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71. 发明公开

KR1020090035665A 폴리올레핀 반응기에서 정전기 전하를 제어하기 위한 방법 및 장치 无效
标题翻译：用于控制聚烯烃反应器静电荷的方法和装置
公开(公告)号：KR1020090035665A
公开(公告)日：2009-04-10
申请号：KR1020087031877
申请日：2007-07-13
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 마켈,에릭,제이. , 하거티,로버트,오. , 후세인,데이비드,에프. , 뮬,마이클,이. , 판넬,리차드,비.
IPC分类号： H05F3/00 , C08F2/00 , C08F10/00 , C08F2/34
CPC分类号： B01J8/1809 , B01J19/002 , B01J2208/00734 , B01J2219/002 , B01J2219/00213 , B01J2219/00231 , B01J2219/00254 , C08F4/65912 , C08F4/65925 , C08F10/00 , C08F2400/02 , C08F2410/02 , Y10S526/901 , C08F2/005 , C08F2/34
摘要： A method for controlling sheeting in a gas phase reactor that includes producing a polyolefin with at least one metallocene catalyst and at least one static control agent in at least one gas phase reactor, measuring entrainment static using a static probe, and adjusting the concentration of the static control agent in response to changes in the measured entrainment static is disclosed.
摘要翻译：一种用于控制气相反应器中的片材的方法，其包括在至少一个气相反应器中使用至少一种金属茂催化剂和至少一种静电控制剂生产聚烯烃，使用静态探针测量夹带静电，并调节公开了响应于测量的夹带静态变化的静电控制剂。

72. 发明公开

KR1020080049728A 개선된 입도 분포를 갖는 지지체 물질을 포함하는 촉매조성물 无效
标题翻译：包含改进的粒度分布的支持材料的催化剂组合物
公开(公告)号：KR1020080049728A
公开(公告)日：2008-06-04
申请号：KR1020087005124
申请日：2006-08-10
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 쿠오,치-아이 , 곽,태,훈 , 리,동밍 , 새넌,포터,씨.
IPC分类号： C08F4/64 , C08F4/646 , C08F10/00 , C08F210/16
CPC分类号： C08F210/16 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08J5/18 , C08J2323/04 , C08F4/6546 , C08F4/65904 , C08F210/14 , C08F2500/17 , C08F2500/12 , C08F2500/05 , C08F2500/24
摘要： A catalyst composition that includes a support material having an improved particle-size distribution is provided. Processes for producing polyolefin composition also are provided. Polymers and films also are provided. An example of a catalyst composition is a supported multi-transition-metal catalyst composition that includes: (a) at least two catalyst components selected from the group consisting of: a nonmetallocene catalyst component and a metallocene catalyst component; (b) a support material that has a D50 of less than about 30 microns and a particle size distribution having a D90/D10 ratio of less than about 6; and (c) an activator.
摘要翻译：提供了包括具有改善的粒度分布的载体材料的催化剂组合物。还提供了生产聚烯烃组合物的方法。还提供聚合物和薄膜。催化剂组合物的实例是负载型多过渡金属催化剂组合物，其包括：（a）至少两种选自非茂金属催化剂组分和茂金属催化剂组分的催化剂组分; （b）具有小于约30微米的D50和D90 / D10比小于约6的粒度分布的载体材料; 和（c）活化剂。

73. 发明公开

KR1020080031977A 폴리에틸렌 수지의 블로우 성형 有权
标题翻译：吹塑聚乙烯树脂
公开(公告)号：KR1020080031977A
公开(公告)日：2008-04-11
申请号：KR1020087004584
申请日：2006-07-21
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 캔,케빈,제이. , 에이싱거,로날드,에스. , 구드,마크,지. , 무어하우스,존,에이치. , 무레,클리프,알. , 재커,스티븐,피. , 아페세츠,마리아,에이.
IPC分类号： C08F10/02 , C08F2/34 , C08F210/02 , C08F4/24
CPC分类号： C08F210/16 , C08F2/34 , C08F4/24 , C08F210/08 , C08F2500/14 , C08F2500/13 , C08F2500/12 , C08F2500/04 , C08F210/14
摘要： Disclosed herein are various processes, including continuous fluidized-bed gas-phase polymerization processes for making a high strength, high density polyethylene copolymer, comprising (including): contacting monomers that include ethylene and optionally at least one non-ethylene monomer with fluidized catalyst particles in a gas phase in the presence of hydrogen gas at an ethylene partial pressure of 100 psi or more and a polymerization temperature of 120°C or less to produce a polyethylene copolymer having a density of 0.945 g/cc or more and an ESCR Index of 1.0 or more wherein the catalyst particles are prepared at an activation temperature of 700°C or less, and include silica, chromium, and titanium.
摘要翻译：本文公开了各种方法，包括用于制备高强度，高密度聚乙烯共聚物的连续流化床气相聚合方法，包括（包括）：使包含乙烯和任选的至少一种非乙烯单体的单体与流化催化剂颗粒接触在气相中，在乙烯分压为100psi以上，聚合温度为120℃以下的氢气存在下，制备密度为0.945g / cc以上的聚乙烯共聚物，ESCR指数为 1.0以上，其中催化剂颗粒在700℃或更低的活化温度下制备，并且包括二氧化硅，铬和钛。

74. 发明公开

KR1020080020683A 저밀도, 중밀도 및 고밀도 폴리에틸렌용 단일 촉매 有权
标题翻译：单一催化剂低，中高密度聚乙烯
公开(公告)号：KR1020080020683A
公开(公告)日：2008-03-05
申请号：KR1020087000877
申请日：2006-05-15
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 콜브,레이너 , 스줄,존,에프.
IPC分类号： C08F10/02 , C08F4/72 , C08F2/34 , C08F2/00
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08F210/16 , Y10S526/901 , Y10S526/905 , C08F2/34 , C08F210/14 , C08F2500/12 , C08F2500/24
摘要： A method of polymerizing olefins comprising combining in one embodiment ethylene and optionally one or more alpha-olefins with a catalyst composition in a continuous polymerization reactor at a pressure of less than 10,000 kPa; wherein the catalyst composition comprises a hafnocene; and isolating a polyethylene having a density in the range of from 0.930 to 0. 975 g/cm. Also provided is a method of transitioning a continuous polymerization reactor from production of a low density polyethylene to a medium or high density polyethylene. Also provided is a medium to high density polyethylene suitable for injection or rotomolding applications. Also provided is a single catalyst composition suitable for such needs. ® KIPO & WIPO 2008
摘要翻译：一种聚合烯烃的方法，包括在一个实施方案中，在连续聚合反应器中，在小于10,000kPa的压力下，将一种或多种α-烯烃和任选的一种或多种α-烯烃与催化剂组合物结合; 其中所述催化剂组合物包含茂金属; 并分离密度在0.930至0.975g / cm 3范围内的聚乙烯。还提供了将连续聚合反应器从生产低密度聚乙烯转变为中等或高密度聚乙烯的方法。还提供适用于注射或滚塑应用的中高密度聚乙烯。还提供了适合于这种需要的单一催化剂组合物。 ®KIPO＆WIPO 2008

75. 发明公开

KR1020070118194A 선행 지표를 이용한 중합반응 모니터링 및 조절 失效
标题翻译：使用引导指标的聚合监测和控制
公开(公告)号：KR1020070118194A
公开(公告)日：2007-12-13
申请号：KR1020077026760
申请日：2002-10-15
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 슐츠키케네스지 , 산타나로버트엘 , 에르만프레드디 , 쉬로드카프라디프피
IPC分类号： C08F2/34 , C08F2/01 , C08F210/00 , C08F210/02
CPC分类号： C08F10/02 , C08F4/65904 , C08F4/65916 , C08F210/16 , C08F2400/02 , C08F2/00 , C08F2/34 , C08F210/14 , C08F2500/12
摘要： Methods of monitoring and controlling polymerization reactions are disclosed. The ratio of concentrations of two reactor components are determined in a gas stream of a reactor to obtain a leading indicator function L. The value of L or a function of L, such as rescaled value or a reciprocal, is compared to a target value, and at least one reactor parameter is adjusted in response to a deviation between L or the function of L and the target value. Monitoring of the leading indicator permits rapid diagnosis of reactor problems, and rapid adjustments of reactor parameters, compared to laboratory analysis of samples of polymer properties.
摘要翻译：公开了监测和控制聚合反应的方法。在反应器的气流中确定两个反应器组分的浓度比，以获得前导指示函数L.将L或L的函数（例如重新缩放值或倒数）的值与目标值进行比较，并且响应于L或L的函数与目标值之间的偏差来调整至少一个电抗器参数。与聚合物性质样品的实验室分析相比，主要指标的监测可以快速诊断反应堆问题，并快速调整反应器参数。

76. 发明公开

KR1020070093066A 지글러-나타계 촉매와 크롬계 촉매간의 전이 방법 无效
标题翻译：基于沸石和基于铬的催化剂之间的转移过程
公开(公告)号：KR1020070093066A
公开(公告)日：2007-09-17
申请号：KR1020077013971
申请日：2005-12-21
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 구드,마크,지. , 칸,케빈,제이. , 후세인,데이비드,에프. , 산타나,로버트,엘. , 슈츠,데이비드,씨. , 아가피오우,아가피오스,케이.
IPC分类号： C08F2/34 , C08F2/42 , C08F10/00
CPC分类号： C08F10/02 , C08F210/16 , C08F2410/05 , Y10S526/901 , C08F2/34 , C08F2/42 , C08F210/14 , C08F2500/12 , C08F2500/07 , C08F2500/18 , C08F210/08
摘要： Embodiments of our invention relate to processes for transitioning among polymerization catalyst systems including processes for transitioning among olefin polymerization reactions using Ziegler-Natta catalysts systems and chromium-based catalyst systems. Among embodiments contemplated are a method of transitioning from a first catalyst to a second catalyst in an olefin polymerization reactor, comprising: adding to the reactor a deactivating agent (DA) selected from one of carbon monoxide, carbon dioxide, or combinations thereof; adding to the reactor a cocatalyst adsorbing agent (CAA), comprising an inorganic oxide selected from one of silica, alumina or combinations thereof; wherein the first catalyst comprises at least one conventional Ziegler-Natta catalyst, and a cocatalyst, wherein the second catalyst comprises at least one chromium-based catalyst, wherein the reactor is a gas-phase, fluidized bed reactor, and wherein the CAA is substantially free of transition metals. In another embodiment a method of transitioning from a first catalyst to a second catalyst in an olefin polymerization reactor is contemplated, comprising: adding a transition aid agent (TAA) wherein the TAA is selected from one of alkoxylated amines, alkoxylated amides, or combinations thereof, wherein the first catalyst comprises at least one Ziegler-Natta catalyst comprising the catalyst, a cocatalyst and optionally a support, and the second catalyst comprises at least one chromium-based catalyst.
摘要翻译：本发明的实施方案涉及在聚合催化剂体系中过渡的方法，包括使用齐格勒 - 纳塔催化剂体系和铬基催化剂体系在烯烃聚合反应中过渡的方法。考虑的实施方案是在烯烃聚合反应器中从第一催化剂转变为第二催化剂的方法，包括：向反应器中加入选自一氧化碳，二氧化碳或其组合中的一种失活剂（DA）; 向所述反应器中加入选自二氧化硅，氧化铝或其组合的无机氧化物的助催化剂吸附剂（CAA）; 其中所述第一催化剂包含至少一种常规齐格勒 - 纳塔催化剂和助催化剂，其中所述第二催化剂包含至少一种铬基催化剂，其中所述反应器是气相流化床反应器，并且其中所述CAA基本上没有过渡金属。在另一个实施方案中考虑了在烯烃聚合反应器中从第一催化剂转变为第二催化剂的方法，包括：加入转移助剂（TAA），其中TAA选自烷氧基化胺，烷氧基化酰胺或其组合之一，其中所述第一催化剂包含至少一种齐格勒 - 纳塔催化剂，所述催化剂包含所述催化剂，助催化剂和任选的载体，所述第二催化剂包含至少一种铬基催化剂。

77. 发明公开

KR1020060135660A 하프노센 촉매화 폴리에틸렌으로부터의 고인열 필름 有权
标题翻译：来自氢化丙烯酰胺的高分子膜
公开(公告)号：KR1020060135660A
公开(公告)日：2006-12-29
申请号：KR1020067011692
申请日：2004-04-13
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 스줄,존,에프. , 파레이,제임스,맥레오드 , 맥큘로그,러플린,쥐. , 임펄만,라이언,윈스톤
IPC分类号： B32B27/28
CPC分类号： C08F10/00 , B29C47/0021 , B29C47/0026 , B29C47/8845 , B29C47/92 , B29C2947/92514 , B29C2947/92704 , B29C2947/92895 , B29C2947/92904 , C08F4/65912 , C08F4/65916 , C08F210/16 , C08J5/18 , C08J2323/08 , Y10T428/31938 , C08F4/65925 , C08F210/14 , C08F2500/12 , C08F2500/03 , C08F2500/06 , C08F2500/11 , C08F2500/26
摘要： A polyethylene film having a balance of improved physical and mechanical properties and a method for making the same are provided. In one aspect, the film includes a 1% secant modulus of greater than 25,000 psi, a dart impact resistance'of greater than 500 g/mil, and a MD tear strength of greater than 500 g/mil. In one aspect, the method comprises reacting ethylene derived units and a comonomer in the presence of a hafnium-based metallocene at a temperature of from 70°C and 90°C, an ethylene partial pressure of from 120 psia and 260 psia, and a comonomer to ethylene ratio of from 0.01 to 0.02 to produce an ethylene based polymer. The method further comprises extruding the ethylene based polymer at conditions sufficient to produce a polyethylene film comprising a secant modulus of greater than 25,000 psi, a dart impact resistance of greater than 500 g/mil, and a MD tear strength of greater than 500 g/mil.
摘要翻译：提供了具有改善的物理和机械性质的平衡的聚乙烯膜及其制备方法。在一个方面，该膜包括大于25,000psi的1％割线模量，大于500g / mil的落镖抗冲击强度和大于500g / mil的MD撕裂强度。在一个方面，该方法包括在铪基茂金属存在下，在70℃和90℃的温度，120psia和260psia的乙烯分压下使乙烯衍生的单元和共聚单体反应，共聚单体与乙烯的比例为0.01至0.02，以生产乙烯基聚合物。该方法还包括在足以产生包含大于25,000psi的正割模数，大于500g / mil的落镖冲击强度和大于500g / mil的MD撕裂强度的聚乙烯膜的条件下挤出基于乙烯的聚合物，密耳。

78. 发明公开

KR1020060135640A 흐림도가 낮고 강도가 높은 폴리에틸렌 조성물 无效
标题翻译：低密度高强度聚乙烯组合物
公开(公告)号：KR1020060135640A
公开(公告)日：2006-12-29
申请号：KR1020067010584
申请日：2004-09-20
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 류,칭-타이 , 퀄크,태,훈
IPC分类号： C08L23/06
CPC分类号： C08L23/0815 , C08L23/06 , C08L2205/02 , C08L2205/025 , C08L2666/06
摘要： A low density substantially linear polyethylene composition is described, including some that have: (a) a density of 0.935 g/cc or less; (b) a Haze of 10% or less, (c) a Dart Impact of 100 grams/mil or more, (d) an average overall long chain branching index of 0.95 or more; and (e) a slice long chain branching (SLCB) index of 0.85 or less for any portion of the composition having a molecular weight of 100,000 or above.
摘要翻译：描述了低密度基本线性的聚乙烯组合物，包括一些具有以下成分：（a）密度为0.935g / cc或更低; （b）10％以下的雾度，（c）100克/密耳以上的镖撞击，（d）平均总长链支化指数为0.95以上; 和（e）对于分子量为100,000或更高的组合物的任何部分，切片长链支化（SLCB）指数为0.85或更小。

79. 发明授权

KR100566855B1 기체 상 중합 방법 失效
标题翻译：气相聚合法
公开(公告)号：KR100566855B1
公开(公告)日：2006-04-03
申请号：KR1020057003703
申请日：2003-08-12
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 이어만,프레드,디. , 뮬,마이클,이. , 시로드카르,프라디프,피. , 트랩프,케이트,더블유.
IPC分类号： C08F2/34
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08F210/16 , Y10S526/901 , Y10S526/905 , C08F4/65904 , C08F2/34 , C08F210/14 , C08F2500/07 , C08F2500/12 , C08F2500/18
摘要： 수소 기체 및 에틸렌 단량체를 포함하여 1종 이상의 단량체를 함유하는 기류를 유동 베드를 포함하는 반응기로 반응 조건 하, 메탈로센을 포함하는 촉매의 존재 하에 통과시켜 폴리올레핀 조성물을 수득하는, 폴리올레핀 조성물의 제조를 위한 기체 상 중합 방법이 개시되며, 하나의 구현예에서 상기 유동화된 벌크 밀도는 고정된 벌크 밀도의 60% 이상(또는 40% 미만의 공극률)이고; 상기 공극률은 특정 구현예에서 (a) 반응기 온도를 100℃ 이하로 유지하는 것; (b) 반응기 내로 도입되는 수소 기체 대 에틸렌의 몰 비가 0.015 이하인 것을 포함하는 다수의 요인에 의해 제어된다.
폴리올레핀, 에틸렌, 메탈로센, 유동 베드, 벌크 밀도, 공극률

80. 发明授权

KR100543842B1 중합 방법 有权
标题翻译：聚合工艺
公开(公告)号：KR100543842B1
公开(公告)日：2006-01-23
申请号：KR1020037007413
申请日：2001-11-27
申请人： 유니베이션 테크놀로지즈, 엘엘씨
发明人： 마우손,시몬 , 카오,선-체 , 크월크,태,훈 , 린,티모시,로저 , 맥컨빌르데이비드,에이치. , 맥케,매튜,게리 , 스줄,존,프랑시즈 , 테리,커스턴,앤 , 웬젤,티모시,티. , 구드,마크,그레고리 , 오스캄,존,헨리 , 조진센,로버트,제이. , 보겔,로버트,해롤드
IPC分类号： C08F10/00
CPC分类号： C08F10/00 , C08F4/659 , C08F4/65912 , C08F4/65925 , C08F210/16 , Y10S526/903 , Y10S526/907 , Y10S526/943 , C08F4/65916 , C08F4/65904 , C08F2/00 , C08F210/14 , C08F2500/12 , C08F2500/24 , C08F2500/18 , C08F2500/26
摘要： The invention provides for polymerization catalyst compositions, and for methods for introducing the catalyst compositions into a polymerization reactor. More particularly, the method combines a catalyst component containing slurry and a catalyst component containing solution to form the completed catalyst composition for introduction into the polymerization reactor. The invention is also directed to methods of preparing the catalyst component slurry, the catalyst component solution and the catalyst compositions, to methods of controlling the properties of polymer products utilizing the catalyst compositions, and to polymers produced therefrom.

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