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    • 9. 发明专利
    • PRODUCTION OF FERROUS POWDER FOR POWDER METALLURGY
    • JPH10265803A
    • 1998-10-06
    • JP8892897
    • 1997-03-24
    • KAWASAKI STEEL CO
    • MARUTA KEIICHIOGURA KUNIAKI
    • B22F9/08B22F1/00
    • PROBLEM TO BE SOLVED: To obtain ferrous powder for powder metallurgy at a low cost by spraying molten steel contg. a specific ratio or below of C by water atomization and drying this powder at a specific temp. range in a nonoxidizing atmosphere, then subjecting the powder to a finish reduction heat treatment in an H2 reducing atmosphere of a specific dew point. SOLUTION: The content of the C in the molten steel is confined to >=0.07 wt.%, by which the hardness at the section of atomized green powder is decreased and the annealing load at the time of the finish treatment is decreased. The powder is dried at 100 to 300 deg.C in the nonoxidizing atmosphere of Ar, N2 , H2 or the gaseous mixture composed thereof, by which the increase of the oxygen quantity in the powder is suppressed. The dew point of the H2 reducing atmosphere (pure H2 or an atmosphere mixture composed of the H2 and the inert gas) in the finish reduction heat treatment is specified to 20 to 45 deg.C. The temp. of the finish reduction heat treatment is preferably specified to 800 to 1,100 deg.C and the finish reduction time to 60 to 180 minutes.
    • 10. 发明专利
    • IRON POWDER FINISH HEAT-TREATING METHOD AND DEVICE THEREFOR
    • JPH09170002A
    • 1997-06-30
    • JP27075096
    • 1996-10-14
    • KAWASAKI STEEL CO
    • MARUTA KEIICHIISHIKAWA HIROYUKIOGURA KUNIAKI
    • B22F1/00F27B9/04
    • PROBLEM TO BE SOLVED: To improve the gas permeability of a raw-powder bed and to improve heat-treating efficiency in the finish heat treatment of iron powder by incorporating moisture into the raw powder while impressing a magnetic field. SOLUTION: An iron powder being a raw powder 7 is supplied to a belt 9 from a raw material hopper 8 and sent to a heat-treating furnace 20. A magnetic field generator 12 having a magnet as a counter electrode is set above and below the belt 9 between the furnace 20 and hopper 8 to impress a magnetic field on the raw powder 7. The pipeline 13 of a moisture feeder is furnished directly below the magnetic field generator 12, and moisture is supplied to the raw powder 7 impressed with the magnetic field. The furnace 20 is divided by a partition wall 1 into a decraburization zone 2, a deoxidation zone 3 and a denitrification zone 4, and one or >=2 kinds of heat treatments are conducted in each zone. An aq. soln of an acid such as carbonic acid, formic acid, acetic acid, benzoic acid and oxalic acid consisting only of C, O and H is preferably used as the moisture to be incorporated. The magnetic field to be impressed on the raw powder 7 is preferably controlled to about 1000 gauss at the bottom of the raw powder 7 bed and to about 200 gauss on the surface.