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1. 发明专利

JP2002128809A METHOD OF MANUFACTURING POLYBUTADIENE 失效
公开(公告)号：JP2002128809A
公开(公告)日：2002-05-09
申请号：JP2000328521
申请日：2000-10-27
申请人： UBE INDUSTRIES
发明人： SUZUKI KATSUNORI , NISHIMURA YOSHIO , KITAMURA TAKASHI , MORIMOTO MASANORI
IPC分类号： C08F2/00 , C08F4/69 , C08F36/00 , C08F36/06
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing polybutadiene which causes no gel adhesion to a polymerization apparatus and contains little gel. SOLUTION: In this method of manufacturing polybutadiene by polymerizing 1,3-butadiene in an inactive organic solvent in the presence of a polymerization catalyst, water needed is added in a mist form to an inactive solvent or to a solution of 1,3-butadiene in the inactive organic solvent and mixed.

2. 发明专利

JPH09249703A VAPOR-PHASE POLYMERIZATION OF OLEFIN 失效
公开(公告)号：JPH09249703A
公开(公告)日：1997-09-22
申请号：JP6264796
申请日：1996-03-19
申请人： UBE INDUSTRIES
发明人： YANO YUJI , SUZUKI KATSUNORI , TAKASHIMA HIDEAKI , NISHIMURA YOSHIO , SHINODA TADAOKI
IPC分类号： C08F2/00 , B01J8/18 , B01J8/24 , C08F2/34 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To prevent the occurrence of a massive polymer in the conventional fluidized bed vapor-phase polymerization process and realize a long-term stable polymerization reaction. SOLUTION: A process for the continuous vapor-phase polymerization of olefins in a fluidized bed reactor, wherein a circulating gas containing an unreacted monomer discharged from the reactor and a supplementary monomer is cooled in such a manner as to satisfy the relation of the formula Td

3. 发明专利

JP2002060410A MANUFACTURING METHOD FOR POLYBUTADIENE 失效
公开(公告)号：JP2002060410A
公开(公告)日：2002-02-26
申请号：JP2000250535
申请日：2000-08-22
申请人： UBE INDUSTRIES
发明人： SUZUKI KATSUNORI , MORIMOTO MASANORI , KITAMURA TAKASHI , NISHIMURA YOSHIO
IPC分类号： C08F4/602 , C08F36/00 , C08F36/06
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing polybutadiene having little gels, without depositing gels onto reaction apparatuses. SOLUTION: Polybutadiene is manufactured by polymerizing 1,3-butadiene in an inert organic solvent and in the presence of a polymerization catalyst, wherein water that has been treated with tourmaline is added to an inert solvent or to 1,3-butadiene in an inert organic solvent to be mixed as a necessary water component.

4. 发明专利

JPH0583866B2 失效
公开(公告)号：JPH0583866B2
公开(公告)日：1993-11-29
申请号：JP7919985
申请日：1985-04-16
申请人： UBE INDUSTRIES
发明人： MYAMOTO MAMORU , NISHIMURA YOSHIO , MIURA MASAO
IPC分类号： G01N31/00 , G01N31/22

5. 发明专利

JP2001288210A DRYING METHOD OF RUBBER 失效
公开(公告)号：JP2001288210A
公开(公告)日：2001-10-16
申请号：JP2000101720
申请日：2000-04-04
申请人： UBE INDUSTRIES
发明人： SENJU HIROHISA , MORIMOTO MASANORI , NISHIMURA YOSHIO
IPC分类号： C08F6/10 , C08F4/70 , C08F36/06
摘要： PROBLEM TO BE SOLVED: To provide a novel method of effectively and uniformly drying a rubber from a rubber solution. SOLUTION: The drying method of the rubber comprises drying with a microwave crumbs made desolvation from the rubber solution, and particularly, from a polybutadiene rubber solution made by solution polymerizing 1,3-butadiene.

6. 发明专利

JP2002020427A METHOD FOR PRODUCING POLYBUTADIENE 失效
公开(公告)号：JP2002020427A
公开(公告)日：2002-01-23
申请号：JP2000210128
申请日：2000-07-11
申请人： UBE INDUSTRIES
发明人： OFUJI MINORU , TSUDA SUSUMU , MORIMOTO MASANORI , NISHIMURA YOSHIO
IPC分类号： C08F2/06 , C08F4/70 , C08F36/06
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a polybutadiene having a low gel content without causing the deposition of gel in a polymerization apparatus. SOLUTION: In a method for producing polybutadiene by polymerizing 1,3-butadiene in an inert organic solvent in the presence of a polymerization catalyst, a necessary amount of water in the form of steam and/or hot water is added to and homogeneously mixed into the inert organic solvent or a solution of 1,3-butadiene in the solvent.

7. 发明专利

JPH09278807A PROCESS FOR GAS-PHASE POLYMERIZATION OF OLEFIN 失效
公开(公告)号：JPH09278807A
公开(公告)日：1997-10-28
申请号：JP9452796
申请日：1996-04-16
申请人： UBE INDUSTRIES
发明人： SHINODA TADAOKI , SUZUKI KATSUNORI , NISHIMURA YOSHIO , YANO YUJI
IPC分类号： C08F2/34 , C08F10/00
摘要： PROBLEM TO BE SOLVED: To provide a process for the gas-phase polymn. of an olefin in a fluidized bed reactor, wherein the content of the reactor are irradiated with βrays to inhibit the formation of polymer masses, thereby enabling a stable polymn. reaction for a long time. SOLUTION: The gas-phase polymn. is conducted by continuously introducing a gas-phase reaction mixture comprising a catalyst component, an olefin monomer, an inert gas and an additive into a fluidized-bed reactor through a feedstock feeding line 8 to carry out the gas-phase polymn. while the catalyst particles and polymer particles are fluidized by the gas-phase component in a gas-phase fluidized bed part 1. In the gas phase polymn., a radiation source 11 is embedded in a cylinder wall of the reactor or a stilling partition wall in an upper part of the reactor to irradiate the contents of the reactor with βrays from the source to thereby conduct the polymn. The polymer is continuously or intermittently extracted through a drawing line 10.

8. 发明专利

JPS61239162A METHOD FOR DETECTING BREAK THROUGH OF GAS ADSORBING DEVICE BY GASEOUS CHLORINE 失效
公开(公告)号：JPS61239162A
公开(公告)日：1986-10-24
申请号：JP7919985
申请日：1985-04-16
申请人： UBE INDUSTRIES
发明人： MIYAMOTO MAMORU , NISHIMURA YOSHIO , MIURA MASAO
IPC分类号： G01N31/00 , G01N31/22
摘要： PURPOSE:To make the exact detection of the break through by gaseous chlorine possible by packing a break through detecting agent prepd. by depositing potassium iodide on a carrier and subjecting the carrier to coating into a gas discharge port of a gas adsorbing device and detecting the break through from the coloration of the detecting agent. CONSTITUTION:An adsorbent 4 is packed into a vessel 3 which constitutes the gas adsorbing device and has a gas introducing port 1 and the gas discharge port 2. A detecting part 6 for the break through of the gaseous chlorine which consists of a vessel to permit the viewing through of the inside is provided near the port 2. The gaseous chlorine break through detecting agent 5 prepd. by depositing the potassium iodide on the carrier consisting of, for example, alpha-alumina and subjecting the carrier to coating by using, for example, polymethacrylate and drying the same is packed into the vessel of the detecting part 6. When the waste gas of dry etching using the gaseous chlorine flows out of the port 2, the agent 5 colors immediately yellowish brown and does not exhibit color fading and therefore the exact detection of the break through of the gaseous chlorine is made possible.

9. 发明专利

JP2002145887A METHOD FOR PRODUCING ALUMOXANE 失效
公开(公告)号：JP2002145887A
公开(公告)日：2002-05-22
申请号：JP2000334542
申请日：2000-11-01
申请人： UBE INDUSTRIES
发明人： SUZUKI KATSUNORI , NISHIMURA YOSHIO , KITAMURA TAKASHI , MORIMOTO MASANORI
IPC分类号： C07C29/54 , C07C31/32 , C07F5/06
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an alumoxane in which a disproportionation reaction is slightly caused by reactng a trialkylalumnum compound with water. SOLUTION: Water in a misty state is added and mixed with the trialkylaluminum compound in the method for producing the alumoxane comprising reacting the trialkylaluminum compound with water in an inert organic solvent.

10. 发明专利

JPS622140A DETECTING AGENT OF BORONTRICHLORIDE AND BREAKTHROUGH DETECTION FOR BORONTRICHLORIDE ADSORBER 失效
公开(公告)号：JPS622140A
公开(公告)日：1987-01-08
申请号：JP14020985
申请日：1985-06-28
申请人： UBE INDUSTRIES
发明人： OIZUMI KYOHEI , MIYAMOTO MAMORU , NISHIMURA YOSHIO , MIURA MASAO
IPC分类号： G01N21/77 , G01N21/78 , G01N31/00 , G01N31/22
摘要： PURPOSE:To detect breakthrough of a boron trichloride adsorber,, by packing a boron trichloride detecting agent comprising carminic acid, hydrochloric acid and sulfuric acid supported on a carrier near the gas exhaust port thereof to check coloring of the detecting agent. CONSTITUTION:A boron trichloride detecting agent 5 is composed of carminic acid, hydrochloric acid and sulfuric acid supported on a carrier. In the method of detecting breakthrough of boron trichloride from a gas adsorber, a boron trichloride breakthrough detector section 6 which comprises a internally see- through container packed with the boron trichloride detecting agent 5 is set near an exhaust port 2 of the gas adsorber which has a container 3 packed with an adsorbant 4 having a gas introduction port 1 and the gas exhaust port 2 to check coloring of boron trichloride of the detecting agent 5. Thus, boron trichloride can be detected while the breakthrough of the boron trichloride adsorber can be detected.

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