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1. 发明专利

JP2010261907A Radioactive waste solidification method 有权
标题翻译：放射性废物固化方法
公开(公告)号：JP2010261907A
公开(公告)日：2010-11-18
申请号：JP2009114778
申请日：2009-05-11
申请人： Toshiba Aitekku Kk , Toshiba Corp , 東芝アイテック株式会社 , 株式会社東芝
发明人： SATO TATSUAKI , SHOJI YUICHI , YAMASHITA TAKEO , KOMATSUBARA MASARU , YASUMURA KEIJIRO
IPC分类号： G21F9/30 , G21F9/16
摘要： PROBLEM TO BE SOLVED: To provide a radioactive waste solidification method for satisfactorily solidifying incineration ash of a relatively high radiation dose, with cement as the solidifying material. SOLUTION: The radioactive waste solidification and disposal method uses a kneading and solidifying container having a powder material cast port and a liquid material cast port; inputs the powder radioactive waste, kneading water, cement, and a setting accelerator into the kneading and solidifying container via the powder material cast port and the liquid material cast port to knead them; and then solidify them in the kneading and solidifying container. The radioactive waste contains one or more kinds of heavy metals selected from among zinc and lead. The number of moles of the amount of the setting accelerator cast to the kneading and solidifying container is not less than 2.1 times the number of moles of the heavy metals of the radioactive waste cast with respect to the kneading and solidifying container. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供放射性废物固化方法，以令人满意地凝固相对较高辐射剂量的焚化灰，其中以水泥作为凝固材料。解决方案：放射性废物固化处理方法使用具有粉末铸造口和液体铸造口的捏合固化容器; 将粉末放射性废物，捏合水，水泥和凝固促进剂经由粉末铸造口和液体铸造口输入捏合固化容器中以进行捏合; 然后将其固化在捏合和固化容器中。放射性废物含有选自锌和铅的一种或多种重金属。添加到捏合固化容器中的凝固促进剂的摩尔数不小于相对于捏合固化容器的放射性废物铸造重金属的摩尔数的2.1倍。版权所有（C）2011，JPO＆INPIT

2. 发明专利

JP2009068947A Method and device for granulating radioactive waste 有权
标题翻译：用于生产放射性废物的方法和装置
公开(公告)号：JP2009068947A
公开(公告)日：2009-04-02
申请号：JP2007236613
申请日：2007-09-12
申请人： Toshiba Aitekku Kk , Toshiba Corp , 東芝アイテック株式会社 , 株式会社東芝
发明人： SATO TATSUAKI , MIKURA MICHITAKA , HARUGUCHI YOSHIKO , MURATA EIICHI , YAMASHITA TAKEO , SHOJI YUICHI , OKANO TOSHIAKI , KAWABE AKIHIRO , YASUMURA KEIJIRO
IPC分类号： G21F9/30
摘要： PROBLEM TO BE SOLVED: To provide a method and a device for granulating radioactive waste which make it possible to stably atomize a binder for granulating fine particles of the radioactive waste over a long period.
SOLUTION: The device is composed of a mixer tank 8 to which powdery radioactive waste is fed, a granulator 11 for granulating the radioactive waste mixed with the binder in the mixer tank 8, a nozzle 4 mounted on the mixer tank 8 to atomize the liquid binder over the powdery radioactive waste and an excitation means 5 to impart impulsive vibration to the nozzle 4.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种使放射性废物造粒的方法和装置，其可以稳定地雾化用于使放射性废物细颗粒成粒的长时间的粘合剂。解决方案：该装置由供给粉状放射性废物的混合罐8，混合罐8中与粘合剂混合的放射性废料造粒的造粒机11，安装在混合罐8上的喷嘴4 将粉末状放射性废物上的液体粘合剂雾化，以及激发装置5，以向喷嘴4施加脉冲振动。版权所有（C）2009，JPO＆INPIT

3. 发明专利

JP2011085552A Method for solidifying concentrated sodium sulfate liquid waste containing boric acid 有权
标题翻译：用于固化含硫酸钠的含硫酸钠液体废物的方法
公开(公告)号：JP2011085552A
公开(公告)日：2011-04-28
申请号：JP2009240467
申请日：2009-10-19
申请人： Toshiba Aitekku Kk , Toshiba Corp , 東芝アイテック株式会社 , 株式会社東芝
发明人： KANEKO MASAAKI , HARUGUCHI YOSHIKO , YAMASHITA TAKEO , MIKURA MICHITAKA , YASUMURA KEIJIRO , SATO TATSUAKI , SHOJI YUICHI , OBATA MASAMICHI , HORIMOTO TAICHI
IPC分类号： G21F9/16
摘要： PROBLEM TO BE SOLVED: To prevent condensation delays when solidifying a concentrated sodium sulfate liquid waste containing boric acid, and to prevent deterioration of the strength necessary for solidification of a cement solidified body.
SOLUTION: The concentration ratio of boron and lithium in a concentrated sodium sulfate liquid waste containing boric acid is detected. The concentration ratio is checked as being not less than 2; and when the concentration ratio is 2 or more, cement is added to and mixed with the concentrated sodium sulfate liquid waste and makes the concentrated sodium sulfate liquid waste solidify. When the concentration ratio is not more than 2, after the concentration ratio is increased to 2 or more by adding a lithium compound to the concentrated sodium sulfate liquid waste, the concentrated sodium sulfate liquid waste is solidified, by adding and mixing cement with the concentrated sodium sulfate liquid waste.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了防止在浓缩含有硼酸的浓硫酸钠废液固化时的冷凝延迟，并且防止水泥固化体凝固所需的强度变差。解决方案：检测含有硼酸的浓硫酸钠废液中硼和锂的浓度比。检查浓度比不小于2; 当浓度比为2以上时，向浓硫酸钠废液中添加水泥并与其混合，使浓硫酸钠液体废液固化。当浓度比不大于2时，通过向浓缩的硫酸钠废液中加入锂化合物使浓缩比增加至2以上后，将浓缩的硫酸钠废液固化，通过将浓缩水泥与浓缩的硫酸钠液体废物。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2011075407A Method for treating drainage containing radioactive ammonia 有权
标题翻译：用于处理含有放射性氨的排水的方法
公开(公告)号：JP2011075407A
公开(公告)日：2011-04-14
申请号：JP2009227206
申请日：2009-09-30
申请人： Toshiba Aitekku Kk , Toshiba Corp , 東芝アイテック株式会社 , 株式会社東芝
发明人： KANEKO MASAAKI , MIKURA MICHITAKA , HARUGUCHI YOSHIKO , YAMASHITA TAKEO , YASUMURA KEIJIRO , OBATA MASAMICHI , HORIMOTO TAICHI
IPC分类号： G21F9/12 , C02F1/00 , C02F1/42 , G21F9/02 , G21F9/16 , G21F9/30
摘要： PROBLEM TO BE SOLVED: To provide a new method which attains easy the removal of ammonia from drainage containing radioactive ammonia and a stabilizing treatment of the drainage.
SOLUTION: A cation exchanger B is submerged in the drainage A, containing radioactive ammonia to fix ammonium ions in the drainage A in the cation exchanger B (S1). Then, the residue of the drainage A, after the fixation of the cation exchanger B and the ammonium ions, is solidified by cement (S2).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种新方法，其可以容易地从含有放射性氨的排水中去除氨并且稳定地处理排水。解决方案：阳离子交换剂B浸没在排放A中，含有放射性氨以将铵离子固定在阳离子交换器B中的排水A中（S1）。然后，将阳离子交换剂B和铵离子固定后的排水A的残渣用水泥固化（S2）。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2010151487A Method for solidifying waste liquid of boric acid 有权
标题翻译：用于固化硼酸的废液的方法
公开(公告)号：JP2010151487A
公开(公告)日：2010-07-08
申请号：JP2008327420
申请日：2008-12-24
申请人： Toshiba Aitekku Kk , Toshiba Corp , 東芝アイテック株式会社 , 株式会社東芝
发明人： SATO TATSUAKI , SHOJI YUICHI , YAMASHITA TAKEO , KANEKO MASAAKI , MIKURA MICHITAKA , AISAKA TAKASHI , NISHIKUBO MASARU , YASUMURA KEIJIRO
IPC分类号： G21F9/16
摘要： PROBLEM TO BE SOLVED: To provide a method for solidifying a waste liquid of boric acid which is excellent in energy efficiency and shortens the treatment time while preventing the instant condensation in the solidification of the waste liquid of boric acid, facilitating the handling of the solidified waste liquid of boric acid and decreasing the quantity of waste by curbing the usage of extra additives and the like. SOLUTION: After a borate solution is prepared by adding a monovalent alkali metal hydroxide to the waste liquid of boric acid to neutralize it, heating treatment is given to it to prepare a condensed borate solution where the concentration of the borate in the borate solution is 62 wt.% or higher in terms of boric acid. Moreover, cement of 0.17 to 0.33% in the total weight is added to and mixed with the condensed borate solution to solidify it. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种固化硼酸废液的方法，其能量效率优异并缩短处理时间，同时防止硼酸废液凝固中的即时冷凝，便于处理的固化的硼酸废液，通过抑制额外的添加剂等的使用来减少废物的量。解决方案：通过向硼酸废液中加入一价碱金属氢氧化物来中和硼酸盐溶液后，加热处理以制备硼酸盐浓度在硼酸盐中的浓缩硼酸盐溶液溶液的硼酸为62重量％以上。此外，将总重量为0.17至0.33％的水泥加入并与冷凝的硼酸盐溶液混合以使其固化。（C）2010，JPO＆INPIT

6. 发明专利

JP2015054282A 溶質の回収方法および溶質の回収装置审中-公开
标题翻译：解决方案和解决方案的恢复方法
公开(公告)号：JP2015054282A
公开(公告)日：2015-03-23
申请号：JP2013188848
申请日：2013-09-11
申请人：株式会社東芝 , Toshiba Corp
发明人： MIYAMOTO MASAYA , IKEI SHUKO , KAWAUCHI KANAE , NAGAMORI YASUHIKO , YAMASHITA TAKEO , MIKURA MICHITAKA
IPC分类号： C02F1/62 , C02F1/58
摘要：【課題】重金属およびリンを含有する強酸性の溶液から、重金属類とリンを選択的に回収することが可能な、溶質の回収方法および溶質の回収装置を提供することを目的とする。【解決手段】実施形態の溶質の回収方法は、初期溶液に重金属除去剤を添加する重金属除去ステップと、重金属除去剤が添加された初期溶液を第1の液相と第1の固相に固液分離する第1の固液分離ステップと、第1の液相にリン除去剤を添加するリン除去ステップと、リン除去剤が添加された第1の液相を第2の液相と第2の固相に固液分離する第2の固液分離ステップと、を備え、初期溶液は焼却灰から放射性核種を抽出した後に放射性核種が回収された溶液であるものとする。【選択図】図3
摘要翻译：要解决的问题：提供能够从包括重金属和磷的强酸性溶液中选择性地回收重金属和磷的溶质的溶质和回收装置的回收方法。解决方案：实施方案的溶质回收方法包括将重金属去除剂添加到初始溶液中的重金属去除步骤，将已经添加有重金属去除剂的初始溶液固液分离到第一液相中的第一固液分离步骤和第一固相，磷除去步骤，向第一液相中加入除磷剂;以及第二固 - 液分离步骤，将已经加入除磷剂的第一液相固液分离到第二液相中，第二固相; 初始溶液是通过从焚烧灰中提取放射性核素然后回收放射性核素获得的溶液。

7. 发明专利

JP2014019898A Method for recovering rhenium 有权
标题翻译：回收铑的方法
公开(公告)号：JP2014019898A
公开(公告)日：2014-02-03
申请号：JP2012159070
申请日：2012-07-17
申请人： Toshiba Corp , 株式会社東芝
发明人： KANEMURA SHOHEI , MIZUGUCHI KOJI , TAKAHASHI YUYA , YAMASHITA TAKEO , YAITA YUMI , OSATO TETSUO , OMORI TAKASHI , YAZAWA TAKASHI , FUJITA REIKO
IPC分类号： C22B61/00 , C22B3/04 , C22B3/44 , C25B1/00
CPC分类号： Y02P10/234
摘要： PROBLEM TO BE SOLVED: To provide a method for recovering rhenium not using an ion exchange resin or a solvent extraction method.SOLUTION: The method for recovering rhenium comprises: a step (S11) of adding bivalent iron ions (Fe)to a rhenium-containing liquid 1a; a step (S12) of adding a Ph regulator 3 to precipitate rhenium; a step (S13) of recovering precipitates 5 from a mother liquid 4 by solid-liquid separation; and a step of adding acid to the precipitates 5 to dissolve rhenium (S14) and producing a rhenium-concentrated liquid 6.
摘要翻译：要解决的问题：提供不使用离子交换树脂的铼的回收方法或溶剂萃取方法。解决方案：回收铼的方法包括：将二价铁离子（Fe）添加到铼 - 容纳液体1a; 添加Ph调节剂3以沉淀铼的步骤（S12）; 通过固液分离从母液4回收沉淀物5的步骤（S13）; 以及向沉淀物5中加入酸以溶解铼的步骤（S14）并产生铼浓缩液体6。

8. 发明专利

JP2013101008A Treatment method and treatment device for radioactive cesium and radioactive strontium contained substance 审中-公开
标题翻译：用于放射性硒和放射性锶含有物质的处理方法和处理装置
公开(公告)号：JP2013101008A
公开(公告)日：2013-05-23
申请号：JP2011244091
申请日：2011-11-08
申请人： Toshiba Corp , 株式会社東芝
发明人： MIKURA MICHITAKA , HARUGUCHI YOSHIKO , OMURA TSUNEO , AKAI YOSHIE , YAMASHITA TAKEO , SUGIMORI TOSHIAKI , MIYAMOTO MASAYA
IPC分类号： G21F9/28 , G21F9/08
摘要： PROBLEM TO BE SOLVED: To easily and efficiently remove radioactive cesium and radioactive strontium from a substance such as soil or mud contaminated by the radioactive cesium and the radioactive strontium.SOLUTION: An organic substance from which cesium and strontium is selectively extractable is brought into contact with a substance containing radioactive cesium and radioactive strontium. Then, at least supercritical carbon dioxide is supplied to and brought into contact with at least the organic substance, and the organic substance is dissolved in the supercritical carbon dioxide. Then, the supercritical carbon dioxide is decompressed, and the supercritical carbon dioxide is converted into carbon dioxide gas so that the organic substance can be separated and removed from the supercritical carbon dioxide.
摘要翻译：要解决的问题：从放射性铯和放射性锶污染的土壤或泥土等物质容易有效地清除放射性铯和放射性锶。解决方案：将铯和锶选择性萃取的有机物质与含有放射性铯和放射性锶的物质接触。然后，至少将超临界二氧化碳供给至少与有机物质接触，有机物质溶解在超临界二氧化碳中。然后，将超临界二氧化碳减压，将超临界二氧化碳转化成二氧化碳，使有机物质从超临界二氧化碳中分离除去。版权所有（C）2013，JPO＆INPIT

9. 发明专利

JP2013014793A Method of producing rare metal 有权
标题翻译：生产稀有金属的方法
公开(公告)号：JP2013014793A
公开(公告)日：2013-01-24
申请号：JP2011146565
申请日：2011-06-30
申请人： Toshiba Corp , 株式会社東芝
发明人： MIZUGUCHI KOJI , KANEMURA SHOHEI , OSATO TETSUO , TAKAHASHI YUYA , YAITA YUMI , YAMASHITA TAKEO , FUJITA REIKO , OMORI TAKASHI , YAZAWA TAKASHI
IPC分类号： C25C1/22 , C22B3/04 , C22B3/26 , C22B3/42 , C22B3/44 , C22B59/00 , C22B61/00 , C25C3/34
CPC分类号： C22B3/0005 , C22B3/42 , C22B3/46 , C22B59/00 , C22B61/00 , C25C3/34 , Y02P10/234
摘要： PROBLEM TO BE SOLVED: To provide a method of producing rare metal of high robustness with respect to a solution composition, including a process of removing impurities from a raw material solution.SOLUTION: The method of producing rare metal includes steps (S11 to S14) of recovering a first residual liquid, steps (S15, S16) of extracting ReO, a step (S17) of back-extracting the same into a first eluent, steps (S18, S19) of collecting Re onto a cathode by way of electrolysis, a step (S20) of recovering a second residual liquid, steps (S21, S22) of adjusting hydrogen ion exponent in a range of not lower than pH 3 and lower than pH 5, steps (S23, S24) of extracting rare earth metal ion (Re), a step (S25) of back-extracting the same into a second eluent, a step (S26) of adding (COOH)to precipitate Re(CO), steps (S27, S28) of converting it to a rare earth metal oxide (ReO), and steps (S29, S30) of collecting rare earth metal (Re) onto a cathode by way of molten salt electrolysis.
摘要翻译：待解决的问题：提供一种制备相对于溶液组合物具有高坚固性的稀有金属的方法，包括从原料溶液中除去杂质的方法。解决方案：稀土金属的制造方法包括回收第一残留液的工序（S11〜S14），提取ReO 4 3 + ），将第二洗脱液反萃取的步骤（S25），添加（COOH） 2 以沉淀Re 2 （C 2 O 4 ） 3 ，将其转换为稀土金属氧化物的步骤（S27，S28）（Re 2 O 3）和通过熔融盐电极将稀土金属（Re）收集到阴极上的步骤（S29,301）裂解。版权所有（C）2013，JPO＆INPIT

10. 发明专利

JP2012225663A Quantitative analysis method of plutonium 审中-公开
标题翻译：钚的定量分析方法
公开(公告)号：JP2012225663A
公开(公告)日：2012-11-15
申请号：JP2011090701
申请日：2011-04-15
申请人： Toshiba Corp , 株式会社東芝
发明人： YAMASHITA TAKEO , MIKURA MICHITAKA , KUROSAWA SETSUMI , MURATA EIICHI , MATSUYAMA KANAE , HARUGUCHI YOSHIKO , SAKURAI JIRO , HIROSE EMIKO
IPC分类号： G01T1/167
摘要： PROBLEM TO BE SOLVED: To provide Pu (plutonium) quantitative analysis method capable of quantitatively analyzing Pu by using radiation measurement such as α-ray spectrometry even in an analysis target sample solution containing much impurity elements such as Ca interrupting α-ray measurement.SOLUTION: The Pu quantitative analysis method for quantitatively analyzing Pu in an analysis target sample solution 10 includes: an iron hydroxide coprecipitation step S101 for generating iron hydroxide coprecipitate 12 containing a rare earth element by adding rare earth compound and iron compound to the analysis target sample solution 10; a rare earth fluoride coprecipitation step S104 for generating rare earth fluoride coprecipitate 15 by adding fluoride to an iron hydroxide coprecipitate solution 13 obtained by dissolving the iron hydroxide coprecipitate 12; and a radiation measurement step S107 for quantitatively analyzing Pu by radiation measurement of a measuring sample 16 prepared from the rare earth fluoride coprecipitate 15.
摘要翻译：要解决的问题：为了提供能够通过使用诸如α射线光谱法的辐射测量来定量分析Pu的Pu（钚）定量分析方法，即使在含有大量杂质元素如Ca中断α-射线的分析目标样品溶液中测量。解决方案：用于在分析对象样品溶液10中定量分析Pu的Pu定量分析方法包括：通过向稀土化合物和铁化合物添加含有稀土元素的氢氧化铁共沉淀物12的氢氧化铁共沉淀步骤S101，分析目标样品溶液10; 稀土氟化物共沉淀步骤S104，用于通过将氟化氢沉淀物12溶解得到的氢氧化铁共沉淀溶液13中加入氟化物来生成稀土氟化物共沉淀物15; 以及辐射测量步骤S107，用于通过由稀土氟化物共沉淀物15制备的测量样品16的辐射测量来定量分析Pu。（C）2013，JPO和INPIT

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