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1. 发明专利

JP2015020917A シラン類の製造方法有权
标题翻译：生产硅烷的方法
公开(公告)号：JP2015020917A
公开(公告)日：2015-02-02
申请号：JP2013147649
申请日：2013-07-16
申请人：三井化学株式会社 , Mitsui Chemicals Inc
发明人： IIJIMA TOMONORI , MURAKAMI MASAMI , TAKAHASHI NAOYA , KUWAMURA HIROKI , SHIMOMOTO KAZUMA , KONNO RIKA
IPC分类号： C01B33/04
摘要：【課題】ケイ化マグネシウムを含む合金粉体を連続して安定的に工業的規模で製造することができる方法、及び、該合金粉体からのシラン類の製造を可能とする方法を提供する。【解決手段】不活性ガス雰囲気下、ケイ素粉体およびマグネシウム粉体を含む原料混合物を、連続的に焼成炉に供給して該原料混合物を連続的に昇温する工程(I−1)、次いで昇温した原料混合物の温度を特定の温度範囲に制御する工程(I−2)、及び、第一焼成工程を経て得られたケイ化マグネシウムを含む合金粉体と酸とを溶媒中にて反応させてシラン類を製造する工程(II)を含み、工程(I−1)が、ケイ素粉体及びマグネシウム粉体を含む原料混合物の温度を、2.5〜50℃/分の昇温速度で480〜520℃の温度範囲にある第一焼成温度に到達させる工程であり、(但し、第一焼成温度とは、480〜520℃の温度範囲で昇温速度が2.5℃/分未満になった温度のことをいう)、工程(I−2)が、昇温した混合物を480〜530℃の温度範囲で30分間(0.5時間以上維持させることを特徴とするシラン類の製造方法である。【選択図】なし
摘要翻译：要解决的问题：提供连续，稳定地和工业规模生产硅化镁合金粉末的方法和从合金粉末制备硅烷的方法。解决方案：制备硅烷的方法包括：步骤（I- 1）在惰性气体气氛中连续供给含有硅粉末和镁粉末的原料混合物到烧制炉中，并连续提高供给的原料混合物的温度; 将温度升高的原料混合物的温度控制在特定温度范围内的工序（I-2）和使通过第一烧成工序得到的硅化镁系合金粉末与酸在溶剂中反应生成硅烷的工序（II）。在步骤（I-1）中，将含有硅粉末和镁粉末的原料混合物的温度升高到温度范围为480-520℃的第一烧成温度，升温速度为2.5-50℃ /分钟（条件是第一次烧成温度在480〜520℃之间，升温速度低于2.5℃/分钟时的温度）。在步骤（I-2）中，将升温的原料混合物保持在480-530℃的另一温度范围内30分钟（0.5小时）以上。

2. 发明专利

JP2013063873A Oxide having perovskite structure, method for producing the same, and photocatalyst 有权
标题翻译：具有PEROVSKITE结构的氧化物，其生产方法和光催化剂
公开(公告)号：JP2013063873A
公开(公告)日：2013-04-11
申请号：JP2011203141
申请日：2011-09-16
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： SHINJO RYO , MURAKAMI MASAMI
IPC分类号： C01G33/00 , B01J23/20 , B01J35/02 , B01J37/03 , B01J37/08
摘要： PROBLEM TO BE SOLVED: To provide a composite oxide having a perovskite-type crystal structure, to provide a method for producing the same, and to provide a highly active photocatalyst composed of the composite oxide.SOLUTION: The composite oxide having a perovskite-type crystal structure includes, as constitutive components, an alkali metal (M1) and a group 5 element (M5) of the periodic table, and is obtained by firing, and the crystallite diameter of the oxide is within the range of 10-35 nm. The composite oxide is obtained by subjecting a mixture including: an alkali metal compound (A) containing the alkali metal (M1) as a constitutive component; and a metal compound (B) containing the group 5 element (M5) of the periodic table as a constitutive component, to a hydrothermal treatment to form a crystalline precipitate having no perovskite structure, and thereafter, subjecting the precipitate to a firing treatment.
摘要翻译：要解决的问题：提供具有钙钛矿型晶体结构的复合氧化物，以提供其制造方法，并提供由复合氧化物构成的高活性光催化剂。解决方案：具有钙钛矿型晶体结构的复合氧化物包括作为构成成分的元素周期表的碱金属（M1）和第5族元素（M5），通过烧成得到，微晶直径的氧化物在10-35nm的范围内。复合氧化物是通过使含有碱金属（M1）的碱金属化合物（A）作为组成成分的混合物进行处理而得到的。和含有周期表第5族元素（M5）作为组成成分的金属化合物（B）进行水热处理，形成不具有钙钛矿结构的结晶沉淀物，然后对沉淀进行烧成处理。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2012120979A Method for manufacturing copper catalyst, and method for aging copper catalyst precursor 有权
标题翻译：制备铜催化剂的方法和老化催化剂前体的方法
公开(公告)号：JP2012120979A
公开(公告)日：2012-06-28
申请号：JP2010273815
申请日：2010-12-08
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： GOTO TOMOYA , YOSHINAGA KATSUMI , MAEDA KEN , MURAKAMI MASAMI
IPC分类号： B01J23/80 , B01J37/03 , B01J37/08
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a copper catalyst with excellent catalytic activity efficiently and reproducibly.SOLUTION: The method for manufacturing the copper catalyst includes (1) a step of mixing an acid aqueous solution A containing a water-soluble copper salt and an aqueous solution B containing a precipitant to obtain slurry containing a carbonate ion with a slurry concentration in terms of a metal hydroxide is 5-10 mass%, and (2) a step of aging the slurry at 45-100°C.
摘要翻译：要解决的问题：提供一种有效且可重复地制造具有优异催化活性的铜催化剂的方法。解决方案：铜催化剂的制造方法包括：（1）将含有水溶性铜盐的酸性水溶液A和含有沉淀剂的水溶液B混合，得到含有碳酸盐离子的浆料以金属氢氧化物计的浓度为5-10质量％，（2）在45-100℃下使浆料老化的步骤。版权所有（C）2012，JPO＆INPIT

4. 发明专利

JP2010248062A Method of manufacturing chlorine from hydrogen chloride using fluidized bed reactor 有权
标题翻译：使用流化床反应器从氯化氢制造氯化物的方法
公开(公告)号：JP2010248062A
公开(公告)日：2010-11-04
申请号：JP2010070380
申请日：2010-03-25
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： HORIUCHI NOBUHIKO , NABETA TAKASHI , SUGIMOTO KENICHI , IWATA KENJI , MURAKAMI MASAMI
IPC分类号： C01B7/01 , B01J23/78
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing chlorine from hydrogen chloride in which the flowability of a catalyst particle in a fluidized bed vessel is improved, thereby a successive reaction is stably possible, and which can manufacture chlorine with a high invert ratio.
SOLUTION: The method of manufacturing chlorine from hydrogen chloride, in which hydrogen chloride is oxidized in a fluidized bed reactor, thereby chlorine is manufactured from hydrogen chloride, comprises as follows. A catalyst particle (A) which satisfies requirements (A1) and (A2), and a reaction inactive particle (B) which satisfies a requirement (B1) exist in the fluidized bed reactor, the content of a copper element is 0.3-4.5 wt.% based on 100 wt.% of the total of the catalyst particles (A) and the reaction inactive particles (B). (A1): The ending velocity of the catalyst particle (A) in the air at 20°C is 1.1 to 100 times of the gas superficial velocity in the fluidized bed reactor. (A2): The catalyst particle (A) includes 0.5-12 wt.% of a copper element based on 100 wt.% of the catalyst particle (A). (B1): The ending velocity of the reaction inactive particle (B) in the air at 20°C is 1.1 to 100 times of the gas superficial velocity in the fluidized bed reactor.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：解决的问题：提供从流化床容器中的催化剂颗粒的流动性提高的氯化氢制造氯的方法，从而可以稳定地进行连续的反应，并且可以制造高氯的氯倒数比。解决方案：氯化氢中的氯化氢在流化床反应器中氧化，由氯化氢制造氯的方法由以下组成。在流化床反应器中存在满足要求（A1）和（A2）的催化剂颗粒（A）和满足要求（B1）的反应活性颗粒（B），铜元素的含量为0.3-4.5重量％％，基于催化剂颗粒（A）和反应无活性颗粒（B）的总量的100重量％。（A1）：在20℃下，空气中的催化剂粒子（A）的终止速度为流化床反应器中气体空速的1.1〜100倍。（A2）：催化剂颗粒（A）包含基于100重量％的催化剂颗粒（A）的0.5-12重量％的铜元素。（B1）：在20℃的空气中的反应无活性粒子（B）的终止速度为流化床反应器中气体空速的1.1〜100倍。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2005225689A Coating liquid for forming porous silica film, porous silica film, method of manufacturing them, semiconductor material and semiconductor device 审中-公开
标题翻译：用于形成多孔二氧化硅膜，多孔硅胶膜，其制造方法，半导体材料和半导体器件的涂覆液
公开(公告)号：JP2005225689A
公开(公告)日：2005-08-25
申请号：JP2004034196
申请日：2004-02-10
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： OIKE SHUNSUKE , TAKAMURA KAZUO , MURAKAMI MASAMI , KURANO YOSHITO
IPC分类号： C01B33/12 , C08G77/02 , C08K5/05 , C08L71/02 , C08L83/02 , H01L21/316
摘要： PROBLEM TO BE SOLVED: To provide a porous silica film having uniform pores, excellent surface smoothness and suitably used for an optical functional material, electronic functional material, a semiconductor material or the like.
SOLUTION: The porous silica film free from radial streak, striped pattern or the like and having excellent surface smoothness is obtained by using a coating liquid for forming the porous silica film which contains a silane compound (A) containing alkoxy silane having at least Si-O-Si bond, a surfactant (B), an organic compound (C) having 150-300°C boiling point, dielectric constant of ≥25 and 2.0-1,000 cP viscosity at 20°C and a solvent (D), applying the coating liquid on a base material, evaporating the solvent (D) and removing the surfactant.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供具有均匀孔的多孔二氧化硅膜，表面光滑性优异，适用于光功能材料，电子功能材料，半导体材料等。解决方案：通过使用含有含有烷氧基硅烷的硅烷化合物（A）的多孔二氧化硅膜形成用涂布液，可以获得不具有径向条纹，条纹图案等并且具有优异的表面光滑度的多孔二氧化硅膜，最低Si-O-Si键，表面活性剂（B），沸点为150-300℃的有机化合物（C），介电常数在20℃时为≥25和2.0-1,000cP粘度和溶剂（D）将涂布液涂布在基材上，蒸发溶剂（D）并除去表面活性剂。版权所有（C）2005，JPO＆NCIPI

6. 发明专利

JP2004051899A Method for producing coating liquid for forming porous silica film, coating liquid obtained by the same and porous silica film excellent in water repellency 有权
标题翻译：生产用于形成多孔硅胶的涂料液的方法，由其获得的涂覆液体和多孔硅胶膜在水中的优异性
公开(公告)号：JP2004051899A
公开(公告)日：2004-02-19
申请号：JP2002214361
申请日：2002-07-23
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TAKAMURA KAZUO , OIKE SHUNSUKE , KUBOTA TAKESHI , KURANO YOSHITO , MURAKAMI MASAMI
IPC分类号： C09D183/04 , C09D183/08 , C09D183/10
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a coating liquid for forming a porous silica film capable of being used as an optically functional material and electronically functional material, the coating liquid obtained by the method and the porous silica film excellent in water repellency.
SOLUTION: This method for producing the coating liquid for forming the porous silica film by mixing (A) a hydrolytic condensate of an alkoxysilane, (B) a hydrolytic co-condensate of (B-1) an alkoxysilane containing a polyalkyleneoxide group and (B-2) a hydrolyzable organic silicon compound not containing the polyalkylene oxide group, and (C) a surfactant is provided by mixing (A) the hydrolytic condensate with (C) the surfactant and adding the mixture into (B) the hydrolytic co-condensate, or mixing (B) the hydrolytic co-condensate with (C) the surfactant and then adding the mixture into (A) the hydrolytic condensate and further agitating. The porous silica film having uniform pores capable of being used for the optically functional materials, electronically functional materials, etc., and excellent in water repellency is obtained by the method for producing the coating liquid for forming the porous silica film and the coating liquid obtained by the method.
COPYRIGHT: (C)2004,JPO
摘要翻译：解决问题的方法为了提供一种用于形成能用作光学功能材料和电子功能材料的多孔二氧化硅膜的涂布液的方法，通过该方法获得的涂布液和多孔二氧化硅膜是优异的具有防水性。＆lt; P＆gt;解决方案：通过混合（A）烷氧基硅烷的水解缩合物，（B）（B-1）的含有聚环氧烷烃的烷氧基硅烷的水解缩合物来制造用于形成多孔二氧化硅膜的涂布液的方法和（B-2）不含聚亚烷基氧基的可水解有机硅化合物，和（C）表面活性剂通过将（A）水解缩合物与（C）表面活性剂混合并将混合物加入（B）水解（B）水解共缩合物与（C）表面活性剂混合，然后将混合物加入到（A）水解缩合物中并进一步搅拌。通过该多孔二氧化硅膜的形成用涂布液的制造方法和得到的涂布液，得到能够用于光学功能材料，电子功能材料等，疏水性优异的孔径均匀的多孔二氧化硅膜通过该方法。版权所有（C）2004，JPO

7. 发明专利

JP2010228952A Method for producing chlorine form hydrogen chloride using fluidizing bed reactor 审中-公开
标题翻译：使用流化床反应器生产氯化氢氯化物的方法
公开(公告)号：JP2010228952A
公开(公告)日：2010-10-14
申请号：JP2009076925
申请日：2009-03-26
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： HORIUCHI NOBUHIKO , NABETA TAKASHI , SUGIMOTO KENICHI , IWATA KENJI , MURAKAMI MASAMI
IPC分类号： C01B7/04 , B01J23/78
摘要： PROBLEM TO BE SOLVED: To provide a method for producing hydrogen chloride stably continuously reacting and producing chlorine with high conversion rate by improving the fluidity of a catalyst particles in a fluidized bed reactor. SOLUTION: In the method for producing chlorine from hydrogen chloride by oxidizing hydrogen chloride in the fluidized bed reactor, a catalyst particle (A) having 70-300 μm average particle diameter and containing copper element and a reaction-inactive particle (B) having 5-50 μm average particle diameter are present in the fluidized bed reactor and the ratio (A)/(B) by weight of the catalyst particle (A) to the reaction-inactive particle (B) present in the reactor is 50/50-99/1. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种通过提高流化床反应器中的催化剂颗粒的流动性来稳定地连续地使氯化氢生产和生产具有高转化率的氯的方法。解决方案：在流化床反应器中通过氧化氯化氢从氯化氢生产氯的方法中，具有70-300μm平均粒径并含有铜元素和反应惰性颗粒（B）的催化剂颗粒（A））在流化床反应器中存在，并且催化剂颗粒（A）与反应器中存在的反应惰性颗粒（B）的重量比（A）/（B）为50 / 50-99 / 1。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2010227793A Fluidized-bed catalyst for production of chlorine and method of producing chlorine using the same 有权
标题翻译：用于生产氯化物的流化床催化剂及其生产方法
公开(公告)号：JP2010227793A
公开(公告)日：2010-10-14
申请号：JP2009076922
申请日：2009-03-26
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： NABETA TAKASHI , HORIUCHI NOBUHIKO , SUGIMOTO KENICHI , IWATA KENJI , MURAKAMI MASAMI
IPC分类号： B01J23/78 , B01J35/08 , C01B7/04
摘要： PROBLEM TO BE SOLVED: To provide a catalyst for production of chlorine which does not change its shape of the particle during the reaction, is capable of retaining a good reaction yield over a long period and allows stable supply at low cost when used in a fluidized-bed reactor for the reaction in which hydrogen chloride is oxidized with oxygen to produce chlorine, and a method of producing chlorine by using the catalyst. SOLUTION: The catalyst for production of chlorine is used to produce chlorine by oxidizing hydrogen chloride with oxygen in a fluidized-bed reactor, includes spherical particles containing copper, alkali metal and rare earth metal elements and has a particle abrasion rate of 0.20 wt.%/h or lower. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供在反应期间不改变其形状的氯的生产催化剂，能够长期保持良好的反应收率，并且当使用时能够以低成本稳定地供应在其中用氧气氧化氯化氢以产生氯的反应的流化床反应器中，以及使用该催化剂生产氯的方法。解决方案：用于生产氯的催化剂用于通过在流化床反应器中用氧气氧化氯化氢来生产氯，包括含有铜，碱金属和稀土金属元素的球形颗粒，并且颗粒磨损率为0.20 重量％/ h以下。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2010194421A Method of producing copper-based catalyst 有权
标题翻译：生产铜基催化剂的方法
公开(公告)号：JP2010194421A
公开(公告)日：2010-09-09
申请号：JP2009040057
申请日：2009-02-23
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： MURAKAMI MASAMI , MAEDA KEN , GOTO TOMOYA
IPC分类号： B01J23/80 , B01J37/03 , B01J37/06 , C07B61/00 , C07C29/154 , C07C31/04
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method of producing a copper catalyst excellent in catalytic activity and reproducibility, and remarkably excellent in durability.
SOLUTION: The method of producing a catalyst for synthesizing methanol from hydrogen and an oxide of carbon, which is constituted of metal oxides including copper oxide, zinc oxide and aluminum oxide as essential components, and zirconium oxide, gallium oxide and silicon oxide as optional components, is characterized by carrying out (1) a process of mixing individual aqueous solutions of an acidic metal salt and an aqueous solution of a precipitant in water to form a precipitate of a metal compound precursor, and thereafter continuously replacing water therein with fresh one while keeping the concentration of the metal compound precursor in the slurry constant to remove the precipitant together with the water being discharged, (2) a process of discharging the slurry from the reaction system without adding water thereto to increase the concentration of the metal compound precursor in the slurry to form a cake of the precipitate, and (3) a process of drying/calcining the cake of the precipitate to form corresponding metal oxides.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：解决的问题：提供催化活性和再现性优异的铜催化剂的制造方法，耐久性优异。解决方案：由氧化铜，氧化锌和氧化铝作为必需成分的金属氧化物和氧化锆，氧化镓和氧化硅构成的由氢和碳的氧化物合成甲醇的催化剂的制造方法作为任选的成分，其特征在于进行（1）将酸性金属盐的各个水溶液与沉淀剂的水溶液混合在水中以形成金属化合物前体的沉淀物的方法，然后用同时保持浆料中金属化合物前体的浓度恒定，以便与排出的水一起除去沉淀剂，（2）从反应体系中排出浆料而不添加水以增加金属的浓度的方法化合物前体，以形成沉淀物的滤饼，和（3）干燥/煅烧p的滤饼的方法选择形成相应的金属氧化物。版权所有（C）2010，JPO＆INPIT

10. 发明专利

JP2010194420A Copper-based catalyst, and pretreatment method therefor 审中-公开
标题翻译：基于铜的催化剂及其预处理方法
公开(公告)号：JP2010194420A
公开(公告)日：2010-09-09
申请号：JP2009040056
申请日：2009-02-23
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： MURAKAMI MASAMI , MAEDA KEN , GOTO TOMOYA
IPC分类号： B01J23/80 , B01J37/18 , C07B61/00 , C07C29/154 , C07C31/04
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a copper-based catalyst excellent in catalytic activity as well as in durability, and a pretreatment method therefor. SOLUTION: The copper-based catalyst is produced by reducing a copper catalyst (I) constituted of metal oxides including copper oxide, zinc oxide and aluminum oxide as essential components, and zircon oxide, gallium oxide and silicon oxide as optional components, at a temperature equal to or higher than the reaction temperature in producing methanol or the like and not higher than the calcination temperature in producing the catalyst (I). The reduction of the catalyst (I) is preferably carried out in a hydrogen-containing gas stream at a temperature of 300 to 550°C. COPYRIGHT: (C)2010,JPO&INPIT

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