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1. 发明专利

JP2012230867A Oxide superconducting thin film, and manufacturing method thereof 有权
标题翻译：氧化物超导薄膜及其制造方法
公开(公告)号：JP2012230867A
公开(公告)日：2012-11-22
申请号：JP2011099999
申请日：2011-04-27
申请人： Sumitomo Electric Ind Ltd , 住友電気工業株式会社 , National Institute Of Advanced Industrial & Technology , 独立行政法人産業技術総合研究所
发明人： HONDA GENKI , NAGAISHI TATSUOKI , NAKANISHI TAKESHI , OKI YASUTARO , YAMAGUCHI TAKASHI , HANAFUSA KEI , YAMAGUCHI IWAO , MANABE TAKAAKI , KUMAGAI TOSHIYA , YAMAZAKI HIROFUMI , SHIMOYAMA JUNICHI , MUKODA MASASHI
IPC分类号： H01B13/00 , C01G1/00 , H01B12/06 , H01F6/06 , H01L39/24
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide an oxide superconducting thin film in which Jc is not lowered and which has high Ic corresponding to a film thickness, even if the oxide superconducting thin film is thick, and to provide a manufacturing method thereof.SOLUTION: The method of manufacturing the oxide superconducting thin film in which nanoparticles are provided in layers at predetermined intervals includes alternately performing: an oxide superconducting layer producing process of applying an organic metal compound solution and performing calcination heat treatment and main burning treatment to produce an oxide superconducting layer having a predetermined thickness; and a nanoparticle depositing process of depositing the nanoparticles on the oxide superconducting layer by using a solution of the nanoparticles. The method of manufacturing the oxide superconducting thin film includes: alternately performing a calcined film producing process of applying an organic metal compound solution and performing calcination heat treating to produce a calcined film having a predetermined thickness, and a nanoparticle depositing process of depositing the nanoparticles on the calcined film by using the solution of the nanoparticles; and subsequently performing main burning treatment.
摘要翻译：要解决的问题：即使氧化物超导薄膜较厚，也可提供其中Jc不降低且对应于膜厚度的Ic具有高Ic的氧化物超导薄膜，并提供其制造方法。解决方案：制备其中纳米颗粒以预定间隔设置的氧化物超导薄膜的方法包括交替执行：施加有机金属化合物溶液并进行煅烧热处理和主要燃烧处理的氧化物超导层制备方法以产生具有预定厚度的氧化物超导层; 以及通过使用纳米颗粒的溶液将纳米颗粒沉积在氧化物超导层上的纳米颗粒沉积工艺。制造氧化物超导薄膜的方法包括：交替地进行施加有机金属化合物溶液的煅烧膜制备方法并进行煅烧热处理以制备具有预定厚度的煅烧膜，以及将纳米颗粒沉积到纳米颗粒沉积工艺上通过使用纳米颗粒的溶液的煅烧膜; 并进行主燃烧处理。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP2007087813A Bi-BASED SUPERCONDUCTOR AND MANUFACTURING METHOD THEREOF, Bi-BASED SUPERCONDUCTIVE WIRE, AND Bi-BASED SUPERCONDUCTIVE EQUIPMENT 有权
标题翻译：双基超导体及其制造方法，双基超导线和双基超导设备
公开(公告)号：JP2007087813A
公开(公告)日：2007-04-05
申请号：JP2005276250
申请日：2005-09-22
申请人： Sumitomo Electric Ind Ltd , 住友電気工業株式会社
发明人： YAMAZAKI KOHEI , KOBAYASHI SHINICHI , KATO TAKESHI , SHIMOYAMA JUNICHI
IPC分类号： H01B12/02 , C01G1/00 , C01G29/00 , H01B12/10 , H01B13/00
CPC分类号： Y02E40/641 , Y02E40/644
摘要： PROBLEM TO BE SOLVED: To provide a superconductor and a superconductive wire having a high critical temperature and high critical current density and containing (Bi, Pb) 2223.
SOLUTION: In a Bi-based superconductor comprising a superconductive phase and a non-superconductive one, the superconductive phase contains (Bi, Pb) 2223, ratio obtained from the comparison of diffraction peak strength by XRD to the (Bi, Pb) 2223 in a Pb compound in the non-superconductive phase is 6% or smaller, and the critical current density at 77K, 0T is higher than 310 A/mm
2 . Oxygen partial pressure x (kPa) and an anneal temperature y (°C) in an anneal process are present in a region (including the segment of each expression) surrounded by segments (1-1) to (1-6) in Fig.1.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供具有高临界温度和高临界电流密度并含有（Bi，Pb）2223的超导体和超导线。解决方案：在包括超导相的Bi基超导体和非超导性超导相，含有（Bi，Pb）2223的超导相比，通过XRD对非超导相Pb化合物中的（Bi，Pb）2223的衍射峰强度的比较得到的比例为6％或更小，并且77K，0T的临界电流密度高于310A / mm 2 。退火过程中的氧分压x（kPa）和退火温度y（℃）存在于由图1中的段（1-1）至（1-6）包围的区域（包括每个表达式的段）中。 1。版权所有（C）2007，JPO＆INPIT

3. 发明专利

JP2012174567A Oxide superconductive wire material and manufacturing method thereof 审中-公开
标题翻译：氧化物超导线材及其制造方法
公开(公告)号：JP2012174567A
公开(公告)日：2012-09-10
申请号：JP2011036560
申请日：2011-02-23
申请人： Sumitomo Electric Ind Ltd , National Institute Of Advanced Industrial & Technology , 住友電気工業株式会社 , 独立行政法人産業技術総合研究所
发明人： HONDA GENKI , NAGAISHI TATSUOKI , NAKANISHI TAKESHI , OKI YASUTARO , YAMAGUCHI TAKASHI , HANAFUSA KEI , YAMAGUCHI IWAO , MANABE TAKAAKI , KUMAGAI TOSHIYA , SHIMOYAMA JUNICHI
IPC分类号： H01B13/00 , C01G1/00 , H01B12/06 , H01F6/06 , H01L39/24
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide an oxide superconductive wire material in which, even though a lamination is thick, Jc is not reduced and an oxide superconducting layer having a sufficiently high Ic proportional to the thickness the lamination is formed on a substrate plate, and provide a manufacturing method of the oxide superconductive wire material.SOLUTION: A manufacturing method for an oxide superconductive wire material in which organic metallic compound is used as raw material and an oxide superconducting layer is formed by a coating pyrolysis method on an orientation metal substrate, includes a coating film forming process for forming a coating film of the organic metallic compound, a temporary baking treatment process for forming a temporary baked film by pyrolyzing and removing organic components contained in the coating film, and a formal baking treatment process for forming a formal baked film by crystallizing the temporary baked film. The coating film forming process, the temporary baking treatment process, and the formal baking treatment process are repeated so as to form and stack a plurality of formal baked films, so that the oxide superconducting layer in which a defective layer is formed between the stacked films is formed. An oxide superconductive wire material has a plurality of formal baked films which are stacked via a defective layer by the coating pyrolysis method.
摘要翻译：要解决的问题：提供一种氧化物超导线材料，其中即使层压较厚，Jc也不会被还原，并且具有足够高的Ic的氧化物超导层与叠片形成在衬底上的厚度成正比并提供氧化物超导线材的制造方法。解决方案：通过在取向金属基板上的涂层热解法形成其中使用有机金属化合物作为原料的氧化物超导线材料的制造方法和氧化物超导层，包括用于形成的涂膜形成工艺有机金属化合物的涂膜，通过热解除去包含在涂膜中的有机成分来形成临时烘烤膜的临时烘烤处理工艺和通过使临时烘烤膜结晶形成正式烘烤膜的正式烘烤处理过程。重复涂膜形成过程，临时烘烤处理过程和正式烘烤处理过程，以形成和堆叠多个正式烘烤膜，使得在层叠膜之间形成有缺陷层的氧化物超导层形成了。氧化物超导线材具有通过涂层热解法通过不良层堆叠的多个正式烘烤膜。版权所有（C）2012，JPO＆INPIT

4. 发明专利

JP2012113864A Superconducting rebco oxide thin film and method for manufacturing the same 有权
标题翻译：超导氧化物薄膜及其制造方法
公开(公告)号：JP2012113864A
公开(公告)日：2012-06-14
申请号：JP2010260114
申请日：2010-11-22
申请人： National Institute Of Advanced Industrial & Technology , Sumitomo Electric Ind Ltd , 住友電気工業株式会社 , 独立行政法人産業技術総合研究所
发明人： NAGAISHI TATSUOKI , OKI YASUTARO , YAMAGUCHI IWAO , SOMA MITSUGI , MANABE TAKAAKI , KUMAGAI TOSHIYA , SHIMOYAMA JUNICHI , MUKODA MASASHI
IPC分类号： H01B13/00 , C01G1/00 , C01G3/00 , C23C28/04 , H01B12/06
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a superconducting oxide thin film offering sufficiently high Ic with stability by thickening the film by a fluorine-free metal organic deposition (FF-MOD) method.SOLUTION: The method for manufacturing a superconducting REBCO oxide thin film comprises the steps of making a superconducting oxide layer by calcining a coating film of a fluorine-free metal organic compound solution and applying firing treatment to the calcined film by a MOD method; forming a non-superconducting material layer on the superconducting oxide layer; and making a dispersion layer by making a superconducting oxide layer on the non-superconducting material layer by the MOD method and dispersing the product of a chemical reaction between the non-superconducting material and the superconducting oxide layer caused by heat applied at the manufacture of the superconducting oxide layer to work as pins. The superconducting REBCO oxide thin film comprises the plurality of superconducting oxide layers made by the MOD method, and contains a dispersion layer made by dispersing the non-superconducting material to work as pins, between the superconducting oxide layers.
摘要翻译：要解决的问题：提供一种通过无氟金属有机沉积（FF-MOD）方法通过使膜增厚而使稳定性提供足够高的Ic的超导氧化物薄膜的制造方法。解决方案：制造超导REBCO氧化物薄膜的方法包括以下步骤：通过煅烧无氟金属有机化合物溶液的涂膜并通过MOD方法对煅烧膜进行焙烧处理来制造超导氧化物层 ; 在超导氧化物层上形成非超导材料层; 以及通过MOD法在非超导材料层上制造超导氧化物层并分散在超导材料与超导氧化物层之间产生的化学反应的产物，从而制造分散层，超导氧化物层作为引脚工作。超导REBCO氧化物薄膜包括通过MOD方法制成的多个超导氧化物层，并且包含通过将非超导材料分散成在超导氧化物层之间作为引脚而制成的分散层。版权所有（C）2012，JPO＆INPIT

5. 发明专利

JP2012064394A Method for manufacturing oxide superconductive thin film 审中-公开
标题翻译：氧化物超导薄膜的制造方法
公开(公告)号：JP2012064394A
公开(公告)日：2012-03-29
申请号：JP2010206697
申请日：2010-09-15
申请人： National Institute Of Advanced Industrial & Technology , Sumitomo Electric Ind Ltd , 住友電気工業株式会社 , 独立行政法人産業技術総合研究所
发明人： HONDA GENKI , NAGAISHI TATSUOKI , YAMAGUCHI IWAO , MANABE TAKAAKI , SHIMOYAMA JUNICHI
IPC分类号： H01B13/00 , C01G1/00 , C01G3/00 , H01B12/06
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing an oxide superconductive thin film, capable of obtaining a thick-film type oxide superconductive thin film formed by sintering a plurality of preliminary sintered films laminated and having a sufficiently high critical current value Ic.SOLUTION: A method for manufacturing an RE123-based (where RE is a rare earth element) oxide superconductive thin film used for manufacturing a superconductive wire rod by an application thermal decomposition method comprises: a preliminary-sintered-film forming step of forming preliminary sintered films having a plurality of films laminated by repeating several times, applying a raw material solution onto a base material and preliminary sintering the applied film; and an oxide-superconductive-thin-film forming step of forming the oxide superconductive thin film by sintering the preliminary sintered films. In the method for manufacturing the oxide superconductive thin film, the raw material solution having a ratio of RE, Ba and Cu deviating from a stoichiometric ratio is used for forming a first layer of the applied film provided on a surface of the base material.
摘要翻译：要解决的问题：为了提供一种制造氧化物超导薄膜的方法，能够获得通过烧结多个预先烧结的薄膜而形成的厚膜型氧化物超导薄膜，并且具有足够高的临界电流值我知道了。解决方案：通过应用热分解方法制造用于制造超导线材的RE123基（其中RE是稀土元素）氧化物超导薄膜的方法包括：预烧结膜形成步骤形成通过重复多次层叠多个膜的初步烧结膜，将原料溶液施加到基材上并预涂烧所述膜; 以及通过烧结预烧结膜来形成氧化物超导薄膜的氧化物超导薄膜形成步骤。在制造氧化物超导薄膜的方法中，使用偏离化学计量比的具有RE，Ba和Cu的比率的原料溶液来形成设置在基材表面上的涂布膜的第一层。版权所有（C）2012，JPO＆INPIT

6. 发明专利

JP2007031266A Bi-BASE SUPERCONDUCTOR AND ITS MANUFACTURING METHOD, SUPERCONDUCTING WIRE MATERIAL AND SUPERCONDUCTING DEVICE 有权
标题翻译：双相超导体及其制造方法，超导材料和超导体器件
公开(公告)号：JP2007031266A
公开(公告)日：2007-02-08
申请号：JP2006163869
申请日：2006-06-13
申请人： Sumitomo Electric Ind Ltd , 住友電気工業株式会社
发明人： SHIMOYAMA JUNICHI , YAMAZAKI KOHEI , KOBAYASHI SHINICHI , KATO TAKESHI
IPC分类号： C01G1/00 , C01G29/00 , H01B12/10 , H01B13/00 , H01F6/06
CPC分类号： Y02E40/644
摘要： PROBLEM TO BE SOLVED: To provide a Bi-base superconductor having a critical temperature of higher than 110.0 K and to provide its manufacturing method. SOLUTION: The Bi-base superconductor contains (Bi, Pb) 2223 as a superconducting phase and has a first critical temperature of 110.0 K or above, at which temperature a magnetic susceptibility measured in a state in which a magnetic field is applied in a direction parallel with a c axis of the (Bi, Pb) 2223 and standardized at 95 K is -0.001. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供临界温度高于110.0K的Bi基超导体并提供其制造方法。解决方案：Bi基超导体包含（Bi，Pb）2223作为超导相，并且具有110.0K以上的第一临界温度，在该温度下，在施加磁场的状态下测量的磁化率在与（Bi，Pb）2223的ac轴平行的方向上并且在95K标准化的方向为-0.001。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2006127898A Sintered body, manufacturing method of sintered body, superconductive wire rod, superconductive apparatus, and manufacturing method of superconductive wire rod 审中-公开
标题翻译：烧结体，烧结体，超导线，超导电极的制造方法及超导线的制造方法
公开(公告)号：JP2006127898A
公开(公告)日：2006-05-18
申请号：JP2004314226
申请日：2004-10-28
申请人： Sumitomo Electric Ind Ltd , 住友電気工業株式会社
发明人： SHIMOYAMA JUNICHI , KATO TAKESHI
IPC分类号： H01B13/00 , C01B35/04 , C01G1/00 , C04B35/58 , H01B12/10
CPC分类号： C04B35/58 , B82Y30/00 , C04B35/58057 , C04B35/653 , C04B2235/3821 , C04B2235/3826 , C04B2235/401 , C04B2235/421 , C04B2235/5454 , C04B2235/77 , C04B2235/94 , C04B2235/96 , H01L39/141 , H01L39/2487 , Y10T428/12014
摘要： PROBLEM TO BE SOLVED: To provide a sintered body capable of enhancing critical current density, a manufacturing method of the sintered body, a superconductive wire rod, a superconductive apparatus, and a manufacturing method of the superconductive wire rod. SOLUTION: This manufacturing method of the sintered body containing Mg and B is provided with a disposition process to dispose Mg powder 3a, 3b and B powder 2 without mixing them each other, and a heat treatment process to apply heat treatment to Mg powder 3a, 3b and B powder 2 after the disposition process. In addition, the temperature in the heat treatment process is not less than 651°C and not more than 1,107°C. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种能够提高临界电流密度的烧结体，烧结体的制造方法，超导线材，超导装置以及超导线材的制造方法。解决方案：含有Mg和B的烧结体的制造方法具有不混合Mg粉末3a，3b和B粉末2的配置处理，并且对Mg进行热处理的热处理工序粉末3a，3b和B粉末2。此外，热处理工序中的温度不低于651℃且不大于1,107℃。版权所有（C）2006，JPO＆NCIPI

8. 发明专利

JP2012230869A Oxide superconducting thin film wiring material, and method of manufacturing the same 有权
标题翻译：氧化物超薄薄膜接线材及其制造方法
公开(公告)号：JP2012230869A
公开(公告)日：2012-11-22
申请号：JP2011100010
申请日：2011-04-27
申请人： Sumitomo Electric Ind Ltd , 住友電気工業株式会社 , National Institute Of Advanced Industrial & Technology , 独立行政法人産業技術総合研究所
发明人： HONDA GENKI , NAGAISHI TATSUOKI , NAKANISHI TAKESHI , OKI YASUTARO , YAMAGUCHI TAKASHI , HANAFUSA KEI , MANABE TAKAAKI , KUMAGAI TOSHIYA , YAMAGUCHI IWAO , SHIMOYAMA JUNICHI , MUKODA MASASHI
IPC分类号： H01B13/00 , C01G1/00 , C01G3/00 , H01B12/06
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide an oxide superconducting thin film wiring material of stable quality which has a good adhesion with an oxide superconducting layer, and has a silver layer formed thereon, which works as a protection layer sufficiently, and a method of manufacturing the same.SOLUTION: The method for manufacturing an oxide superconducting thin film wiring material comprises: the step of forming an oxide superconducting layer on an orientated metal substrate; the step of applying a silver-containing material solution to a surface of the oxide superconducting layer and then forming a silver particle-containing oxide superconducting layer so that silver particles are partially exposed from the surface by MOD method; and the step of forming, as a protection layer, a silver layer on the silver particle-containing oxide superconducting layer. The oxide superconducting thin film wiring material comprises: an orientated metal substrate; an oxide superconducting layer formed on the orientated metal substrate; a silver particle-containing oxide superconducting layer which is formed on the oxide superconducting layer so that silver particles are partially exposed from the surface; and a silver layer formed on the silver particle-containing oxide superconducting layer, which serves as a protection layer.
摘要翻译：要解决的问题：提供一种质量稳定的氧化物超导薄膜布线材料，其与氧化物超导层具有良好的粘附性，并且其上形成有银层，充分地用作保护层，以及方法的制造相同。解决方案：制造氧化物超导薄膜布线材料的方法包括：在取向的金属基板上形成氧化物超导层的步骤; 将含银材料溶液施加到氧化物超导层的表面上，然后形成含银颗粒的氧化物超导层，使得银颗粒通过MOD方法从表面部分暴露出来的步骤; 以及在含有银颗粒的氧化物超导层上形成作为保护层的银层的步骤。氧化物超导薄膜布线材料包括：定向金属基板; 形成在取向金属基板上的氧化物超导层; 形成在氧化物超导层上的含银颗粒的氧化物超导层，使得银颗粒从表面部分露出; 以及形成在作为保护层的含有银粒子的氧化物超导层上形成的银层。版权所有（C）2013，JPO＆INPIT

9. 发明专利

JP2009289502A CERAMIC SHEET, MANUFACTURING METHOD FOR Bi2223 OXIDE SUPERCONDUCTIVE WIRE, AND Bi2223 OXIDE SUPERCONDUCTIVE WIRE 审中-公开
标题翻译：陶瓷片，Bi2223氧化物超导线的制造方法和Bi2223氧化物超导线
公开(公告)号：JP2009289502A
公开(公告)日：2009-12-10
申请号：JP2008138830
申请日：2008-05-28
申请人： Sumitomo Electric Ind Ltd , 住友電気工業株式会社
发明人： SHIMOYAMA JUNICHI , AYAI NAOKI
IPC分类号： H01B13/00 , C01G1/00 , C01G29/00 , H01B12/10 , H01F6/06
CPC分类号： Y02E40/644
摘要： PROBLEM TO BE SOLVED: To provide a heat-treating member for generating effective Bi vapor during heat treatment in order to manufacture a long Bi2223 oxide superconductive wire having a high critical current value, and to provide a manufacturing method for a Bi2223 oxide superconductive wire using the heat-treating member. SOLUTION: In the manufacturing method for the Bi2223 oxide superconductive wire, a ceramic sheet for heat-treatment of the Bi2223 oxide superconductive wire, the ceramic sheet being formed with a binder made of a material vanishing through its gasifying by the heat-treatment, ceramic fibers and oxide including Bi, and a precursor Bi2223 oxide superconductive wire, are wound and heat-treated together. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：为了提供一种用于在热处理期间产生有效的Bi蒸气的热处理构件，以便制造具有高临界电流值的长Bi2223氧化物超导线，并且提供Bi2223氧化物的制造方法超导线使用热处理部件。解决方案：在Bi2223氧化物超导线的制造方法中，用于对Bi2223氧化物超导线进行热处理的陶瓷片，陶瓷片由具有由通过热交换器气化而消失的材料制成的粘合剂形成，处理，陶瓷纤维和包括Bi的氧化物和前体Bi2223氧化物超导线一起被卷绕和热处理。版权所有（C）2010，JPO＆INPIT

10. 发明专利

JP2012129084A Oxide superconductive thin film wire rod manufacturing method 审中-公开
标题翻译：氧化物超导薄膜生产线制造方法
公开(公告)号：JP2012129084A
公开(公告)日：2012-07-05
申请号：JP2010280105
申请日：2010-12-16
申请人： National Institute Of Advanced Industrial & Technology , Sumitomo Electric Ind Ltd , 住友電気工業株式会社 , 独立行政法人産業技術総合研究所
发明人： HANAFUSA KEI , NAKANISHI TAKESHI , HONDA GENKI , NAGAISHI TATSUOKI , YAMAGUCHI IWAO , KUMAGAI TOSHIYA , MANABE TAKAAKI , SHIMOYAMA JUNICHI
IPC分类号： H01B13/00 , C01G1/00 , H01B12/06 , H01L39/24
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method of an oxide superconductive thin film wire rod which, in manufacturing an oxide superconductive thin film wire rod by an MOD process, restrains a heterogeneous phase from being formed on an orientated metal substrate to ensure that an oxide superconductive thin film wire rod having desired superconducting characteristics will be manufactured.SOLUTION: A manufacturing method of an oxide superconductive thin film wire rod involves forming an oxide superconductive thin film from a metal organic compound by an application thermal decomposition process using an atmosphere furnace to manufacture an oxide superconductive thin film wire rod. The manufacturing method comprises a coated film making step in which a solution of a metal organic compound is applied to an orientated metal substrate having an intermediate layer formed therein to make a coated film, a temporary calcining step in which organic components contained in the metal organic compound of the coated film are removed by thermal decomposition to make a temporarily calcined film, and a formal calcining step in which the temporarily calcined film is crystallized to make an oxide superconductive thin film. The formal calcining step is a heat treatment step in which formal calcining is carried out under a low oxygen partial pressure and high temperature atmosphere, after which, in a region other than an oxide superconductor decomposition region, operation is performed to reduce oxygen partial pressure while the temperature is lowered to cool.
摘要翻译：解决的问题：提供一种氧化物超导薄膜线材的制造方法，其在通过MOD工艺制造氧化物超导薄膜线材时抑制在取向的金属基板上形成非均匀相，确保制造具有期望的超导特性的氧化物超导薄膜线材。解决方案：氧化物超导薄膜线材的制造方法包括通过使用气氛炉的施加热分解方法从金属有机化合物形成氧化物超导薄膜，以制造氧化物超导薄膜线材。制造方法包括：涂膜制作步骤，其中将金属有机化合物的溶液施加到其中形成有中间层的定向金属基材上以制备涂膜;临时煅烧步骤，其中有机组分包含在金属有机通过热分解除去涂膜的化合物以制备临时煅烧的膜，并且将临时煅烧的膜结晶以制备氧化物超导薄膜的正式煅烧步骤。正式煅烧步骤是在低氧分压和高温气氛下进行正式煅烧的热处理步骤，然后在氧化物超导体分解区域以外的区域中进行操作以降低氧分压，同时将温度降低冷却。版权所有（C）2012，JPO＆INPIT

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