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    • 22. 发明公开
    • 아세틸렌 전환공정을 이용한 C4 유분으로부터1,3-부타디엔을 분리하는 방법
    • 用乙炔转化器从C4原料中分离1,3-丁二烯的方法
    • KR1020100009009A
    • 2010-01-27
    • KR1020080069677
    • 2008-07-17
    • 에스케이이노베이션 주식회사
    • 이희두오경종고민수박민규이성준임윤재오승훈김태진김용승박덕수김홍찬
    • C10G45/32C10G65/12C07C11/167
    • C10G67/04C07C7/08C07C11/107C10G21/00C10G21/28C10G45/32C10G2300/44C10G2400/20C07C11/167
    • PURPOSE: A method of separating 1,3-butadiene from C4 fraction using an acetylene conversion process is provided to reduce the time that foreign materials are generated. CONSTITUTION: A method of separating 1,3-butadiene from C4 fraction using an acetylene conversion process is as follows: A C4 fraction is supplied to a multi-stage hydrogenation reactor. The content of acetylenes is reduced under 70 wtppm by selectively converting acetylenes through a liquid-phase hydrogenation reaction. The fraction from the multi-stage hydrogenation reactor and an extractive solvent is supplied to an extractive distillation tower. A gas-phase fraction of the top of a pre-treatment separator is supplied to a solvent recovery tower, and a liquid-phase fraction of the bottom of the pre-treatment separator is supplied to a solvent stripping tower by applying a bottom fraction of the extractive distillation tower to the pre-treatment separator. The fraction from the solvent stripping tower, the fraction of butadiene and acetylenes, and the fraction of the pre-treatment separator are supplied to the solvent recovery tower. The overhead fraction of the solvent recovery tower is applied to a refining tower, and then, high purity 1.3- butadiene is obtained.
    • 目的:提供使用乙炔转化法从C4馏分中分离1,3-丁二烯的方法,以减少产生异物的时间。 构成:使用乙炔转化法从C4馏分中分离1,3-丁二烯的方法如下:将C4级分提供给多级氢化反应器。 通过液相氢化反应选择性地转化乙炔,乙炔的含量降低到70wtppm以下。 来自多级氢化反应器的馏分和萃取溶剂被供应到萃取蒸馏塔。 将预处理分离器的顶部的气相分数供给到溶剂回收塔,并且将预处理分离器的底部的液相部分通过施加底部馏分供给到溶剂汽提塔 萃取蒸馏塔到预处理分离器。 来自溶剂汽提塔的馏分,丁二烯和乙炔的馏分以及预处理分离器的馏分被供给到溶剂回收塔。 将溶剂回收塔的塔顶馏分应用于精制塔,然后得到高纯度的1,3-丁二烯。
    • 26. 发明公开
    • 유동층 접촉 분해 유분으로부터 청정 석유제품 및 방향족제품을 제조하는 방법
    • 从油气混合物制备清洁燃料和芳烃的方法催化裂化在流化床上
    • KR1020090020776A
    • 2009-02-27
    • KR1020070085346
    • 2007-08-24
    • 에스케이이노베이션 주식회사
    • 김철중유재욱성경학장병무임병수이종형노경석이혁재박삼룡최선오승훈김용승김경록
    • C10G35/14C10G45/68
    • C10G45/68C10G35/14C10G2300/202C10G2400/04C10G2400/06C10G2400/30
    • A method for preparing LPG, low sulfur gasoline and aromatic product from the hydrocarbon mixture catalytic fluid cracked on the fluid bed is provided to improve the efficiency of the cracking on the fluid bed. A method for preparing LPG, low sulfur gasoline and aromatic product from the hydrocarbon mixture catalytic fluid cracked on the fluid bed comprises the steps of (U1) distilling the hydrocarbon mixture catalytic fluid cracked on the fluid bed to separate into the distillate and the residue; (U2) reacting the distillate by hydrogenation desulfurization/denitration to remove a sulfur compound and nitrogen compound contained in the distillate; (U3) converting the aromatic hydrocarbon compound of the distillate into an aromatic hydrocarbon compound rich in xylene, benzene and toluene by dealkylation, and converting the nonaromatic hydrocarbon compound into the nonaromatic hydrocarbon compound rich in LPG by hydrocracking process; separating fuel gas, LPG and aromatic products; and reacting the residue by desulfurization/denitration toobtain low sulfur gasoline.
    • 提供了一种从烃混合物制备液化石油气,低硫汽油和芳香族产物在液床上裂解的催化流体的方法,以提高流化床上开裂的效率。 从烃混合物制备LPG,低硫汽油和芳香族产物的方法,在流化床上裂解催化流体包括以下步骤:(U1)蒸馏在流化床上裂解的烃混合物催化流体,分离成馏出物和残余物; (U2)通过氢化脱硫/脱硝反应馏出物以除​​去馏出物中所含的硫化合物和氮化合物; (U3)通过脱烷基转化将馏出物的芳烃化合物转化为富二甲苯,苯和甲苯的芳烃化合物,并通过加氢裂化法将非芳族烃化合物转化成富含LPG的非芳族烃化合物; 分离燃气,液化石油气和芳香族产品; 并通过脱硫/脱硝反应残留物以获得低硫汽油。
    • 28. 发明授权
    • 아연 페라이트 촉매, 이의 제조방법 및 이를 이용한1,3-부타디엔의 제조방법
    • 锌铁素体催化剂及其制备方法及其制备1,3-丁二烯的方法
    • KR100847206B1
    • 2008-07-17
    • KR1020070045499
    • 2007-05-10
    • 에스케이이노베이션 주식회사
    • 정영민이성준김태진오승훈김용승송인규김희수정지철이호원
    • B01J23/80B01J23/74B01J23/06C07C5/333
    • B01J23/80B01J23/002B01J35/002B01J37/031B01J2523/00C07C5/3332C07C2523/80C07C11/167B01J2523/27B01J2523/842
    • A preparation method is provided to prepare a zinc ferrite catalyst of which components are simple, and which is synthesized easily and advantageous in securing of reproducibility as a catalyst for producing 1,3-butadiene, and a method of producing 1,3-butadiene by performing an oxidative dehydrogenation on the zinc ferrite catalyst by directly using a C4 mixture as a reactant without performing an additional separation process is provided. A method of preparing a zinc ferrite catalyst for the production of 1,3-butadiene comprises the steps of: (a) dissolving a zinc precursor and an iron precursor into distilled water; (b) adjusting a pH range of a coprecipitation solution to 6 to 10 while mixing a basic solution with a mole concentration of 1.5 to 4.0 with the aqueous precursor solution; (c) filtering the pH-adjusted mixed solution to obtain a solid catalyst; (d) drying the solid catalyst at 70 to 200 deg.C; and (e) heat-treating the dried catalyst at 350 to 800 deg.C. A method of producing 1,3-butadiene comprises the steps of: (a) providing a mixed gas of a C4 mixture, air, and steam as a reactant; (b) performing an oxidative dehydrogenation by continuously passing the reactant through a catalyst layer to which the zinc ferrite catalyst for the production of 1,3-butadiene is fixed; and (c) obtaining 1,3-butadiene. Further, an atomic ratio of Fe/Zn of the zinc precursor and the iron precursor is 1.5 to 2.5, and the basic solution is sodium hydroxide.
    • 提供一种制备方法,其制备成分简单的锌铁氧体催化剂,其易于且有利于确保作为生产1,3-丁二烯的催化剂的再现性,以及通过以下方法制备1,3-丁二烯: 提供了通过直接使用C4混合物作为反应物而在铁酸锌催化剂上进行氧化脱氢而不进行额外的分离工艺。 制备1,3-丁二烯的铁酸锌催化剂的制备方法包括以下步骤:(a)将锌前体和铁前体溶解在蒸馏水中; (b)将共沉淀溶液的pH范围调节至6至10,同时用前驱体溶液混合摩尔浓度为1.5至4.0的碱性溶液; (c)过滤pH调节的混合溶液以获得固体催化剂; (d)在70〜200℃干燥固体催化剂; 和(e)在350至800℃下热处理干燥的催化剂。 制备1,3-丁二烯的方法包括以下步骤:(a)提供C4混合物,空气和蒸汽的混合气体作为反应物; (b)通过使反应物连续通过固定用于生产1,3-丁二烯的铁酸锌催化剂的催化剂层进行氧化脱氢; 和(c)获得1,3-丁二烯。 此外,锌前体和铁前体的Fe / Zn的原子比为1.5〜2.5,碱性溶液为氢氧化钠。