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1. 发明专利

JPS5365884A PREPARATION OF 44MORPHOLINOOANILINEE33SULPHONEAMIDES 失效
公开(公告)号：JPS5365884A
公开(公告)日：1978-06-12
申请号：JP14195576
申请日：1976-11-26
申请人： PENTEL KK
发明人： BOU DENKICHI , IWATA MASAHIRO , NAGAHAMA MASAMITSU , IIZUKA SAYOKO
IPC分类号： C07D295/12 , C07D217/06 , C07D265/28
摘要： PURPOSE:4-Morpholinoaniline-3-sulphoneamides of formula I(R1-2 are H, alkyl, aralkyl, alkylol, aryl, piperidine, morpholino piperazine or pyrrolidine).

2. 发明专利

JPS58209867A MANUFACTURE OF AIR ELECTRODE 失效
公开(公告)号：JPS58209867A
公开(公告)日：1983-12-06
申请号：JP9255682
申请日：1982-05-31
申请人： PENTEL KK
发明人： DEGUCHI KATSUO , TOYAMA TAKESHI , BOU DENKICHI
IPC分类号： H01M4/88 , H01M4/90
摘要： PURPOSE:To make adhere highly concentrated metal phthalocyanine by immersing carbon in an alcohol solution of lithium phthalocyanine and treating it in an alcohol solution of a metal salt. CONSTITUTION:In making adhere metal phthalocyanine on carbon, lithium phthalocyanine is made to adhere on carbon, then they are treated in a solution prepared by dissolving metal chloride, bromide, iodide, or sulfate in alcohol, dimethylformamide, or methylsulfoxide to convert lithium phthalocyanine to metal phthalocyanine. By this process, phthalocyanine of noble metal such as sulver, platinum, palladium, or rhodium can be easily made to adhere on carbon. And phthalocyanine of transition metal such as nickel, cobalt, chromium, iron, or copper can be made to adhere to carbon.

3. 发明专利

JPS5875776A AIR ELECTRODE 失效
公开(公告)号：JPS5875776A
公开(公告)日：1983-05-07
申请号：JP17392781
申请日：1981-10-30
申请人： PENTEL KK
发明人： DEGUCHI KATSUO , BOU DENKICHI , OOTAGURO KUNIHIKO
IPC分类号： H01M4/88 , H01M4/90
摘要： PURPOSE:In an air electrode having excellent polarization characteristic, to adsorb the metal phthalocyanine to the surface of a carbon member, by solving the metal phthalocyanine having the alkyl-amino-methyl group into the water solution of low cendensation volatile acid and after impregnating the carbon material and drying heating it to disperse the volatile acid. CONSTITUTION:Phthalocyanine of iron, nickel, cobalt, copper, etc. is preferable as the metal phthalocyanine while the mono-methyle amino-methyl, dimethyl amino-methyl, monoethyl amino-methyl, diethyl amino-methyl group is preferable as the alkyl amino methyl group. The inorganic acid such as the hydrochloric acid or the organic acid such as the formic acid or the acetic acid is employed as the volatile acid to be dispersed at the temperature of 150-200 deg.C. Since the metal phthalocyanine is fixed uniformly and rigidly on the surface of a carbon member in the air electrodes 2, 3, the polarization characteristic of the air electrode is excellent.

4. 发明专利

JPS5875775A AIR ELECTRODE 失效
公开(公告)号：JPS5875775A
公开(公告)日：1983-05-07
申请号：JP17392681
申请日：1981-10-30
申请人： PENTEL KK
发明人： DEGUCHI KATSUO , BOU DENKICHI
IPC分类号： H01M4/90
摘要： PURPOSE:In an air electrode to be employed for an air cell or a fuel cell, to improve the catalytic performance by performing the oxidizing condensation on a metal phthalocyanine which functions as a catalyst thus performing one kind of polymerization and increasing the molecular weight. CONSTITUTION:When performing the polymarization through -N=N- coupling, the tetra-nitro is reduced by the soda sulfide is case of the copper phthalocyanine or performed directly of the amination by the hydroxylamine to produce the polyamino copper phthalocyanine then it is treated by an oxidizing agent to produce a oxidized condensate. Said condensate is molded together with a carbon material or adsorbed to a molded carbon material to produce an air electrode. A kind of carbon black, active carbon, graphite, etc. or their compound is preferable as the carbon material. 1-20wt% of the oxidized condensate is preferable when considering the performance or the strength.

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