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1. 发明专利

JP2010126499A Naphthalocyanine compound and method for producing the same 有权
标题翻译：萘磺酰胺化合物及其制备方法
公开(公告)号：JP2010126499A
公开(公告)日：2010-06-10
申请号：JP2008304175
申请日：2008-11-28
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： NISHIGUCHI IKUZO , HARADA AIKO , MAEKAWA HIROSHI
IPC分类号： C07D487/22 , C09B47/00
摘要： PROBLEM TO BE SOLVED: To provide a new naphthalocyanine compound which is excellent in solubility in organic solvents and can be produced in simple processes at a low cost, and to provide a method for producing the same. SOLUTION: This naphthalocyanine compound is such as 1,6,10,15,19,24,28,33-octapentyloxy-3,4,12,13,21,22,30,31-octa(4'-fluorophenyl)-37H,39H-naphthalocyanine. The compound is obtained by heating a 2,3-dicyanonaphthalene derivative such as 6,7-di(4'-fluorophenyl)-1,4-dipentyloxy-2,3-dicyanonaphthalene in the presence of metal lithium in an organic solvent. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种在有机溶剂中溶解性优异的新型萘酞菁化合物，可以以简单的方法以低成本制备，并提供其制备方法。解决方案：该萘酞菁化合物是1,6,10,15,19,24,28,33-八辛氧基-3,4,12,13,21,22,30,31-八（4'- 氟苯基）-37H，39H-萘。该化合物通过在有机溶剂中在金属锂存在下加热6,7-二（4'-氟苯基）-1,4-二戊氧基-2,3-二氰基萘等2,3-二氰基萘衍生物而得到。版权所有（C）2010，JPO＆INPIT

2. 发明专利

JP2012051812A Production method of aromatic series containing fluorine asymmetric acyloin compound 审中-公开
标题翻译：含有氟不对称铝酸盐化合物的芳族体系的生产方法
公开(公告)号：JP2012051812A
公开(公告)日：2012-03-15
申请号：JP2010193236
申请日：2010-08-31
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： MAEKAWA HIROSHI , KUDO MASASHI , NISHIGUCHI IKUZO
IPC分类号： C07C45/00 , C07C49/82 , C07D333/22
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently producing at low cost, various aromatic-containing asymmetric acyloin compounds by a simple process.SOLUTION: The production method of the aromatic-containing fluorine asymmetric acyloin compound of formula (5) is characterized in that in an organic solvent, an aldehyde compound of formula (1) is reacted with a fluorine containing ester compound of formula (2) and a silica compound of formula (3) in the existence of the reducer, an acetal compound of formula (4) is produced, and the obtained acetal compound of formula (4) is treated by using a desilylation agent. In the formulas, Ar denotes phenyl, substituted phenyl, naphthyl or five-membered heteroaromatic ring, and Rf denotes 1C-4C polyfluoroalkyl or perfluoroalkyl, and Rdenotes 1C-8C alkyl.
摘要翻译：待解决的问题：提供一种通过简单的方法以低成本高效地生产各种含芳族的不对称偶姻化合物的方法。解决方案：式（5）的含芳族的氟不对称共轭亚嗪化合物的制备方法的特征在于，在有机溶剂中，将式（1）的醛化合物与式（1）的含氟酯化合物 2）和存在还原剂的式（3）的二氧化硅化合物，制备式（4）的缩醛化合物，通过使用脱甲硅烷化剂处理得到的式（4）的缩醛化合物。在该式中，Ar表示苯基，取代的苯基，萘基或五元杂芳环，Rf表示1C-4C多氟烷基或全氟烷基，R表示1〜8个碳原子。版权所有（C）2012，JPO＆INPIT

3. 发明专利

JP2005330190A Method for producing polyfluorobenzoquinones 有权
标题翻译：生产聚氟虫腈的方法
公开(公告)号：JP2005330190A
公开(公告)日：2005-12-02
申请号：JP2004147589
申请日：2004-05-18
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： NISHIGUCHI IKUZO , MAEKAWA HIROSHI , AKIYAMA SHOICHI
IPC分类号： C07C46/02 , C07C50/24 , C07C50/28
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently and inexpensively producing polyfluorobenzoquinones by simple operation using an inexpensive raw material. SOLUTION: A polyfluorobenzene represented by general formula (1) äwherein, R 1 denotes each a hydrogen atom, a halogen atom or an OR 2 (wherein, R 2 denotes a 1-5C alkyl group)} is anodized in a mixed solvent of trifluoroacetic acid with a halogenated hydrocarbon. Thereby, the polyfluoro-1,4-benzoquinone represented by general formula (2) äwherein, R 1 and R 2 are each the same as in general formula (1)} is produced. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种通过使用廉价原料的简单操作来有效且廉价地生产多氟苯醌的方法。解决方案：由通式（1）表示的多氟苯，其中R 1表示氢原子，卤素原子或OR 2，其中R 1， SP> 2 表示1-5C烷基）}在三氟乙酸与卤代烃的混合溶剂中阳极氧化。由此，由通式（2）表示的多氟-1,4-苯醌与通式（1）中的R 1和R 2相同。生产。版权所有（C）2006，JPO＆NCIPI

4. 发明专利

JP2010235480A Naphthalocyanine compound and method for producing the same 有权
标题翻译：萘磺酰胺化合物及其制备方法
公开(公告)号：JP2010235480A
公开(公告)日：2010-10-21
申请号：JP2009083693
申请日：2009-03-30
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： NISHIGUCHI IKUZO , HARADA AIKO , MAEKAWA HIROSHI
IPC分类号： C07D491/22 , C09B47/04 , C09K3/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a naphthalocyanine compound by a simple step at a low cost.
SOLUTION: The method for producing a naphthalocyanine compound includes heating a 5,6,7,8-tetrasubstituted-1,4-dialkoxy-5,8-epoxy-2,3-dicyano-5,8-dihydronaphthalene derivative represented by formula (1) in the presence of lithium metal in an organic solvent.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种通过简单的步骤以低成本制备萘酞菁化合物的方法。解决方案：萘酞菁化合物的制备方法包括加热5,6,7,8-四取代-1,4-二烷氧基-5,8-环氧-2,3-二氰基-5,8-二氢萘衍生物通过式（1）在有机溶剂中在金属锂存在下进行。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2009132624A 2,3-dicyanonaphthalene derivative 有权
标题翻译： 2,3-DICYANONAPHTHALENE DERIVATIVE
公开(公告)号：JP2009132624A
公开(公告)日：2009-06-18
申请号：JP2007307506
申请日：2007-11-28
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： NISHIGUCHI IKUZO , HARADA AIKO , MAEKAWA HIROSHI
IPC分类号： C07C255/54
摘要： PROBLEM TO BE SOLVED: To provide a new 2,3-dicyanonaphthalene derivative substituted by various hydrocarbon groups at the fifth to eighth positions of the 2,3-dicyanonaphthalene ring.
SOLUTION: This 2,3-dicyanonaphthalene derivative is expressed by formula (1) [wherein, R
1 to R
4 are each independently a group selected from among H, a 1-8C alkyl and a group expressed by -C
6 H
4 X {wherein, X is a group selected from among Cl, F, CH
3 , OCH
3 , CF
3 , CN and COOR (wherein, R is a 1-6C alkyl), but at least one of the R
1 to R
4 is a group other than H}; and R
5 , R
6 are each independently a 1-12C alkyl].
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供在2,3-二氰基萘环的第五至第八位置由各种烃基取代的新的2,3-二氰基萘衍生物。解决方案：该2,3-二氰基萘衍生物由式（1）表示[其中，R“SP”至R“SP”4各自独立地选自H ，一个1-8C的烷基和一个由-C 6 S 6表示的基团X，其中X是选自Cl，F，CH 3， / SB>，OCH 3 SB 3，CF 3 SB，CN和COOR（其中，R是1-6C烷基），但R SP 1中的至少一个到R 4 是H以外的组} 和R“SP 5”，R“SP 6”各自独立地是1-12C烷基]。版权所有（C）2009，JPO＆INPIT

6. 发明专利

JP2010235592A Substituted azulene, and method of producing the same 审中-公开
标题翻译：取代的三聚氰胺及其生产方法
公开(公告)号：JP2010235592A
公开(公告)日：2010-10-21
申请号：JP2010050003
申请日：2010-03-08
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： MAEKAWA HIROSHI , NISHIGUCHI IKUZO , HONDA JUNYA
IPC分类号： C07C45/27 , C07C49/21 , C07C49/613 , C07D311/20
摘要： PROBLEM TO BE SOLVED: To provide a method of efficiently producing a substituted azulene from azulene at a low cost using a simple process.
SOLUTION: The method of producing a substituted azulene compound represented by formula (3) is characterized by allowing an azulene compound to react with an unsaturated compound in the presence of a reducing agent and a silicon compound and subsequently oxidizing the resulting compound (in the formula, R
1 to R
9 , and X each represent a hydrogen atom, an aliphatic hydrocarbon group that may contain a substituent, or the like, and Y represents an acyl group or an ester group).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种使用简单的方法以低成本有效地从薁生产取代的薁的方法。解决方案：制备由式（3）表示的取代的薁化合物的方法的特征在于使薁化合物与不饱和化合物在还原剂和硅化合物的存在下反应，随后氧化所得化合物（在式中，R 1 至R 9 ，X各自表示氢原子，可以含有取代基的脂肪族烃基等，Y表示酰基或酯基）。版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2010235589A 4-polyfluoroacylphenylalkyl ketone, and method of producing the same 审中-公开
标题翻译： 4-聚氟乙基苯甲酮酮及其生产方法
公开(公告)号：JP2010235589A
公开(公告)日：2010-10-21
申请号：JP2010044829
申请日：2010-03-02
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： MAEKAWA HIROSHI , NISHIGUCHI IKUZO , OZAKI TARO , DIANA BINTI ZULKIFLI , MURAKAMI TARO
IPC分类号： C07C45/45 , C07C49/80
摘要： PROBLEM TO BE SOLVED: To provide a method of efficiently producing a various species of 4-polyfluoroacylphenylalkyl ketones at a low cost using a simple process.
SOLUTION: A 4-polyfluoroacylphenylalkyl ketone represented by formula (4) is produced by allowing a ketone compound comprising a phenyl group or a substituted phenyl group to react with a silicon compound and an ester compound comprising a perfluoroalkyl group in an organic solvent in the presence of a reducing agent to convert the same into an acetal compound and subsequently treating the acetal compound with a desilylation agent (in the formula, R
1 represents a 1-8C alkyl group or a 3-8C cycloalkyl group, Rf represents a 1-4C poly or perfluoroalkyl group, R represents a hydrogen atom or a substituent, and n represents an integer of 1 to 4).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种以简单的方法以低成本有效地生产各种4-聚氟酰基苯基烷基酮的方法。解决方案：由式（4）表示的4-多氟酰基苯基烷基酮通过使含有苯基或取代的苯基的酮化合物与有机溶剂中的硅化合物和包含全氟烷基的酯化合物反应来制备在还原剂的存在下将其转化为缩醛化合物，并随后用脱甲硅基化剂处理缩醛化合物（在该式中，R“SP”表示1-8C烷基或3- 8C环烷基，Rf表示1-4C的多或全氟烷基，R表示氢原子或取代基，n表示1〜4的整数。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2006213617A Acetylene aldehyde, its manufacturing method, acetylene aldehyde acetal and its manufacturing method 审中-公开
标题翻译：乙烯醛，其制造方法，乙炔醛和其制造方法
公开(公告)号：JP2006213617A
公开(公告)日：2006-08-17
申请号：JP2005026303
申请日：2005-02-02
申请人： Nagaoka Univ Of Technology , Nippon Kasei Chem Co Ltd , 国立大学法人長岡技術科学大学 , 日本化成株式会社
发明人： NISHIGUCHI IKUZO , HIOKI YUJIRO
IPC分类号： C07F7/08 , C25B3/02
摘要： PROBLEM TO BE SOLVED: To provide an acetylene aldehyde which has high productivity and a small environmental load and is low-cost, and its manufacturing method.
SOLUTION: The acetylene aldehyde is represented by formula (1): R
1 R
2 R
3 Si-C≡C-CHO (wherein R
1 , R
2 and R
3 are each an alkyl group or a phenyl group, excepting that one of R
1 to R
3 is a methyl group and the remaining are phenyl groups). The method for manufacturing the acetylene aldehyde comprises subjecting an acetylene alcohol represented by formula (2): R
1 R
2 R
3 Si-C≡C-CH
2 OH (wherein R
1 , R
2 and R
3 are each an alkyl group or a phenyl group, excepting that one of R
1 to R
3 is a methyl group and the remaining are phenyl groups) to electrolytic oxidation in the presence of an oxidizing agent.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种生产率高，环境负荷小，成本低的乙炔醛及其制造方法。解决方案：乙炔醛由式（1）表示：R 1 SP 2 3 Si-C≡C-CHO （其中R 1，R 2，R 2，R 2和R 3均为烷基或苯基，除了R 1，至R 3 为甲基，其余为苯基）。制备乙炔醛的方法包括使由式（2）表示的乙炔醇：R 1 SP 1，R 2，S 2，C 3， C-CH 2，其中R 1，R 2，R 2，R 3和R 3各自为烷基或苯基，除了R“SP 1至R 3中的一个是甲基，其余为苯基）在氧化剂存在下进行电解氧化。版权所有（C）2006，JPO＆NCIPI

9. 发明专利

JP2005200310A Phthalocyanine derivative having crown ether ring in molecule and intermediate therefor 审中-公开
标题翻译：在其分子和中间体中具有环状醚的酞菁衍生物
公开(公告)号：JP2005200310A
公开(公告)日：2005-07-28
申请号：JP2004005099
申请日：2004-01-13
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： NISHIGUCHI IKUZO , MAEKAWA HIROSHI , MATSUNAMI MASATO
IPC分类号： C07D498/22
摘要： PROBLEM TO BE SOLVED: To provide a new phthalocyanine derivative containing asymmetric binaphthyl groups in crown ether rings and different benzene rings in the phthalocyanine molecule bridged with the crown ether groups and to provide a new bis(polyethylene glycol)-substituted asymmetric binaphthylbisphthalonitrile derivative to be an intermediate therefor.
SOLUTION: The phthalocyanine derivative having the crown ether rings in the molecule is represented by general formula (1) (wherein, Xs are each independently a hydrogen atom or a halogen atom; Ys are each independently a hydrogen atom or a halogen atom; Rs are each a 1-10C alkyl group; M denotes a bivalent metal; and n is 0, 2 or 3).
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种新的酞菁衍生物，其在冠醚环中的不对称联萘基和与冠醚基团桥连的酞菁分子中的不同苯环，并提供新的双（聚乙二醇）取代的非对称联萘双苯腈衍生物为其中间体。解决方案：分子中具有冠醚环的酞菁衍生物由通式（1）表示（其中，Xs各自独立地为氢原子或卤素原子; Y各自独立地为氢原子或卤素原子 ; R 5各自为1-10C烷基; M表示二价金属; n为0或2或3）。版权所有（C）2005，JPO＆NCIPI

10. 发明专利

JP2010126500A 5,6,7,8-tetra-substituted-1,4-dialkoxy-5,8-epoxy-2,3-dicyano-5,8-dihydronaphthalene derivative and its production method 有权
标题翻译： 5,6,7,8-四取代的1,4-二烷氧基-5,8-环氧-2,3-二氰基-5,8-二氢萘基衍生物及其制备方法
公开(公告)号：JP2010126500A
公开(公告)日：2010-06-10
申请号：JP2008304176
申请日：2008-11-28
申请人： Nagaoka Univ Of Technology , 国立大学法人長岡技術科学大学
发明人： NISHIGUCHI IKUZO , HARADA AIKO , MAEKAWA HIROSHI
IPC分类号： C07D493/08
摘要： PROBLEM TO BE SOLVED: To provide a new 5,6,7,8-tetra-substituted-1,4-dialkoxy-5,8-epoxy-2,3-dicyano-5,8-dihydronaphthalene derivative (1) in which the 5 to 8-positions of the 2,3-dicyanonaphthalene ring are substituted with various kinds of hydrocarbon groups or the like, and to provide its production method. SOLUTION: A furan compound is reacted with a 2,3-dicyanobenzene derivative in the presence of metal magnesium to obtain the naphthalene derivative (1). COPYRIGHT: (C)2010,JPO&INPIT

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