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1. 发明专利

JP2012193418A Method for producing ferrioxide-containing metal composite nickel nanoparticles, and ferrioxide-containing metal composite nickel nanoparticle 有权
标题翻译：含有含氧化铵的金属复合镍基纳米粒子的制备方法，含有金属氧化物的金属复合镍基纳米粒子
公开(公告)号：JP2012193418A
公开(公告)日：2012-10-11
申请号：JP2011058706
申请日：2011-03-17
申请人： Nippon Steel Chem Co Ltd , Osaka Univ , Iwatani Internatl Corp , 国立大学法人大阪大学 , 岩谷産業株式会社 , 新日鐵化学株式会社
发明人： INOUE SHUJI , YAMADA KATSUHIRO , NOMOTO HIDEAKI , YAMAUCHI TOMOHISA , WADA YUJI , TSUKAHARA YASUNORI , KAWABATA RYOJI , OKUMURA HARUKI
IPC分类号： B22F9/24 , B22F1/00 , C22C19/03
摘要： PROBLEM TO BE SOLVED: To obtain, in a liquid phase reaction technique, nickel nanoparticles having a properly high sintering temperature while securing proper size and distribution of the particle size.SOLUTION: The method for producing ferrioxide-containing metal composite nickel nanoparticles includes: a complexing reaction solution generation step of heating a mixture of nickel carboxylate, iron salt and primary amine to a temperature within the range of 100-165°C to obtain a reaction solution; and a nanoparticle slurry generation step of heating the reaction solution to a temperature of 170°C or higher by microwave irradiation to obtain a metal composite nickel nanoparticle slurry containing ferrioxide. In the nanoparticle containing ferrioxide, the total amount of nickel element, iron element and oxygen element is 95 pts.mass or more relative to 100 pts.mass of the metal composite nickel nanoparticle, the amount of iron element is within the range of 5-50 pts.mass relative to 100 pts.mass of the total amount of nickel element and iron element, the average particle size is within the range of 30-150 nm, and the ferrioxide is mainly composed of triiron tetraoxide.
摘要翻译：要解决的问题为了在液相反应技术中获得具有适当高的烧结温度的镍纳米颗粒，同时确保了适当的粒度和粒度的分布。解决方案：含有氧化亚铁的金属复合镍纳米颗粒的制造方法包括：将羧酸镍，铁盐和伯胺的混合物加热到100-165℃的温度范围内的络合反应溶液生成步骤，获得反应溶液; 以及通过微波照射将反应溶液加热至170℃以上的纳米粒子浆料生成工序，得到含有二氧化碳的金属复合镍纳米粒子浆料。在含有三氧化二铁的纳米粒子中，镍元素，铁元素和氧元素的总量比金属复合镍纳米粒子的100质量份高95个或更多，铁元素的量在5- 相对于镍元素和铁元素总量的100pts.mass，平均粒径为30〜150nm，氧化铁主要由四氧化三铁构成。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP2013007070A Apparatus and method of continuously producing nickel nanoparticles 审中-公开
标题翻译：连续生产镍基纳米粒子的装置及方法
公开(公告)号：JP2013007070A
公开(公告)日：2013-01-10
申请号：JP2011138767
申请日：2011-06-22
申请人： Nippon Steel & Sumikin Chemical Co Ltd , 新日鉄住金化学株式会社 , Osaka Univ , 国立大学法人大阪大学 , Iwatani Internatl Corp , 岩谷産業株式会社
发明人： YAMADA KATSUHIRO , NOMOTO HIDEAKI , INOUE SHUJI , TAKEKOSHI TETSUHITO , HIGUCHI MASAKAZU , KONO TAKUMI , TSUKAHARA YASUNORI , YAMAUCHI TOMOHISA , WADA YUJI , OKUMURA HARUKI
IPC分类号： B22F9/24 , H01B13/00
摘要： PROBLEM TO BE SOLVED: To provide a practically useful continuous production apparatus and continuous production method, capable of synthesizing nickel nanoparticles in a large amount.SOLUTION: In the continuous production apparatus 100, raw materials namely a complexed reaction solution and a metal salt are continuously or intermittently supplied via a raw material introduction member 1B into a reaction vessel 1 separately or in a mixed state. A microwave generated by a microwave generating part 10 is introduced into the reaction vessel 1 from a microwave introduction part 1A to irradiate a mixed reaction solution comprising nickel acetate and a metal salt. Thereby, the metal salt is reduced by heating to form fine particles of metal such as silver, and nickel acetate is reduced to allow metallic nickel to grow on nuclei, i.e., the resulting fine particles, whereby nickel nanoparticles are formed.
摘要翻译：要解决的问题：提供能够大量合成镍纳米颗粒的实用有用的连续制备装置和连续制备方法。解决方案：在连续生产设备100中，将原料即复合反应溶液和金属盐经由原料引入构件1B连续或间歇地分别供入反应容器1或混合状态。由微波产生部10产生的微波从微波导入部1A引入反应容器1，照射包含乙酸镍和金属盐的混合反应液。由此，金属盐通过加热而还原，形成细小的金属如银，并且还原乙酸镍以使金属镍在核上生长，即所得细小颗粒，从而形成镍纳米颗粒。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2013013862A Biofiltration material for cleaning treatment of organic wastewater 审中-公开
标题翻译：用于清洁有机废水处理的生物材料
公开(公告)号：JP2013013862A
公开(公告)日：2013-01-24
申请号：JP2011148991
申请日：2011-07-05
申请人： Iwatani Internatl Corp , 岩谷産業株式会社
发明人： OKUMURA HARUKI , KOIKE KUNIHIKO , INOUE GOICHI , NAKAGAWA MASAMI
IPC分类号： C02F3/10 , B01D39/14 , C01B25/32
CPC分类号： Y02W10/15
摘要： PROBLEM TO BE SOLVED: To provide a biofiltration material for eliminating organic matter in water cleaning treatment by chemically bonding biocompatible particles with biocompatibility to a base material.SOLUTION: A surface treatment comprising at least one method selected from acid, alkali, ozone, ozone water, ozone bubbling, plasma, corona discharge and ultraviolet irradiation is applied onto the organic or inorganic base material to produce a reactive functional group such as a hydroxy group or a carboxyl group, and a calcium phosphate sintered body (hydroxyapatite) which is biocompatible particles, is chemically bonded to the produced reactive functional group.
摘要翻译：要解决的问题：提供一种生物过滤材料，用于通过将与生物相容性的生物相容性颗粒化学键合到基材上来消除水洗处理中的有机物质。解决方案：在有机或无机基材上施加包括至少一种选自酸，碱，臭氧，臭氧水，臭氧起泡，等离子体，电晕放电和紫外线照射的方法的表面处理，以产生反应性官能团作为羟基或羧基，作为生物相容性粒子的磷酸钙烧结体（羟基磷灰石）与所生成的反应性官能团化学键合。版权所有（C）2013，JPO＆INPIT

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