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1. 发明专利

JP2014237630A 有機ホウ素化合物の製造方法有权
标题翻译：有机硼化合物的生产方法
公开(公告)号：JP2014237630A
公开(公告)日：2014-12-18
申请号：JP2014095207
申请日：2014-05-02
申请人：和光純薬工業株式会社 , Wako Pure Chem Ind Ltd , 国立大学法人北海道大学 , Hokkaido Univ
发明人： ITO HAJIME , YAMAMOTO EIJI
IPC分类号： C07F5/04
摘要：【課題】重金属を用いない、適用基質の範囲が広いアリールボロン酸エステルの製造方法の提供。【解決手段】一般式R−Xで示される有機ハロゲン化合物(XはBr又はI;RはC1〜20のアルキル基、C6〜14のアリール基、或いは、N、O及びSから選ばれる異性原子を1〜3個含む複素環基等)と、一般式(VI)で示される化合物とを、ナトリウムアルコキシド又はカリウムアルコキシドの存在下で反応させ、置換Si部分と前記R部分を置換し、アリールボロン酸エステルを得る。(3個のR3は各々独立して、C1〜6のアルキル基又はC6〜10のアリール基;4個のR4は各々独立して、C1〜3のアルキル基)【選択図】なし
摘要翻译：要解决的问题：提供一种不含重金属的具有广泛应用底物的芳基硼酸酯的制备方法。溶液：由通式RX表示的有机卤素化合物（其中X为Br或I; R 是C 1〜20烷基，C 6〜14芳基，含有1〜3个选自N，O和S的杂原子的杂环基等）和通式（VI）表示的化合物在存在烷氧基化钠或醇钾以代替取代的Si部分和R部分以获得芳基硼酸酯。（式中，3个Rare各自独立地为C1〜6的烷基或C6〜10的芳基; 4个独立地为C1〜3的烷基）。

2. 发明专利

JP2014078484A Nonaqueous secondary battery, and flame retardant and additive for nonaqueous secondary battery 有权
标题翻译：非等级二次电池非阻燃二次电池及阻燃剂及其添加剂
公开(公告)号：JP2014078484A
公开(公告)日：2014-05-01
申请号：JP2013077816
申请日：2013-04-03
申请人： Sharp Corp , シャープ株式会社 , Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： UCHIUMI HISAYUKI , MITACHI TAKEHITO , NISHIMURA NAOTO , KIYOSU TAKAHIRO , OKAMOTO NORIAKI , WATABIKI TSUTOMU
IPC分类号： H01M10/0567 , H01M10/0569
CPC分类号： H01M10/0567 , H01M10/052 , H01M10/0569 , H01M10/4235 , H01M2300/0025 , H01M2300/0028
摘要： PROBLEM TO BE SOLVED: To improve flame retardancy and battery characteristics of a nonaqueous secondary battery.SOLUTION: This nonaqueous secondary battery includes a positive electrode, a negative electrode, and a nonaqueous electrolyte. The nonaqueous electrolyte contains at least an annular nitrogen containing compound expressed by the following general formula (1)(in the formula, Ris selected from a halogen atom, a low-grade alkyl group, a low-grade alkenyl group, a low-grade alkoxy group, a low-grade alkoxycarbonyl group, a low-grade alkyl carbonyl group, and an aryl group, Ris selected from a hydrogen atom, a halogen atom, a low-grade alkyl group, a low-grade alkenyl group, a low-grade alkoxy group, a low-grade alkoxycarbonyl group, a low-grade alkyl carbonyl group, and an aryl group, or Rand Rare mutually combined and selected from a ring structure containing either one of a methylene group, a vinylene group, and a divalent linking group containing a complex atom.).
摘要翻译：要解决的问题：提高非水二次电池的阻燃性和电池特性。解决方案：该非水二次电池包括正电极，负电极和非水电解质。所述非水电解质至少含有由以下通式（1）表示的环状含氮化合物（式中，R 1选自卤素原子，低级烷基，低级烯基，低级烷氧基，低级烷氧基羰基，低级烷基羰基和芳基，选自氢原子，卤素原子，低级烷基，低级烯基，低级烷基低级烷氧基羰基，低级烷基羰基和芳基，或兰德尔稀土相互组合并选自含有亚甲基，亚乙烯基和含有复合原子的二价连接基团）。

3. 发明专利

JP2014031351A Method for producing 2,3,6,7,10,11-hexahydroxytriphenylenes 有权
标题翻译：用于生产2,3,6,7,10,11-十六烷基羟基苯乙烯的方法
公开(公告)号：JP2014031351A
公开(公告)日：2014-02-20
申请号：JP2012174480
申请日：2012-08-06
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社 , Ritsumeikan , 学校法人立命館
发明人： MORIMOTO KOJI , DOI TOSHIFUMI , KITA YASUYUKI
IPC分类号： C07C37/11 , C07B61/00 , C07C39/12
摘要： PROBLEM TO BE SOLVED: To provide a practical method for producing hexahydroxytriphenylenes by simple operations in excellent yield, while taking into consideration an environmental load reduction.SOLUTION: A method for producing 2,3,6,7,10,11-hexahydroxytriphenylenes expressed by a general formula (1) includes: a first step of reacting catechol expressed by a general formula (2) in presence of a hypervalent iodine reagent; and a second step of treating a reaction liquid of the first step with a reducing agent. (In the formulae, R independently represents a hydrogen atom, a halogen atom, an alkyl group having 1-3 carbon atoms or an alkoxy group having 1-3 carbon atoms.)
摘要翻译：要解决的问题：考虑到环境负荷的降低，提供通过简单的操作简便地制备六羟基三苯基的实用方法。解决方案：一种制备2,3,6,7,10,11-六羟基三苯基的方法，由通式（1）包括：使通式（2）表示的儿茶酚在高价碘试剂存在下反应的第一步骤; 以及用还原剂处理第一步骤的反应液的第二步骤。（式中，R独立地表示氢原子，卤原子，碳原子数1〜3的烷基或碳原子数1〜3的烷氧基）。

4. 发明专利

JP2013236027A Etchant, and method for manufacturing silicon-based substrate using the same 审中-公开
标题翻译：蚀刻剂和使用其制造基于硅的基板的方法
公开(公告)号：JP2013236027A
公开(公告)日：2013-11-21
申请号：JP2012108968
申请日：2012-05-11
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： OUCHI NAOKO , KAKIZAWA MASAHIKO , TSURUMOTO HIROYUKI , WATANABE TERUMI , KAWAHARA SHINJI
IPC分类号： H01L21/308 , H01L21/306 , H01L31/04
CPC分类号： Y02E10/546
摘要： PROBLEM TO BE SOLVED: To provide: an alkali etchant for solar battery manufacturing which allows a fine uneven structure to be formed uniformly on an entire surface of a wafer including silicon as a primary component, and which is applicable to various wafers; and a method for manufacturing a silicon-based substrate for solar battery manufacturing by use of the etchant.SOLUTION: The alkali etchant for solar battery manufacturing comprises (A) a monosulfonic acid given by the general formula [1] or a salt thereof, (B) an alkali compound, and (C) water. The method for manufacturing a silicon-based substrate for solar battery manufacturing comprises: etching a wafer including silicon as its primary component by use of the etchant, thereby forming an uneven structure on a surface of the wafer. In the general formula 1, Rand Rindependently represent a hydrogen atom or an alkyl group having 1C-5C (C is a symbol of carbon), M represents a hydrogen atom, an alkali metal atom, an ammonium (NH) group, or a tetraalkylammonium (RN) group, where Ris an alkyl group having 1C-4C, and n represents an integer of 1-5.
摘要翻译：要解决的问题：提供：一种用于太阳能电池制造的碱性蚀刻剂，其允许在包括硅作为主要成分的晶片的整个表面上均匀地形成微细的不均匀结构，并且可应用于各种晶片; 以及通过使用蚀刻剂制造太阳能电池制造用硅基基板的方法。解决方案：太阳能电池制造用碱蚀刻剂包含（A）由通式[1]表示的单磺酸或其盐（（ B）碱性化合物，（C）水。用于制造太阳能电池制造用硅基基板的方法包括：通过使用蚀刻剂来蚀刻包括硅作为其主要成分的晶片，从而在晶片的表面上形成不均匀的结构。在通式1中，兰德独立地表示氢原子或具有1C-5C的烷基（C是碳的符号），M表示氢原子，碱金属原子，铵（NH）基或四烷基铵（RN）基团，其中R是具有1C-4C的烷基，n表示1-5的整数。

5. 发明专利

JP2012186480A Method for treating surface of semiconductor substrate 有权
标题翻译：用于处理半导体衬底表面的方法
公开(公告)号：JP2012186480A
公开(公告)日：2012-09-27
申请号：JP2012088705
申请日：2012-04-09
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： MIZUTA HIRONORI , KAKIZAWA MASAHIKO , HAYASHIDA KAZUYOSHI
IPC分类号： H01L21/304 , C11D1/04 , C11D1/12 , C11D1/34 , C11D1/72 , C11D3/20 , C11D3/28 , C11D3/30 , C11D3/34 , C11D3/36 , C11D3/43 , C11D7/26 , C11D7/32 , C11D7/36 , C11D7/50 , C11D11/00 , C23G5/02 , C23G5/032 , H01L21/306
CPC分类号： H01L21/02052 , C11D7/261 , C11D7/262 , C11D7/263 , C11D7/264 , C11D7/3245 , C11D7/36 , C11D11/0047 , C23G5/02 , C23G5/032
摘要： PROBLEM TO BE SOLVED: To provide a treatment method which can remove fine particles and metal impurities on the surface of a semiconductor substrate without causing corrosion or oxidation of the semiconductor substrate and a metal wiring, and can simultaneously remove carbon defect on the surface of the substrate without removing a metal corrosion inhibitor-Cu coating film.SOLUTION: The treatment method includes treating the semiconductor substrate having been treated with benzotriazol or slurry containing a derivative thereof with a cleaning agent containing (I) 0.05-50 wt.% of an organic acid having at least one carboxyl group, (II) 0.01-30 wt.% of at least one complexing agent selected from the group consisting of polyphosphonic acids, aryl phosphonic acids and ammonium salt or alkali metal salt thereof, and (III) 0.05-50 wt.% of at least one organic solvent selected from the group consisting of saturated aliphatic monohydric alcohol having 1-5 carbon atoms, alkoxy alcohol having 3-10 carbon atoms, glycol having 2-16 carbon atoms, glycol ether having 3-20 carbon atoms, ketone having 3-10 carbon atoms and nitrile having 2-4 carbon atoms.
摘要翻译：要解决的问题：提供一种能够在不引起半导体衬底和金属布线的腐蚀或氧化的情况下去除半导体衬底的表面上的细小颗粒和金属杂质的处理方法，并且可以同时清除半导体衬底上的碳缺陷的表面，而不去除金属腐蚀抑制剂Cu涂膜。解决方案：处理方法包括用含有（I）0.05-50重量％的具有至少一个羧基的有机酸的清洁剂处理已经用苯并三唑或含有其衍生物的浆料处理的半导体衬底（ II）0.01-30重量％的至少一种选自多膦酸，芳基膦酸和铵盐或其碱金属盐的络合剂，和（III）0.05-50重量％的至少一种有机选自具有1-5个碳原子的饱和脂族一元醇，具有3-10个碳原子的烷氧基醇，具有2-16个碳原子的二醇，具有3-20个碳原子的二醇醚，具有3-10个碳原子的酮的溶剂具有2-4个碳原子的原子和腈。版权所有（C）2012，JPO＆INPIT

6. 发明专利

JP2012051820A Optical resolving agent and method for producing optically active alcohol using the same 审中-公开
标题翻译：光学分解剂和使用其的生产光学活性醇的方法
公开(公告)号：JP2012051820A
公开(公告)日：2012-03-15
申请号：JP2010193889
申请日：2010-08-31
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： YASUNAMI MASABUMI , YOSHIDA YUICHI
IPC分类号： C07C61/39 , C07B57/00 , C07C27/02 , C07C35/12 , C07C61/35 , C07C61/40 , C07C69/753
摘要： PROBLEM TO BE SOLVED: To provide a novel optical resolving agent comprising an optically active azulene derivative which facilitates separation in column chromatography by observation with the naked eye, and a novel method for producing optically active alcohol using the optical resolving agent.SOLUTION: There are provided the optical resolving agent represented by formula [1] and a method for producing optically active alcohol, in which an optical isomer mixture of alcohol is optically resolved using the optical resolving agent. (In the formula, Rrepresents a halogen atom, a hydroxyl group or an alkoxy group having 1-6 carbon atoms, Rrepresents an alkenyl group having 2-10 carbon atoms, an alkeynyl group having 2-10 carbon atoms, an optionally substituted aryl group having 6-10 carbon atoms or the like, Rrepresents an alkyl group having 1-6 carbon atoms, Rrepresents a hydrogen atom or the like, Rrepresents an alkyl group having 1-6 carbon atoms or the like, and n represents an integer of 0-5).
摘要翻译：要解决的问题：提供一种新颖的光学拆分剂，其包含光学活性薁衍生物，其通过肉眼观察在柱色谱中分离，以及使用光学拆分剂制备光学活性醇的新方法。提供由式[1]表示的光学拆分剂和光学活性醇的制造方法，其中使用光学拆分剂光学拆分醇的旋光异构体混合物。（式中，R 1 表示卤原子，羟基或具有1-6个碳原子的烷氧基，R 2 < SP>表示具有2-10个碳原子的烯基，具有2-10个碳原子的烷基，具有6-10个碳原子的任选取代的芳基等，R 3 = SP>表示具有1-6个碳原子的烷基，R 4表示氢原子等，其中R 1表示氢原子等。具有1-6个碳原子的烷基等，n表示0-5的整数）。版权所有（C）2012，JPO＆INPIT

7. 发明专利

JP2011090004A Hyaluronic acid measuring kit for immune-aggregation method 有权
标题翻译：用于免疫聚集方法的HYALURONIC ACID MEASURING KIT
公开(公告)号：JP2011090004A
公开(公告)日：2011-05-06
申请号：JP2010271682
申请日：2010-12-06
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： TSUNODA KYOICHI , FUJIO KAZUNARI , OBATA SHINZO
IPC分类号： G01N33/543 , G01N21/82 , G01N33/53 , G01N33/545
CPC分类号： G01N33/543 , G01N21/82 , G01N2400/40
摘要： PROBLEM TO BE SOLVED: To provide a hyaluronic acid measuring kit for immune-aggregation method, and having little sedimentation of the carrier, superior preservation stability thereof, and high accuracy which is equivalent to those of conventional reagents. SOLUTION: A monoclonal antibody to a hyaluronic acid binding protein (hereinafter, may be abbreviated as "HABP") is sensitized beforehand to latex particles, and a complex of HABP and hyaluronic acid is reacted therewith, to thereby efficiently generate a latex particle agglutination reaction corresponding to a hyaluronic acid quantity. Furthermore, latex particles to which the monoclonal antibody to HABP is sensitized, and the hyaluronic acid binding protein are preserved as different reagents, to thereby acquire a reagent for hyaluronic acid measurement having superior preservation stability. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种用于免疫聚集方法的透明质酸测量试剂盒，并且载体几乎没有沉淀，其优异的保存稳定性和与常规试剂相当的高精度。解决方案：将透明质酸结合蛋白的单克隆抗体（以下简称为“HABP”）预先对胶乳颗粒进行致敏，并使HABP和透明质酸的络合物与其反应，从而有效地产生胶乳颗粒凝集反应对应于透明质酸量。此外，将对HABP的单克隆抗体敏感的胶乳颗粒和透明质酸结合蛋白作为不同的试剂保留，从而获得具有优异的保存稳定性的透明质酸测试用试剂。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2011053229A Analysis assisting method, analyzer, remote computer, data analyzing method, program, and reagent container 有权
标题翻译：分析辅助方法，分析仪，远程计算机，数据分析方法，程序和试剂容器
公开(公告)号：JP2011053229A
公开(公告)日：2011-03-17
申请号：JP2010277509
申请日：2010-12-13
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： SATOMURA MASAHIRO , KOMIYAMA KISHISATO
IPC分类号： G01N35/00 , G01N35/02 , G06Q50/22 , G06Q50/24
CPC分类号： G01N35/00663 , B01L3/545 , G01N1/28 , G01N35/00732 , G01N35/00871 , G01N2035/00673 , G01N2035/00782 , G01N2035/00811 , G01N2035/00841 , G01N2035/00851 , Y10T436/11 , Y10T436/115831 , Y10T436/12
摘要： PROBLEM TO BE SOLVED: To enable appropriate management of reagents. SOLUTION: In an analysis system having an analysis apparatus using a reagent container having a memory to store reagent information concerning a reagent in the container and a remote computer, the following steps are executed: reading out the reagent information from the memory of the reagent container; determining, based on the reagent information, whether or not the reagent in the reagent container is usable; writing data representing the reagent is unusable into the memory of the reagent container when the reagent in the reagent container is determined to be unusable; and registering the data representing the reagent is unusable in a reagent database managed by the remote computer corresponding to reagent container ID when the reagent in the reagent container is determined to be unusable. Thus, it is possible to manage reagents so as not to use a reagent, which must not be used, for analysis by automatically identifying it. In addition, it is possible to use the data for improvement of the efficiency in business operations such as the automatic order of reagents, stock management in a manufacturer and the like. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：实现对试剂的适当管理。解决方案：在具有分析装置的分析系统中，使用具有存储器的试剂容器，该容器具有存储容器中的试剂的试剂信息和远程计算机，执行以下步骤：从存储器中读取试剂信息试剂容器; 基于试剂信息确定试剂容器中的试剂是否可用; 当试剂容器中的试剂被确定为不可用时，表示试剂的写入数据不能用于试剂容器的存储器中; 并且当试剂容器中的试剂被确定为不可用时，在与试剂容器ID相对应的由远程计算机管理的试剂数据库中登记表示试剂的数据不可用。因此，可以管理试剂，以便不使用不能使用的试剂进行自动识别的试剂进行分析。此外，可以使用用于提高商业操作的效率的数据，例如试剂的自动顺序，制造商中的库存管理等。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2010190906A Solvent for high-sensitivity analysis, and preservation method therefor 审中-公开
标题翻译：用于高灵敏度分析的溶剂及其保存方法
公开(公告)号：JP2010190906A
公开(公告)日：2010-09-02
申请号：JP2010094368
申请日：2010-04-15
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： OHARA MASAHIRO , SAITO REI , IWAMOTO YOSHIAKI
IPC分类号： G01N30/26 , G01N30/34
CPC分类号： G01N30/34
摘要： PROBLEM TO BE SOLVED: To provide a solvent having small amount of impurities (hardly increasing an impurity content) by enhancing difficulty of elution of alkali metals into the solvent.
SOLUTION: This invention is directed to methanol or acetonitrile which is preserved in a glass container subjected to a removal processing of alkali metals, and which is used for a liquid chromatography method, a liquid chromatography/mass spectrum method (LC/MS), a liquid chromatography/mass spectrum/mass spectrum method (LC/MS/MS), an inductively coupled plasma emission spectrometry (ICP/AES), an inductively coupled plasma mass spectrometry (ICP/MS), a capillary electrophoresis method, or an ion chromatograph method.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：通过增加碱金属向溶剂中的洗脱的难度，提供具有少量杂质（几乎不增加杂质含量）的溶剂。解决方案：本发明涉及保存在经过碱金属去除处理的玻璃容器中的甲醇或乙腈，用于液相色谱法，液相色谱/质谱法（LC / MS ），液相色谱/质谱/质谱法（LC / MS / MS），电感耦合等离子体发射光谱法（ICP / AES），电感耦合等离子体质谱法（ICP / MS），毛细管电泳法离子色谱法。版权所有（C）2010，JPO＆INPIT

10. 发明专利

JP2010169497A Treatment device of microplate 审中-公开
标题翻译：麦芽汁处理装置
公开(公告)号：JP2010169497A
公开(公告)日：2010-08-05
申请号：JP2009011531
申请日：2009-01-22
申请人： Wako Pure Chem Ind Ltd , 和光純薬工業株式会社
发明人： YAMASHITA SHIRO , HIGUCHI AKIRA , SHIMOKAWA KOJI
IPC分类号： G01N35/02 , G01N35/04
摘要： PROBLEM TO BE SOLVED: To provide a treatment device of a microplate capable of holding a lid stably, even when a heavy lid such as metal one is used as an object.
SOLUTION: A lid holding mechanism 7 for holding a metal lid 4 separated from a microplate 3 on a prescribed position has a constitution including a first holding member 22A and a second holding member 22B provided respectively with an abutting part 22a abutting on each holding side surface 4b on both sides of the lid 4 and a locking part for locking the under surface of the lid 4, a first spring member 24A and a second spring member 24B for pressing the abutting part 22a from the X-direction by energizing each holding member, and a rotation prevention part 26 for preventing rotation of the lid 4 caused by a self-weight by fulcruming a locking point by a locking part by abutment on the upper surface of the lid 4. Hereby, even when a heavy lid 4 is used as an object, rotation of the lid 4 caused by a self-weight can be surely prevented.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：即使当使用诸如金属的重型盖作为对象时，提供能够稳定地保持盖的微孔板的处理装置。解决方案：用于保持与微孔板3在规定位置分离的金属盖4的盖保持机构7具有包括第一保持构件22A和第二保持构件22B的构造，第一保持构件22A和第二保持构件22B分别设置有邻接部分22a 保持在盖4的两侧的侧表面4b和用于锁定盖4的下表面的锁定部分;第一弹簧构件24A和第二弹簧构件24B，用于通过向每个保持构件，以及防止旋转的部分26，用于通过在盖4的上表面上邻接而通过由锁定部分支撑锁定点，防止由自重引起的盖4的旋转。因此，即使当重的盖4 被用作物体，可以可靠地防止由自重引起的盖4的旋转。版权所有（C）2010，JPO＆INPIT

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