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1. 发明专利

JP2007254236A Black composite oxide particle, its production method, black slurry, black paste, and black matrix 有权
标题翻译：黑色复合氧化物颗粒，其生产方法，黑色浆料，黑色浆料和黑色矩阵
公开(公告)号：JP2007254236A
公开(公告)日：2007-10-04
申请号：JP2006083963
申请日：2006-03-24
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： KATSUYAMA KOICHI , HOSHINO TOMOYUKI , FUJIYASU SHOICHI , SHIMAMURA HIROYUKI
IPC分类号： C01G51/00 , C09C1/00 , C09D17/00
摘要： PROBLEM TO BE SOLVED: To provide a material which, when used as a black pigment based on a metal oxide, is excellent in a degree of blackness, hue, dispersibility in the case of use for coating materials, and surface smoothness shown by a coating film made from a coating material containing it, and has a sharp primary particle size distribution in spite of being in a microparticulate form.
SOLUTION: The particulate black composite oxide particles comprise 60 to 80 mass% cobalt and 0.1 to 5 mass% manganese and has an average primary particle diameter of 0.05 to 0.3 μm (as measured by observation with a scanning electron microscope (SEM)).
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种当用作基于金属氧化物的黑色颜料时，在涂覆材料的使用情况下的黑色度，色调，分散性以及表面平滑度方面优异的材料通过由含有它的涂层材料制成的涂膜，并且尽管是微粒形式，但具有尖锐的初级粒度分布。解决方案：颗粒状黑色复合氧化物颗粒包含60至80质量％的钴和0.1至5质量％的锰，并且平均初级粒径为0.05至0.3微米（通过用扫描电子显微镜（SEM）观察测量））。版权所有（C）2008，JPO＆INPIT

2. 发明专利

JP2006306712A Composite oxide particle having black color 有权
标题翻译：具有黑色颜料的复合氧化物颗粒
公开(公告)号：JP2006306712A
公开(公告)日：2006-11-09
申请号：JP2006086441
申请日：2006-03-27
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： FUJIYASU SHOICHI , KATSUYAMA KOICHI , HOSHINO TOMOYUKI , MIWA MASAHIRO , SHIMAMURA HIROYUKI
IPC分类号： C01G51/00 , C01G53/00
摘要： PROBLEM TO BE SOLVED: To provide spinel type cobalt oxide particles having more excellent blackness and electric conductivity, and having a well balance in oxidation resistance, dispersibility when being converted into a coating material, the surface smoothness of a coating film upon the conversion of the coating material into a coating film or the like, to provide a method for producing the same, and to provide a black conductive coating material and paste.
SOLUTION: The composite oxide particles have conductivity and a black color. The particles contain one or more of copper, nickel, and molybdenum and have a cobalt content of 40 to 65 mass% in terms of the amount of the metallic element based on the whole particles.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：为了提供具有更优异的黑色和电导率的尖晶石型氧化钴颗粒，并且在耐氧化性，转化成涂料时的分散性具有良好的平衡，涂膜的表面平滑度将涂料转化成涂膜等，以提供其制备方法，并提供黑色导电涂料和糊料。解决方案：复合氧化物颗粒具有导电性和黑色。颗粒含有铜，镍和钼中的一种或多种，并且以基于整个颗粒的金属元素的量计，钴含量为40至65质量％。版权所有（C）2007，JPO＆INPIT

3. 发明专利

JP2007302798A Cobalt-containing black pigment 有权
标题翻译：含钴黑色素
公开(公告)号：JP2007302798A
公开(公告)日：2007-11-22
申请号：JP2006133267
申请日：2006-05-12
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： HOSHINO TOMOYUKI , KATSUYAMA KOICHI , FUJIYASU SHOICHI , NAKAJIMA TAKASHI , SHIMAMURA HIROYUKI
IPC分类号： C09C1/00 , C01G51/04 , C09C3/00
摘要： PROBLEM TO BE SOLVED: To provide a cobalt-containing black pigment which essentially has a black degree and high electric resistance as black pigment powder for forming light-shielding layers and black electrodes for plasma displays, plasma address liquid crystals, and the like, has a small average primary particle diameter and a small coagulated particle diameter, and is excellent in initial dispersibility.
SOLUTION: This cobalt-containing black pigment is characterized in that an average primary particle diameter is 0.03 to 0.5 μm, and D
50 by the measurement of particle sizes based on the number of particles by a laser diffraction scattering method is 0.05 to 1.5 μm.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：为了提供基本上具有黑色度和高电阻的含钴黑色颜料作为用于形成遮光层的黑色颜料粉末和用于等离子体显示器的黑色电极，等离子体寻址液晶和具有小的平均一次粒径和小的凝固粒径，并且初始分散性优异。解决方案：该含钴黑色颜料的特征在于，通过基于颗粒数量a的颗粒尺寸的测量，平均一次粒径为0.03至0.5μm，D 50 激光衍射散射法为0.05〜1.5μm。版权所有（C）2008，JPO＆INPIT

4. 发明专利

JP2007302491A Cobalt hydroxide particle and cobalt oxide particle 有权
标题翻译：碳酸氢氧化钴颗粒和氧化钴颗粒
公开(公告)号：JP2007302491A
公开(公告)日：2007-11-22
申请号：JP2006130989
申请日：2006-05-10
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： HOSHINO TOMOYUKI , KATSUYAMA KOICHI , FUJIYASU SHOICHI , SHIMAMURA HIROYUKI
IPC分类号： C01G51/04
摘要： PROBLEM TO BE SOLVED: To provide cobalt oxide particles desirable to obtain cobalt oxide particles which simultaneously satisfy a high degree of blackness and a high electrical resistance.
SOLUTION: The cobalt hydroxide particles are characterized in that the primary particle in-plane average diameter is 0.05-0.7 μm when observed by SEM (scanning electron microscopy) and the particle shape is flaky.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供期望获得同时满足高度黑色度和高电阻的氧化钴颗粒的氧化钴颗粒。解决方案：氢氧化钴颗粒的特征在于，当通过SEM（扫描电子显微镜）观察时，一次颗粒的平面直径为0.05-0.7μm，并且颗粒形状为片状。版权所有（C）2008，JPO＆INPIT

5. 发明专利

JP2005255426A Composite black oxide particle, method for producing the same, black coating material and black matrix 有权
标题翻译：复合黑氧化物颗粒，其制造方法，黑色涂料和黑色基质
公开(公告)号：JP2005255426A
公开(公告)日：2005-09-22
申请号：JP2004066201
申请日：2004-03-09
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： FUJIYASU SHOICHI , HAYASHI TOMIO , KATSUYAMA KOICHI , SHIMAMURA HIROYUKI
IPC分类号： C01G51/00 , C09C1/62 , C09C3/06 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a composite black oxide particle in which blackness, oxidation resistance, and surface smoothness in a coating film when converted into a coating material and converted into the coating film are more excellent, and which has high electric resistance as well, to provide a method for producing the same, to provide a black coating material and to provide a black matrix.
SOLUTION: The spinel type or inverse-spinel type composite black oxide particle is composed of oxides of cobalt, copper and manganese. The copper/cobalt molar ratio is 0.1 to 0.5, and the manganese/cobalt molar ratio is 0.2 to 1.0. The surface of the composite black oxide particle is coated with Al oxide. In the method for producing the composite black oxide particle, a metal salt-mixed aqueous solution prepared by using water soluble salts of cobalt, copper and manganese is neutrally mixed with an alkali hydroxide, the pH of the obtained metal hydroxide slurry is held to 10 to 13, oxidation is performed at >40 to 60°C, the obtained precursor is aged at 80 to 150°C, thereafter, a water soluble aluminum salt aqueous solution is added thereto to prepare the pH to 5 to 9, subsequently, solid-liquid separation is performed, and thereafter, heat treatment is performed at 400 to 700°C for >1 to 3 hr.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种复合黑色氧化物粒子，其中当转化成涂料并转化成涂膜时，涂膜中的黑色，抗氧化性和表面光滑度更优异，并且具有高电电阻也提供其制造方法，以提供黑色涂层材料并提供黑色矩阵。解决方案：尖晶石型或反尖晶石型复合黑色氧化物颗粒由钴，铜和锰的氧化物组成。铜/钴摩尔比为0.1〜0.5，锰/钴摩尔比为0.2〜1.0。复合黑色氧化物颗粒的表面涂有Al氧化物。在复合黑氧化物粒子的制造方法中，通过使用钴，铜和锰的水溶性盐制备的金属盐混合水溶液与碱金属氢氧化物中性混合，将得到的金属氢氧化物浆料的pH保持在10 至13℃，在40〜60℃下进行氧化，将得到的前体在80〜150℃下老化，然后向其中加入水溶性铝盐水溶液使pH为5〜9，进行液体分离，然后在400〜700℃下进行1〜3小时的热处理。版权所有（C）2005，JPO＆NCIPI

6. 发明专利

JP2007284340A Method for producing granular cobalt oxide black pigment, and granular cobalt oxide black pigment 有权
标题翻译：生产颗粒状氧化钴黑色颜料的方法和颗粒状氧化钴黑色颜料
公开(公告)号：JP2007284340A
公开(公告)日：2007-11-01
申请号：JP2007074575
申请日：2007-03-22
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： HOSHINO TOMOYUKI , KATSUYAMA KOICHI , FUJIYASU SHOICHI , NAKAJIMA TAKASHI
IPC分类号： C01G51/04 , C09C1/00 , C09C3/04
CPC分类号： C01G51/04 , C09C1/00 , C09C1/0009
摘要： PROBLEM TO BE SOLVED: To provide a method for producing granular cobalt oxide black pigment with a small grain size and a sharp grain size distribution combining excellent blackness and high electric resistivity.
SOLUTION: Regarding the method for producing granular cobalt oxide black pigment, the neutralization of a cobalt (bivalent) salt aqueous solution and an alkali solution is performed at the pH of 10 to 13, on and after the start of the mixing and neutralization or on and after the completion of the mixing and neutralization, an oxygen-containing gas is continuously bubbled while the temperature of the reaction slurry is held at 10 to 40°C, so as to obtain a cobalt hydroxide precursor, and the cobalt hydroxide precursor is subjected to filtering, washing, drying and cracking, and is thereafter fired at 500 to 850°C for 0.5 to 3 hr in a sealed atmosphere, or is fired at 500 to 850°C in an inert gas-enriched air atmosphere in which the concentration of oxygen is held to 15 to
摘要翻译：解决的问题：提供一种结合优异的黑色度和高电阻率的具有小晶粒度和尖锐的晶粒尺寸分布的颗粒状氧化钴黑色颜料的制备方法。解决方案：关于生产颗粒状氧化钴黑色颜料的方法，在混合开始和之后，在10至13的pH下进行钴（二价）盐水溶液和碱溶液的中和，和中和或在混合和中和完成之后或之后，将含氧气体连续鼓泡，同时将反应浆料的温度保持在10至40℃，以获得氢氧化钴前体，并将氢氧化钴将前体进行过滤，洗涤，干燥和裂化，然后在密封气氛中在500〜850℃下烧制0.5〜3小时，或在惰性气体富集空气气氛中在500〜850℃下烧成其中氧气的浓度保持在15至22体积％。版权所有（C）2008，JPO＆INPIT

7. 发明专利

JP2005289653A Composite black oxide particle, method for producing the same, black coating material, and black matrix 有权
标题翻译：复合黑氧化物颗粒，其制造方法，黑色涂料和黑色矩阵
公开(公告)号：JP2005289653A
公开(公告)日：2005-10-20
申请号：JP2004102539
申请日：2004-03-31
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： FUJIYASU SHOICHI , KATSUYAMA KOICHI , HOSHINO TOMOYUKI , SHIMAMURA HIROYUKI
IPC分类号： C01G53/00 , C09C1/00 , C09C3/06 , C09D7/12 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide composite black oxide particles which are excellent in blackness and flowability, and good in balance between oxidation resistance, dispersibility at the time of being used in a coating material, surface flatness of a coating formed from the coating material, and the like, and to provide a method for producing the same, a black coating material, and a black matrix.
SOLUTION: The spinel type or inverse-spinel type composite black oxide particles consist of oxides of cobalt, nickel and manganese, and has a molar ratio of nickel to cobalt of 0.2-0.6 and a molar ratio of manganese to cobalt of 0.5-1.0. The method for producing the composite black oxide particles comprises mixing an aqueous mixed solution prepared by using water-soluble metal salts of cobalt, nickel and manganese, and an alkali hydroxide so as to neutralize, then oxidizing the obtained slurry of the metal hydroxides at a temperature of >40°C to ≤60°C while keeping its pH at a value of 10-13, aging the obtained precursor at 80-150°C, subjecting the aged precursor to solid-liquid separation, and heat-treating the obtained solid at 400-700°C for >1 to ≤3 h.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供黑色度和流动性优异，耐氧化性，涂布时使用时的分散性，平滑度均匀的复合黑氧化物粒子，由涂层材料等，并提供其制造方法，黑色涂层材料和黑色矩阵。解决方案：尖晶石型或反尖晶石型复合黑氧化物颗粒由钴，镍和锰的氧化物组成，镍与钴的摩尔比为0.2-0.6，锰与钴的摩尔比为0.5 -1.0。复合黑氧化物粒子的制造方法包括将通过使用钴，镍和锰的水溶性金属盐和碱金属氢氧化物制备的水性混合溶液混合以中和，然后将所得到的金属氢氧化物的浆料在温度> 40℃至≤60℃，同时保持其pH值为10-13，将所得前体在80-150℃下老化，对老化前体进行固液分离，并将所得到的在400-700℃下固化> 1〜≤3h。版权所有（C）2006，JPO＆NCIPI

8. 发明专利

JP2005139063A Composite black oxide particle, its manufacturing method, black paint and black matrix 有权
标题翻译：复合黑氧化物颗粒，其制造方法，黑色和黑色矩阵
公开(公告)号：JP2005139063A
公开(公告)日：2005-06-02
申请号：JP2004299497
申请日：2004-10-14
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： HAYASHI TOMIO , FUJIYASU SHOICHI , KATSUYAMA KOICHI , SHIMAMURA HIROYUKI
IPC分类号： G02B5/00 , C01G51/00 , C09D7/12 , C09D201/00 , G02F1/1335
摘要： PROBLEM TO BE SOLVED: To provide a composite black oxide particle excellent in blackness, oxidation resistance, dispersibility at painting and the surface smoothness of a coated film and to provide its manufacturing method, a black paint and a black matrix. SOLUTION: The spinel-type or inverse-spinel-type composite black oxide particle consists of oxides of cobalt, copper and manganese, has a molar ratio of copper to cobalt of 0.1-0.5 and has a molar ratio of manganese to cobalt of 0.2-1.0. The method for manufacturing the composite black oxide particle is characterized in that a mixed metal salts aqueous solution prepared by water soluble salts of cobalt, copper and manganese and an alkali hydroxide are mixed for neutralization, the obtained slurry of the metal hydroxides is oxidized at higher than 40°C and 60°C or lower while keeping its pH value of 10-13 and an obtained precursor is aged at 80-150°C and heat-treated at 400-700°C and for more than 1 hour and 3 hours or less after solid-liquid separation. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供黑色，耐氧化性，涂装分散性和涂膜表面平滑性优异的复合黑氧化物粒子，并提供其制造方法，黑色涂料和黑色矩阵。解决方案：尖晶石型或反尖晶石型复合黑氧化物颗粒由钴，铜和锰的氧化物组成，铜与钴的摩尔比为0.1-0.5，具有锰与钴的摩尔比为0.2-1.0。复合黑氧化物粒子的制造方法的特征在于，将由钴，铜和锰的水溶性盐和碱金属氢氧化物制成的混合金属盐水溶液混合进行中和，所得到的金属氢氧化物的浆料在较高温度下被氧化在40℃和60℃以下，同时保持其pH值为10-13，所得前体在80-150℃下老化并在400-700℃下热处理1小时3小时或更低。版权所有（C）2005，JPO＆NCIPI

9. 发明专利

JP2008247705A Black multiple oxide particles, black slurry, black paste and black matrix 有权
标题翻译：黑色多种氧化物颗粒，黑色浆液，黑色和黑色矩阵
公开(公告)号：JP2008247705A
公开(公告)日：2008-10-16
申请号：JP2007093932
申请日：2007-03-30
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： MINOWA HIKARI , MIYAKE KOJI , IWATA SUSUMU , FUJIYASU SHOICHI , NAKAYAMA MINORU , KATSUYAMA KOICHI
IPC分类号： C01G51/00 , H01B1/08 , H01B1/20
CPC分类号： H01B1/08 , B82Y30/00 , C01G3/02 , C01G51/00 , C01G51/04 , C01P2004/45 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/42 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C01P2006/66 , H01B1/20
摘要： PROBLEM TO BE SOLVED: To provide black multiple oxide particles having excellent blackness and electric conductivity, a small primary particle diameter, a small agglomerated particle diameter and excellent initial dispersibility, ensuring thin line property when a coating material containing the particles is prepared and used to form an electrode pattern, and suitable for applications such as a colored composition for a black matrix and black pigment powder for forming a black electrode or a light shielding layer of a front panel of a plasma display, a plasma address liquid crystal or the like, and to provide a black coating material and black paste.
SOLUTION: The black multiple oxide particles comprise an oxide of cobalt and copper, have an average primary particle diameter of 0.03-0.5 μm and D
50 in particle size measurement of 0.05-1.0 μm, and show a granular shape, wherein the particle size measurement is based on a number basis by a laser diffraction scattering method.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供具有优异的黑色和电导率的黑色多重氧化物颗粒，初级粒径小，聚集粒径小和初始分散性优异，确保了含有颗粒的涂料时的细线性能并且用于形成电极图案，并且适用于诸如用于黑色矩阵的着色组合物和用于形成等离子体显示器的前面板的黑色电极或遮光层的黑色颜料粉末，等离子体寻址液晶或并提供黑色涂料和黑色浆料。解决方案：黑色多重氧化物颗粒包含钴和铜的氧化物，其平均初级粒径为0.03-0.5μm，D 50 的粒度测量为0.05-1.0μm，以及显示出粒状测量，其中粒度测量基于激光衍射散射法的数量。版权所有（C）2009，JPO＆INPIT

10. 发明专利

JP2007302492A Cobalt hydroxide particle and cobalt oxide particle 有权
标题翻译：碳酸氢氧化钴颗粒和氧化钴颗粒
公开(公告)号：JP2007302492A
公开(公告)日：2007-11-22
申请号：JP2006131000
申请日：2006-05-10
申请人： Mitsui Mining & Smelting Co Ltd , 三井金属鉱業株式会社
发明人： HOSHINO TOMOYUKI , KATSUYAMA KOICHI , FUJIYASU SHOICHI , SHIMAMURA HIROYUKI
IPC分类号： C01G51/04 , H01L21/768 , H01L23/522
摘要： PROBLEM TO BE SOLVED: To provide cobalt oxide particles desirable to obtain cobalt oxide particles which simultaneously satisfy a high degree of blackness and a high electrical resistance.
SOLUTION: The cobalt hydroxide particles are characterized in that the D
50 is 0.1-1 μm when measured by a laser diffraction/scattering particle size distribution measurement method.
COPYRIGHT: (C)2008,JPO&INPIT

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