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1. 发明专利

JP2011037651A Method for improving thermal conductivity of graphite 审中-公开
标题翻译：改善石墨热导率的方法
公开(公告)号：JP2011037651A
公开(公告)日：2011-02-24
申请号：JP2009184745
申请日：2009-08-07
申请人： Mitsubishi Gas Chemical Co Inc , 三菱瓦斯化学株式会社
发明人： EBATA HIDEJI , GOCHO YOSHIHIRO
IPC分类号： C01B31/04
摘要： PROBLEM TO BE SOLVED: To provide graphite having further enhanced thermal conductivity, a method for producing the graphite, and a method for enhancing thermal conductivity of graphite, irrespective of that graphite is known as a good conductor and a substance excellent in thermal conductivity.
SOLUTION: The graphite has enhanced purity of stable isotopes of carbon. The method for producing graphite is characterized by using a carbon compound having enhanced purity of stable isotopes of carbon as a raw material of the graphite. The method for enhancing thermal conductivity of graphite comprises enhancing the purity of stable isotopes of carbon in graphite.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供进一步提高导热性的石墨，石墨的制造方法和提高石墨导热性的方法，而不管石墨是什么，已知有良好的导体和热性优异的物质电导率。
解决方案：石墨具有提高的稳定同位素碳的纯度。石墨的制造方法的特征在于，使用碳稳定同位素纯度高的碳化合物作为石墨的原料。提高石墨导热性的方法包括提高石墨中碳稳定同位素的纯度。版权所有（C）2011，JPO＆INPIT

2. 发明专利

JP2010024188A Method for producing aromatic nitrile 有权
标题翻译：生产芳香植物的方法
公开(公告)号：JP2010024188A
公开(公告)日：2010-02-04
申请号：JP2008188063
申请日：2008-07-22
申请人： Mitsubishi Gas Chemical Co Inc , 三菱瓦斯化学株式会社
发明人： YAMAMOTO KAZUNARI , EBATA HIDEJI , KUKO YOICHI
IPC分类号： C07C253/28 , B01J23/26 , C07B61/00 , C07C255/50 , C07C255/51
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aromatic nitrile in a high yield, stably with time and economically advantageously by performing ammoxidation by the gas phase catalytic reaction of an alkyl-substituted aromatic hydrocarbon. SOLUTION: This method for producing the corresponding aromatic nitrile by performing the catalytic reaction of the mixed gas containing the alkyl-substituted aromatic hydrocarbon, ammonia and oxygen on the catalyst is provided by using the catalyst constituted by the oxides of vanadium and chromium, having the ≥0.10 and ≤0.30 cc/g total volume of pores of the catalyst having a ≥100 Å diameter, and a carrier. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：通过烷基取代的芳烃的气相催化反应进行氨氧化，提供了一种以高产率稳定地以时间和经济上的方式稳定地制备芳族腈的方法。解决方案：通过使用由钒和铬的氧化物构成的催化剂，通过在催化剂上进行含有烷基取代的芳香烃，氨和氧的混合气体的催化反应来生产相应的芳族腈的方法，具有≥0.10和≤0.30cc/ g直径的直径的催化剂总孔体积和载体。版权所有（C）2010，JPO＆INPIT

3. 发明专利

JP2010024187A Method for producing aromatic nitrile 审中-公开
标题翻译：生产芳香植物的方法
公开(公告)号：JP2010024187A
公开(公告)日：2010-02-04
申请号：JP2008188062
申请日：2008-07-22
申请人： Mitsubishi Gas Chemical Co Inc , 三菱瓦斯化学株式会社
发明人： YAMAMOTO KAZUNARI , EBATA HIDEJI , KUKO YOICHI
IPC分类号： C07C253/28 , B01J23/26 , B01J35/10 , B01J37/08 , C07B61/00 , C07C255/50 , C07C255/51
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aromatic nitrile in a high yield, stably with time and economically advantageously by performing the catalytic reaction of a mixed gas containing an alkyl-substituted aromatic hydrocarbon, ammonia and oxygen on a catalyst.
SOLUTION: This method for producing the corresponding aromatic nitrile by performing the catalytic reaction of the mixed gas containing the alkyl-substituted aromatic hydrocarbon, ammonia and oxygen on the catalyst is provided by using the catalyst constituted by the oxides of vanadium and chromium prepared by the mechanical compression-molding of powder of them, having a ≥10 and ≤100 m
2 /g specific surface area and further burning, and a carrier.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：为了通过在含有烷基取代的芳香烃，氨和氧的混合气体的催化反应中提供以高产率生产芳族腈的方法，通过时间和经济上的有利地进行催化反应催化剂。解决方案：通过使用由钒和铬的氧化物构成的催化剂，通过在催化剂上进行含有烷基取代的芳香烃，氨和氧的混合气体的催化反应来生产相应的芳族腈的方法通过其粉末的机械压制成型制备，具有≥10和≤100m比例的表面积并进一步燃烧，以及载体。版权所有（C）2010，JPO＆INPIT

4. 发明专利

JP2003238511A METHOD FOR PRODUCING NITRILE COMPOUND 审中-公开
公开(公告)号：JP2003238511A
公开(公告)日：2003-08-27
申请号：JP2002360605
申请日：2002-12-12
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： NAKAMURA KENICHI , EBATA HIDEJI , TANAKA FUMIO , SHIDARA TAKUJI , AMAKAWA KAZUHIKO
IPC分类号： C07C253/28 , C07B61/00 , C07C253/34 , C07C255/51
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a nitrile compound from a carbocyclic compound or a heterocyclic compound having an organic substituent, ammonia and air by a vapor-phase catalytic ammoxidation reaction, realizing a reaction under a good condition by adjusting a supplied gas composition and the contact time, or the like, without using a particular auxiliary apparatus and producing the nitrile compound on an industrial scale in high yield at a low cost. SOLUTION: The residual gas component left after the separation of the nitrile compound from the ammoxidation reaction gas is returned to a reactor at a specific ratio while keeping the molar ratio of the molecular oxygen to the organic substituent of the carbocyclic compound or heterocyclic compound supplied to the reactor within a specific range. COPYRIGHT: (C)2003,JPO

5. 发明专利

JPH07275701A PRODUCTION OF SILICA-TITANIA CATALYST 失效
公开(公告)号：JPH07275701A
公开(公告)日：1995-10-24
申请号：JP2049795
申请日：1995-02-08
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： ABE MARIKO , EBATA HIDEJI , ABE TAKAFUMI , HIGUCHI HIROBUMI
IPC分类号： B01J21/06 , C07B61/00 , C07C67/08 , C07C69/54
摘要： PURPOSE:To obtain an excellent catalytic activity by specifying respectively the proportion of an acid and the amount of an titanium compd. in an acidic soln. in the production of silica-titania catalyst by adding basic compd. to the acidic soln. in which silicon compd. and the titanium compd. are dissolved to coprecipitate the catalyst. CONSTITUTION:This catalyst is produced by adding the basic compd. to the acidic soln. in which the silicon compd. and the titanium compd. are dissolved to coprecipitate the catalyst. In this case, the acidic soln. made from nitric or sulfuric acid is used. The ratio of equivalence of the nitric acid or the sulfuric acid to the amount (mol) of the silicon compd. in the acidic soln. is specified to 0.5-50. Moreover, the amount of the titanium compd. in the acidic soln. is specified to the amount in which the proportion of the titania (TiO2) in the silica-titania catalyst to be produced is 1-50wt.%. The silica-titania catalyst produced by the coprecipitation method under high acid concn. shows the excellent catalytic activity in esterification reaction, etc., and is high in industrial value.

6. 发明专利

JPH0338546A PRODUCTION OF METHYL METHACRYLATE 失效
公开(公告)号：JPH0338546A
公开(公告)日：1991-02-19
申请号：JP17119089
申请日：1989-07-04
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： HIGUCHI HIROBUMI , KIDA KOICHI , EBATA HIDEJI
IPC分类号： C07C69/54 , C07C67/20 , C07C67/22 , C07C231/06
摘要： PURPOSE:To obtain the objective substance from methacrylamide and methyl formate and circulate hydrogen cyanide for use by reacting the prussic acid with acetone, hydrating the resultant acetone cyanhydrin, dehydrating the formed hydration product alpha-hydroxyisobutyramide and providing the methacrylamide. CONSTITUTION:Hydrogen cyanide and acetone are reacted in the presence of a basic catalyst at about 10 deg.C to provide acetone cyanhydrin, which is subsequently brought into contact with water in the presence of a catalyst, such as MnO2d, at 40-100 deg.C to afford alpha-hydroxyisobutyramide. The resultant compound is then subjected to dehydration reaction in the vapor phase preferably using an amide compound (e.g. N-methylpyrrolidone) as a diluent to provide methacrylamide, which is subsequently reacted with methyl formate or methanol and CO in the presence of an alkali metal alcoholate or alkaline earth metal oxide as a catalyst to afford the objective substance and formamide. Hydrogen cyanide is subsequently obtained from the formamide and circulated for use. thereby, the subject substance is obtained from the readily available raw materials in high yield.

7. 发明专利

JPH02268137A PREPARATION OF CARBOXYLIC ACID ESTER AND FORMAMIDE 失效
公开(公告)号：JPH02268137A
公开(公告)日：1990-11-01
申请号：JP8973789
申请日：1989-04-11
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： ISHIKAWA JIRO , HIGUCHI HIROBUMI , EBATA HIDEJI , KIDA KOICHI
IPC分类号： B01J31/02 , C07B61/00 , C07C67/20 , C07C69/54 , C07C69/675 , C07C231/08 , C07C231/10 , C07C233/03
摘要： PURPOSE:To prepared the subject compound in high selectivity under a mild condition by reacting a carboxylic acid amide with a formic acid ester or reacting the carboxylic acid amide with the alcohol and CO in the presence of an alkaline earth metal oxide as a catalyst. CONSTITUTION:When a carboxylic acid amide is reacted with a formic acid ester or with an alcohol and carbon monoxide to prepare a carboxylic acid ester and formamide, an alkaline earth metal oxide is employed as a catalyst. The catalyst includes the oxides of one kinds or more of magnesium, calcium, strontium and barium. The method permits to carry out the reaction under an extremely mild condition to effectively give the objective compound. The carboxylic acid ester is an industrially important compound. The formation is useful as a solvent, a treating agent for various purposes, an electrolyte, an antifreezing agent or an intermediate for dyes, pigments, drugs, etc.

8. 发明专利

JP2003238512A METHOD FOR PRODUCING POLYNITRILE COMPOUND 审中-公开
公开(公告)号：JP2003238512A
公开(公告)日：2003-08-27
申请号：JP2002360606
申请日：2002-12-12
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： NAKAMURA KENICHI , EBATA HIDEJI , TANAKA FUMIO , SHIDARA TAKUJI , AMAKAWA KAZUHIKO
IPC分类号： C07C253/28 , C07B61/00 , C07C255/51
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a polynitrile compound in high yield while suppressing a combustion side reaction to reduce the loss of raw materials without lowering the productivity by the vapor-phase catalytic reaction of a carbocyclic compound or heterocyclic compound having plural organic substituents (polysubstituted organic compound) with ammonia and an oxygen- containing gas to effect an ammoxidation reaction. SOLUTION: At least a part of an unreacted polysubstituted organic compound and a mononitrile compound formed as an intermediate are separated and recovered from a reaction gas discharged from a reactor and returned to the reactor while controlling the flow rate of the mononitrile compound in the discharged reaction gas to a level falling within a specific range. COPYRIGHT: (C)2003,JPO

9. 发明专利

JP2002173302A METHOD OF PRODUCING GASEOUS MIXTURE OF CARBON MONOXIDE WITH HYDROGEN 失效
公开(公告)号：JP2002173302A
公开(公告)日：2002-06-21
申请号：JP2000368561
申请日：2000-12-04
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： WATANABE TOSHIYASU , NAKAMURA KENJI , YONEOKA MIKIO , EBATA HIDEJI
IPC分类号： C01B3/22 , C01B32/40 , C01B31/18
摘要： PROBLEM TO BE SOLVED: To provide an industrially advantageous method of producing a gaseous mixture of carbon monoxide with hydrogen by decomposing methanol or a mixture of methanol with methyl formate in a liquid state in the presence of a solid catalyst. SOLUTION: The producing method is performed by using the solid catalyst containing copper, chromium, manganese and barium.

10. 发明专利

JP2002102711A METHOD FOR REGENERATING HIGHLY BASIC ANION EXCHANGE RESIN 失效
公开(公告)号：JP2002102711A
公开(公告)日：2002-04-09
申请号：JP2000299436
申请日：2000-09-29
申请人： MITSUBISHI GAS CHEMICAL CO
发明人： EBATA HIDEJI , YONEOKA MIKIO , NAKAMURA KENJI , IKOMA FUTOSHI
IPC分类号： B01J31/40 , B01J49/00 , C01B32/40
摘要： PROBLEM TO BE SOLVED: To provide a method for regenerating a highly basic anion exchange resin catalyst used in the production of carbon monoxide by the decomposition of methyl formate in a process-wise and economically advantageous manner. SOLUTION: The deactivated ion exchange resin is activated with 1.0-10.0 times (mol) as much metallic alcoholate as its ion exchange capacity.

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