会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 7. 发明专利
    • PRODUCTION OF PHOSPHORIC ACID MONOESTER
    • JPH01143880A
    • 1989-06-06
    • JP29957987
    • 1987-11-27
    • LION CORP
    • HABATA YOICHITAKAHASHI TOSHIO
    • C07F9/09
    • PURPOSE:To obtain the title substance by dissolving a mixture of phosphorus oxychloride and an organic hydroxyl compound in a hydrocarbon solvent and dropping in portions an organic tertiary amine, as the reaction system is kept at a relatively low temperature. CONSTITUTION:A mixture of 1.0mole of phosphorus oxychloride with 1.0-1.1mole of an organic hydroxy compound such as ethanol or phenol is dissolved in a hydrocarbon solvent, then a stoichiometric or a little excessive amount of an organic tertiary amine such as triethylamine, or pyridine is added dropwise in the course of 30 minutes to 1 hour, as the reaction mixture is kept below 30 deg.C. Then, the product is hydrolyzed to give the title substance of high purity and quality easily in high yield. The title substance is used as a detergent, emulsifier, antistatic or fiber finishing oil and the product from the process according to the present invention is excellent in foaming and cleaning power, reduced in irritation, and good in touch and color tone.