time so that a solution with a deactivated catalyst is effectively concentrated. CONSTITUTION: A method of reclaiming alkylene carbonate and/or a catalyst for synthesizing alkylene glycol comprises the following steps: C2-C6 alkylene oxide and carbon dioxide are reacted with more than one catalyst among a quaternary phosphonium iodine compound and a quaternary phosphonium bromine compound. The produced compounds are concentrated by a system for evaporating a thin film. The concentrated products react with more than one type of halogenated salt compounds selected from iodinized salt and bromide salt. The step of using the system for evaporating thin film is carried out under a pressure of 10^-3 torr to 100 torr.
摘要翻译：目的：提供回收碳酸亚烃酯和/或用于合成亚烷基二醇的催化剂的方法和制备碳酸亚烷基酯和/或亚烷基二醇的方法，以在短时间内有效地除去乙二醇，使得具有失活的溶液催化剂有效集中。构成：回收碳酸亚烃酯和/或用于合成亚烷基二醇的催化剂的方法包括以下步骤：在季鏻碘化合物和季鏻溴化合物中使C2-C6环氧烷和二氧化碳与多于一种的催化剂反应。通过用于蒸发薄膜的系统浓缩所产生的化合物。浓缩产物与选自碘化盐和溴化物盐的多种类型的卤化盐化合物反应。使用蒸发薄膜的系统的步骤在10 -3 -3乇至100乇的压力下进行。

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