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1. 发明专利

JP2007176890A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2007176890A
公开(公告)日：2007-07-12
申请号：JP2005379648
申请日：2005-12-28
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU , TERASAKA MICHIO
IPC分类号： C07C209/22 , B01J23/76 , B01J23/847 , B01J23/89 , C07B61/00 , C07C211/03
CPC分类号： C07C209/16 , C07C211/07
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aliphatic primary amine in high selectivity from an aliphatic alcohol. SOLUTION: The method for producing the aliphatic amine comprises bringing a saturated or unsaturated aliphatic alcohol having straight chain, branch or ring into contact with ammonia and hydrogen in the presence of a catalyst containing (A) each component of nickel, copper and zirconium and (B) at least one kind of metal component selected from elements of the group III of the periodic table and elements of the group V of the periodic table and elements of the platinum group. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供从脂肪醇以高选择性制备脂族伯胺的方法。解决方案：制备脂族胺的方法包括使含有直链，支链或环的饱和或不饱和脂族醇与氨和氢接触，所述催化剂含有（A）镍，铜和锆和（B）选自周期表第III族元素和元素周期表第V族元素中的至少一种金属组分和铂族元素。版权所有（C）2007，JPO＆INPIT

2. 发明专利

JP2007176892A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2007176892A
公开(公告)日：2007-07-12
申请号：JP2005379660
申请日：2005-12-28
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU , TERASAKA MICHIO
IPC分类号： C07C209/16 , B01J23/89 , C07B61/00 , C07C211/03
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aliphatic primary amine in high activity and high selectivity from an aliphatic alcohol. SOLUTION: The method for producing the aliphatic amine comprises bringing a 6-22C saturated or unsaturated aliphatic alcohol having straight chain, branch or ring into contact with ammonia and hydrogen in the presence of a catalyst in which (A) a ruthenium component, (B) at least one kind of metal component selected from nickel and cobalt and (C) at least one kind of metal component selected from lanthanum, yttrium, magnesium and barium are supported on a porous oxide. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种脂肪族伯胺以高活性和高选择性从脂族醇生产的方法。解决方案：制备脂族胺的方法包括使具有直链，支链或环的6-22C饱和或不饱和脂族醇在氨和氢中与催化剂接触，其中（A）钌组分，（B）选自镍和钴的至少一种金属成分和（C）至少一种选自镧，钇，镁和钡的金属成分负载在多孔氧化物上。版权所有（C）2007，JPO＆INPIT

3. 发明专利

JP2009040732A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2009040732A
公开(公告)日：2009-02-26
申请号：JP2007208408
申请日：2007-08-09
申请人： Kao Corp , 花王株式会社
发明人： TERASAKA MICHIO , FUKUSHIMA TETSURO , TANIGUCHI HIDEKI , JONO MASAHARU
IPC分类号： C07C209/50 , B01J23/72 , B01J23/78 , B01J23/89 , B01J29/76 , B01J29/78 , C07B61/00 , C07C211/08 , C07C291/04
CPC分类号： C07C209/50 , C07C209/02 , C07C211/08 , C07C291/04
摘要： PROBLEM TO BE SOLVED: To provide a method for economically producing a high-purity aliphatic tertiary amine with a small amount of a by-product by subjecting a fatty acid amide to hydrogenation reduction under mild conditions and an amine derivative from the amine in high productivity. SOLUTION: The method for producing a tertiary amine in the presence of a catalyst containing copper and at least one element selected from the group consisting of elements belonging to Groups 2, 3, 7 and 12 of the periodic table (long form of the periodic table) includes (a) a process for reducing an amide compound in a hydrogen atmosphere, and (b) a process for introducing a dialkylamine containing 1-6C alkyl groups into the reaction product obtained in the process. The method for producing amine oxide comprises reacting the tertiary amine obtained by the production method with hydrogen peroxide. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种通过在温和条件下使脂肪酸酰胺进行氢化还原和来自胺的胺衍生物来经济地制备具有少量副产物的高纯度脂族叔胺的方法生产力高。解决方案：在含有铜的催化剂和选自元素周期表第2,3,7和12族的元素中的至少一种元素的存在下制备叔胺的方法（长形式周期表）包括（a）在氢气氛中还原酰胺化合物的方法，和（b）将含有1-6C烷基的二烷基胺引入到该方法获得的反应产物中的方法。生产氧化胺的方法包括使通过制备方法获得的叔胺与过氧化氢反应。版权所有（C）2009，JPO＆INPIT

4. 发明专利

JP2007269788A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2007269788A
公开(公告)日：2007-10-18
申请号：JP2007057076
申请日：2007-03-07
申请人： Kao Corp , 花王株式会社
发明人： JONO MASAHARU , TERASAKA MICHIO , TANIGUCHI HIDEKI , FUKUSHIMA TETSURO
IPC分类号： C07C209/50 , B01J23/78 , B01J29/072 , B01J29/076 , C07B61/00 , C07C211/08 , C07C291/04
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for economically advantageously producing in high productivity a high-purity aliphatic tertiary amine with slight byproducts by hydrogenation reduction of a fatty acid amide under mild conditions, and a method for economically advantageously producing in high productivity an amine derivative from the above amine. SOLUTION: The method for producing the aliphatic tertiary amine comprises hydrogenation reduction of a specific aliphatic amide in the presence of a catalyst containing copper and at least one element selected from groups 2, 3 and 7 elements. The catalyst is also provided. The method for producing an amine oxide as the amine derivative comprises conducting a reaction between the tertiary amine obtained above and hydrogen peroxide. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：为了在温和条件下通过氢化还原脂肪酸酰胺提供经济上有利地高生产率地生产高纯度脂族叔胺与轻微副产物的方法，以及经济上有利地生产高的方法生产率来自上述胺的胺衍生物。解决方案：用于制备脂族叔胺的方法包括在含有铜的催化剂和选自组2,3和7元素的至少一种元素的存在下氢化还原特定的脂族酰胺。还提供催化剂。作为胺衍生物的氧化胺的制造方法包括在上述得到的叔胺与过氧化氢之间进行反应。版权所有（C）2008，JPO＆INPIT

5. 发明专利

JP2007197422A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2007197422A
公开(公告)日：2007-08-09
申请号：JP2006337204
申请日：2006-12-14
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU , TERASAKA MICHIO
IPC分类号： C07C209/16 , B01J37/03 , B01J37/08 , B01J37/16 , C07B61/00 , C07C211/07
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aliphatic primary amine from an aliphatic alcohol in high selectivity and activity.
SOLUTION: An aliphatic amine is produced by bringing a straight-chain, branched-chain or cyclic 6-22C saturated or unsaturated aliphatic alcohol into contact with ammonia and hydrogen in the presence of a catalyst obtained by supporting (A) a ruthenium component and (B) at least one kind of metal component selected from a group composed of nickel, cobalt and tungsten and formed by the hydrolysis of (A') a ruthenium compound and (B') at least one kind of metal compound selected from a group composed of nickel, cobalt and tungsten on a carrier.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供以高选择性和活性的脂肪族醇制备脂族伯胺的方法。解决方案：通过使直链，支链或环状的6-22C饱和或不饱和脂族醇与氨和氢接触，在通过负载（A）钌获得的催化剂存在下，制备脂族胺组分和（B）选自镍，钴和钨组成的组中的至少一种金属组分，并通过水解（A'）钌化合物和（B'）形成至少一种选自以下的金属化合物：在载体上由镍，钴和钨组成的组。版权所有（C）2007，JPO＆INPIT

6. 发明专利

JP2007176891A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2007176891A
公开(公告)日：2007-07-12
申请号：JP2005379652
申请日：2005-12-28
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU , TERASAKA MICHIO
IPC分类号： C07C209/16 , B01J23/46 , B01J29/068 , B01J37/03 , B01J37/08 , B01J37/16 , C07B61/00 , C07C211/03
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aliphatic primary amine in high activity and high selectivity from an aliphatic alcohol. SOLUTION: The method for producing the aliphatic amine comprises bringing a 6-22C saturated or unsaturated aliphatic alcohol having straight chain, branch or ring into contact with ammonia and hydrogen in the presence of a catalyst in which a ruthenium component produced by hydrolysis of a ruthenium compound is supported on a porous oxide. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种脂肪族伯胺以高活性和高选择性从脂族醇生产的方法。解决方案：制备脂肪族胺的方法包括使具有直链，支链或环的6-22C饱和或不饱和脂族醇在氨和氢的存在下，在其中通过水解产生的钌组分的催化剂存在下进行接触的钌化合物负载在多孔氧化物上。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2007176889A Method for producing nitrogen-containing compound 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：JP2007176889A
公开(公告)日：2007-07-12
申请号：JP2005379635
申请日：2005-12-28
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU , TERASAKA MICHIO
IPC分类号： C07C209/16 , C07B61/00 , C07C211/03
CPC分类号： C07C209/16 , C07C211/07
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aliphatic primary amine in good yield and high productivity from an aliphatic alcohol.
SOLUTION: The method for producing the aliphatic amine comprises bringing a saturated or unsaturated aliphatic alcohol having straight chain or branch or ring in the presence of a catalyst containing (A) nickel, copper and zirconium and (B) at least one kind of metal component selected from the group I elements of the periodic table into contact with ammonia and hydrogen.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种从脂肪族醇得到的高产率和高生产率的脂肪族伯胺的制造方法。解决方案：制备脂族胺的方法包括在含有（A）镍，铜和锆的催化剂和（B）至少一种的催化剂存在下，使具有直链或支链或环的饱和或不饱和脂族醇的选自元素周期表的I族元素的金属组分与氨和氢接触。版权所有（C）2007，JPO＆INPIT

8. 发明专利

JP2007175662A Amination catalyst of fatty alcohol and method for manufacturing amine using the same 有权
标题翻译：脂肪醇的氨化催化剂及其制造方法
公开(公告)号：JP2007175662A
公开(公告)日：2007-07-12
申请号：JP2005379667
申请日：2005-12-28
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU , SUZUKI YUTA , TERASAKA MICHIO
IPC分类号： B01J23/89 , B01J27/185 , B01J35/10 , C07B61/00 , C07C209/16 , C07C211/03
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a catalyst that manufactures aliphatic primary amine with high selectivity, particularly from fatty alcohol and manufactures the aliphatic primary amine using the catalyst with high selectivity. SOLUTION: The method for manufacturing the fatty amine, saturated or unsaturated fatty alcohol of 6-22C having straight or branched chains is allowed to contact ammonia and hydrogen in the presence of the amination catalyst of fatty alcohol consisting of a crystalline porous body having mean pore diameter of a scope of 1 to 50 nm and at least one kind of metal component selected from (A) ruthenium, platinum, nickel, cobalt, and copper and the amination catalyst. COPYRIGHT: (C)2007,JPO&INPIT

9. 发明专利

JP2005048086A Method for manufacturing polyoxyalkylene triamine 审中-公开
标题翻译：制备聚氧亚甲基三胺的方法
公开(公告)号：JP2005048086A
公开(公告)日：2005-02-24
申请号：JP2003282482
申请日：2003-07-30
申请人： Kao Corp , 花王株式会社
发明人： FUKUSHIMA TETSURO , JONO MASAHARU
IPC分类号： C07C213/02 , C07C217/08 , C07C217/42 , C08G65/325
CPC分类号： C07C213/02 , C07C217/08 , C07C217/42
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a polyoxyalkylene triamine usable in both batch and continuous systems, sufficiently active and selective in a low-pressure reaction, not requiring an assistant for selectivity improvement, not vulnerable to a catalytic poison such as water, and capable of providing a high conversion rate and selectivity under reaction conditions where the molar ratio of ammonia to the hydroxy groups is relatively small.
SOLUTION: A polyoxyalkylene triol having hydroxy groups at its ends is brought into contact with ammonia and hydrogen for manufacturing the polyoxylalkylene triamine in the presence of a catalyst. In the catalyst, the ruthenium metal accounts for 0.5-20 wt.% of the total of the catalyst and is supported on at least one support selected from the group consisting of alumina, silica, silica-alumina, titanium, and titanium-silica.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供可用于批次和连续系统中的聚氧化烯三胺的制备方法，在低压反应中具有足够的活性和选择性，不需要助催化剂改进，不易于催化毒物例如水，并且能够在氨与羟基的摩尔比相对较小的反应条件下提供高转化率和选择性。解决方案：在催化剂存在下，使其末端具有羟基的聚氧化烯三醇与氨和氢接触以制备聚氧基亚烷基三胺。在催化剂中，钌金属占催化剂总量的0.5-20重量％，并且负载在选自氧化铝，二氧化硅，二氧化硅 - 氧化铝，钛和钛 - 二氧化硅中的至少一种载体上。版权所有（C）2005，JPO＆NCIPI

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