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1. 发明专利

JP2009041074A Insulation-film treatment liquid free from chromium for grain-oriented electromagnetic steel sheet and method for manufacturing grain-oriented electromagnetic steel sheet provided with insulation film 有权
标题翻译：用于晶粒电磁钢板的铬的绝缘膜处理液和制造用绝缘膜提供的面向导向的电磁钢板的方法
公开(公告)号：JP2009041074A
公开(公告)日：2009-02-26
申请号：JP2007207674
申请日：2007-08-09
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： MURAKI MINEO , SHIGEKUNI TOMOFUMI , TAKASHIMA MINORU
IPC分类号： C23C22/00 , C21D9/46 , C22C38/00 , C22C38/60 , H01F1/16 , H01F1/18
CPC分类号： C23C22/40 , C21D1/70 , C21D8/1283 , C21D2201/05 , C22C38/60 , C23C22/68 , C23C22/74 , C23C26/00 , H01F1/18 , H01F41/005 , H01F41/024
摘要： PROBLEM TO BE SOLVED: To provide an insulation-film treatment liquid free from chromium for a grain-oriented electromagnetic steel sheet, which prevents the lowering of its film tension and moisture absorption resistance, which is a problem occurring when the insulation-film treatment liquid does not contain chromium, and which gives properties required for the insulation film of a grain-oriented electromagnetic steel sheet, specifically, film tension, moisture absorption resistance, corrosion resistance and a space factor equivalent to those in an insulation film obtained by using an insulation-film treatment liquid containing a chromium compound, to the insulation film. SOLUTION: This treatment liquid includes: one or more phosphates selected from the phosphates of Mg, Ca, Ba, Sr, Zn, Al and Mn; and colloidal silica in an amount of 0.5 to 10 mol in terms of SiO 2 and a water-soluble vanadium compound in an amount of 0.1 to 2.0 mol in terms of V with respect to 1 mol of the PO 4 which is contained in the above selected phosphate and shall be a reference value. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供一种防止其膜张力和耐吸湿性降低的晶粒取向电磁钢板的不含铬的绝缘膜处理液，这是当绝缘层 - 膜处理液不含铬，赋予晶粒取向电磁钢板的绝缘膜所需的特性，特别是膜张力，耐吸湿性，耐腐蚀性以及与绝缘膜中的绝缘膜相同的空间因子对绝缘膜使用含有铬化合物的绝缘膜处理液。该处理液包括：一种或多种选自Mg，Ca，Ba，Sr，Zn，Al和Mn的磷酸盐的磷酸盐; 和相对于1摩尔PO的量为0.5至10摩尔（以SiO 2 SB 2）计的胶态二氧化硅和以V计为0.1至2.0摩尔的水溶性钒化合物上述选择的磷酸盐中含有的 4 作为参考值。版权所有（C）2009，JPO＆INPIT

2. 发明专利

JP2008240080A Insulating film treatment liquid for grain-oriented electrical steel sheet and method for manufacturing grain-oriented electrical steel sheet 有权
标题翻译：用于面向电工钢板的绝缘膜处理液和用于制造面向导电电工钢板的方法
公开(公告)号：JP2008240080A
公开(公告)日：2008-10-09
申请号：JP2007083325
申请日：2007-03-28
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： TAKASHIMA MINORU , WATANABE MAKOTO , SHIGEKUNI TOMOFUMI , MURAKI MINEO
IPC分类号： C23C22/00 , C21D8/12 , C21D9/46
CPC分类号： C23C22/08 , C23C22/74
摘要： PROBLEM TO BE SOLVED: To provide an insulating film treating liquid for a grain-oriented electrical steel sheet which does not contain chromium, and is excellent in film tension, moisture absorption resistance, rust preventiveness, and space factor and method for manufacturing the grain-oriented electrical steel sheet using the treating liquid.
SOLUTION: The insulating film is formed on the surface of the grain-oriented electrical steel sheet by using the insulating film treating liquid containing colloidal silica at 0.5 to 1.0 mol in terms of SiO
2 of 1 mol phosphoric acid (PO
4 ) of the phosphate in one or more selected from phosphates of Mg, Ca, Ba, Sr, Zn, Al, and Mn and containing one or more selected from hypochlorite, chlorite, chlorate, and perchlorate of Ca, Mn, Fe, Mg, Zn, Co, Ni, Cu and Al at 0.005 to 3.0 mol in total with respect to the molar number of the metallic elements.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种不含铬的方向性电磁钢板的绝缘膜处理液，膜张力，耐吸湿性，防锈性和空间因素以及制造方法优异使用处理液的方向性电磁钢板。解决方案：通过使用含有胶体二氧化硅的绝缘膜处理液，以SiO 2 SB 1为0.5〜1.0摩尔，形成绝缘膜，该绝缘膜为1 一种或多种选自Mg，Ca，Ba，Sr，Zn，Al和Mn的磷酸盐中的磷酸（PO 4 ），并且含有一种或多种选自次氯酸盐，亚氯酸盐，相对于金属元素的摩尔数，总计0.005〜3.0摩尔的Ca，Mn，Fe，Mg，Zn，Co，Ni，Cu和Al的氯酸盐和高氯酸盐。版权所有（C）2009，JPO＆INPIT

3. 发明专利

JP2008127635A Method for coating annealing-separation agent for grain-oriented magnetic steel sheets, and method for manufacturing grain-oriented magnetic steel sheet 有权
标题翻译：用于涂覆用于面向导电磁性钢板的退火分离剂的方法以及制造面向导向的磁性钢板的方法
公开(公告)号：JP2008127635A
公开(公告)日：2008-06-05
申请号：JP2006314455
申请日：2006-11-21
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： TODA HIROAKI , TERAJIMA TAKASHI , MURAKI MINEO
IPC分类号： C21D8/12 , C21D1/70 , C22C38/00 , C22C38/60 , C23C22/00
摘要： PROBLEM TO BE SOLVED: To provide a method for newly evaluating magnesia for annealing-separation agent when a grain-oriented magnetic steel sheet is manufactured, and to stably obtain the grain-oriented magnetic steel shhet excellent in not only a film characteristic, but magnetic characteristic, by using the magnesia satisfying the characteristic value evaluated with the above evaluating method.
SOLUTION: As the magnesia in the annealing-separation agent, a powdery material having impurities with the concentrations 0.01-0.04 mass% Cl, 0.25-0.70 mass% CaO, 0.05-0.15 mass% B, 0.05-0.50 mass% SO
3 and satisfying 50-90 sec in 40% of CAA(citiric acid activity), and further, 1.5-2.5 mass% of a hydrate quantity at 20°C for 30 min of a hydrate-test, and 3.0-5.0 mass% of the hydrate quantity at 20°C for 180 min of the hydrate-test, is used. The annealing-separation agent which is hydrated so that the hydrate quantity of the magnesia becomes 1.0-3.5 mass% after coating and drying by making the slurry-state to this powdery material with the adjustment of the hydrate temperature and the average hydrate time of the slurry, is coated and dried on the surface of this steel sheet.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种当制造晶粒取向的电磁钢板时，重新评估退火分离剂的氧化镁的方法，并且稳定地获得不仅膜特性优异的晶粒取向磁钢，但是磁特性，通过使用满足用上述评价方法评价的特性值的氧化镁。解决方案：作为退火分离剂中的氧化镁，具有浓度为0.01〜0.04质量％的Cl，0.25〜0.70质量％的CaO，0.05〜0.15质量％的B，0.05〜0.50质量％的SO的杂质的粉末状物质在30％的水合物试验中，在40％的CAA（柑橘酸活性）中满足50-90秒，并且在20℃下的水合物量为1.5-2.5质量％，30分钟，使用水合物试验在20℃下水合物量的3.0-5.0质量％180分钟。水合后的退火分离剂，通过调节水合物的温度和水合物的平均时间，在涂布干燥后使氧化镁的水合物量成为1.0〜3.5质量％浆料在该钢板的表面上进行涂布和干燥。版权所有（C）2008，JPO＆INPIT

4. 发明专利

JP2006144036A Non-oriented magnetic steel sheet for modular type motor and its production method 有权
标题翻译：模块式电动机非磁性磁钢片及其生产方法
公开(公告)号：JP2006144036A
公开(公告)日：2006-06-08
申请号：JP2004332227
申请日：2004-11-16
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： TODA HIROAKI , SADAHIRO KENICHI , MURAKI MINEO
IPC分类号： C22C38/00 , B21B3/02 , C21D8/12 , C22C38/14 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide a non-oriented magnetic steel sheet which has reduced magnetic anisotropy and is excellently suitable for a modular type motor, and to provide its production method. SOLUTION: The non-oriented magnetic steel sheet has a composition containing, by mass, ≤0.005% C, 2.5 to 4.0% Si, ≤2.0% Al, 0.05 to 1.5% Mn, 0.02 to 0.5% P, ≤0.004% S, ≤0.004% N and ≤0.004% Ti, wherein regarding magnetic flux densities, B 10 (D)≥0.98×[B 10 (L)+B 10 (C)]/2, B 50 (D)≥0.98×[B 50 (L)+B 50 (C)]/2, and [B 50 (L)+B 50 (C)+2×B 50 (D)]/4≥1.65(T), are satisfied. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种具有降低的磁各向异性并且非常适合于模块型电动机的非取向磁钢板，并提供其制造方法。解决方案：无取向电磁钢板具有质量分数为：含有≤0.005％C，2.5〜4.0％Si，≤2.0％Al，0.05〜1.5％Mn，0.02〜0.5％P，≤0.004 ％S，≤0.004％N，≤0.004％Ti，其中关于磁通密度，B 10（D）≥0.98×[B 10 （L）+ B < SB> 10（C）] / 2，B 50（D）≥0.98×[B 50 （L）+ B SB>（C）] / 2和[B 50 （L）+ B 50（C）+ 2×B 50 ）] /4≥1.65（T）。版权所有（C）2006，JPO＆NCIPI

5. 发明专利

JP2005290445A Method for preparing annealing separating agent slurry and method for producing grain oriented silicon steel sheet 审中-公开
标题翻译：制备退火分离剂浆料的方法和生产面向硅的硅钢板的方法
公开(公告)号：JP2005290445A
公开(公告)日：2005-10-20
申请号：JP2004105236
申请日：2004-03-31
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： OKABE SEIJI , TOGE TETSUO , MURAKI MINEO
IPC分类号： C23C22/00 , C21D9/46 , C22C38/00 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide a method for preparing annealing separating agent slurry capable of stably reducing core loss which is used in a method for producing a grain oriented silicon steel sheet in which a forsterite film is not formed, and to provide a method for producing a grain oriented silicon steel sheet using the annealing separating agent slurry. SOLUTION: Regarding the method for preparing annealing separating agent slurry comprising chloride of 0.1 to 10 pts.mass expressed in terms of chlorine to 100 pts.mass magnesia, in the case, as the chloride, water-soluble chloride is added, a solution obtained by dissolving the water-soluble chloride into water is used; in the case water-insoluble chloride is added, chloride grains in which the cumulative 90% size is ≤20 μm are used; and in the case Sn chloride and/or Sb chloride is added, a chloride solution obtained by charging Sn chloride and/or Sb chloride into water or slurry stirred at a flow velocity of ≥0.2 m/s, and a chloride-dispersed mixed solution are used, so as to prepare the annealing separating agent slurry for a grain oriented silicon steel sheet. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种制备能够稳定地降低铁损的退火分离剂浆料的方法，该方法用于制备不形成镁橄榄石膜的晶粒取向硅钢板的方法，并提供使用退火分离剂浆料的晶粒取向硅钢板的制造方法。解决方案：关于制备包含0.1至10质量ppm的氯化物的退火分离剂浆料的方法，以氯表示至100质量度的氧化镁，在这种情况下，作为氯化物，加入水溶性氯化物，使用通过将水溶性氯化物溶解在水中得到的溶液; 在加入水不溶性氯化物的情况下，使用累积90％尺寸≤20μm的氯化物粒子; 在添加氯化锡和/或氯化Sb的情况下，将氯化锡和/或氯化Sb中的氯化物和/或氯化钡加入水中或以≥0.2m/ s的流速搅拌的浆料和氯化物分散混合溶液，以制备晶粒取向硅钢板的退火分离剂浆料。版权所有（C）2006，JPO＆NCIPI

6. 发明专利

JP2005264236A Grain oriented silicon steel sheet having extremely low core loss and excellent film adhesion and its production method 有权
标题翻译：具有极低的核心损失和优异的薄膜粘合剂及其生产方法的面向硅的硅钢片
公开(公告)号：JP2005264236A
公开(公告)日：2005-09-29
申请号：JP2004078754
申请日：2004-03-18
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： TOGE TETSUO , HINA EIJI , MURAKI MINEO
IPC分类号： C23C22/00 , C22C38/00 , C22C38/04 , C22C38/60 , H01F1/16 , H01F1/18
摘要： PROBLEM TO BE SOLVED: To provide a grain oriented silicon steel sheet having extremely low core loss and excellent film adhesion even after annealing for high temperature stress relieving. SOLUTION: Regarding the grain oriented silicon steel sheet has an amorphous film containing titanium and nitrogen formed on the surface, wherein the ratio of the number of Ti atoms to the number of N atoms (Ti/N) in the film is controlled to >1 to ≤5. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：即使在高温应力消除退火之后，也提供具有极低的铁心损耗和优异的膜粘合性的晶粒取向硅钢板。解决方案：关于晶粒取向硅钢片具有在表面上形成的含有钛和氮的非晶体膜，其中控制膜中Ti原子数与N原子数（Ti / N）的比例 > 1〜≤5。版权所有（C）2005，JPO＆NCIPI

7. 发明专利

JP2005240079A Grain oriented silicon steel sheet low in iron loss deterioration ratio 审中-公开
标题翻译：颗粒定向硅钢板低于铁损测量比
公开(公告)号：JP2005240079A
公开(公告)日：2005-09-08
申请号：JP2004049184
申请日：2004-02-25
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： HIRATANI TATSUHIKO , WATANABE MAKOTO , MURAKI MINEO
IPC分类号： C23C22/00 , C21D9/46 , C22C38/00 , C22C38/60 , H01F1/16 , H01F1/18
CPC分类号： Y02P10/212
摘要： PROBLEM TO BE SOLVED: To provide a grain oriented silicon steel sheet low in iron loss deterioration ratio which is appropriately usable for iron cores, such as laminated iron cores and EI cores, which are high in the deterioration of the characteristics of the portions magnetized in a direction perpendicular to the rolling of the sheet. SOLUTION: The grain oriented silicon steel sheet has an insulating film of ≤3 MPa in tension on the grain oriented silicon steel sheet of the material of ≥3 to ≤8° in the average value α a of the slippage angle from the rolling direction of a crystal grain 001 axis and ≤0.5 in the ratio α (a) /α a of the standard deviation (a) of the slippage angle to the average value α a of the slippage angle and is small in the iron loss deterioration ratio. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供低铁损恶化率的晶粒取向硅钢片，其可适用于铁芯的层叠铁芯和EI铁心，其特征在于，在垂直于片材滚动的方向上磁化的部分。解决方案：晶粒取向硅钢板在平均值α a （a） /α a 的晶粒001轴的轧制方向的滑动角度≤0.5 与滑移角的平均值α a 的滑移角度，铁损退化率小。版权所有（C）2005，JPO＆NCIPI

8. 发明专利

JP2004225153A Method for producing grain-oriented electrical steel sheet 有权
公开(公告)号：JP2004225153A
公开(公告)日：2004-08-12
申请号：JP2003017953
申请日：2003-01-27
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： HAYAKAWA YASUYUKI , IMAMURA TAKESHI , MURAKI MINEO
IPC分类号： B21B3/02 , C21D9/46 , C22C38/00 , C22C38/06 , C22C38/58 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide a new grain-oriented electrical steel sheet excellent in a punching-out workability and a magnetic characteristic, especially, the magnetic characteristic in the direction orthogonal to the rolling. SOLUTION: To a hot-rolled plate obtained by hot-rolling after heating a steel slab having component composition by mass% of ≤ 0.08% C, 1.0-4.0% Si, 0.005-3.0% Mn, 0.010-0.030% sol.Al and 30-100 ppm N and reduced to ≤ 50 ppm S and Se at ≥ 1200°C, cold-rolling is applied at one time or two or more times interposing an intermediate annealing, and successively, recrystallize-annealing combined with decarburization is performed and thereafter, a last finish-annealing is performed without applying an annealing parting agent mainly containing MgO. COPYRIGHT: (C)2004,JPO&NCIPI

9. 发明专利

JP2004191237A Method of evaluating manufacturing condition of grain-oriented magnetic steel sheet and method of manufacturing the steel sheet 审中-公开
公开(公告)号：JP2004191237A
公开(公告)日：2004-07-08
申请号：JP2002360801
申请日：2002-12-12
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： FUJIMURA TORU , SATO SUSUMU , WATANABE MAKOTO , MURAKI MINEO
IPC分类号： G01N21/67 , C21D9/46 , C22C38/00
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing a grain-oriented magnetic steel sheet excellent in magnetic characteristics, which evaluates the quality of a final product beforehand in a stage after decarbonization/annealing treatment, enhances the yield of the final product and controls the manufacturing condition on the basis of an evaluated value.
SOLUTION: In the method of evaluating the manufacturing condition of the magnetic steel sheet, a sample is taken out from the steel sheet in the stage after decarbonization/annealing in a manufacturing process and one surface of the sample steel sheet is measured by a high frequency glow discharge emission spectrum analyzing method (rf-GDS). Then, the manufacturing process of the grain-oriented magnetic steel sheet is evaluated on the basis of a change in the depth direction of the amount of a least one element in the steel sheet.
COPYRIGHT: (C)2004,JPO&NCIPI

10. 发明专利

JP2004136424A Pre-welding grinding method of electromagnetic steel plate 审中-公开
公开(公告)号：JP2004136424A
公开(公告)日：2004-05-13
申请号：JP2002305624
申请日：2002-10-21
申请人： Jfe Steel Kk , Jfeスチール株式会社
发明人： IMAMURA TAKESHI , YOSHIKAWA SHINICHI , TOMITA HIROKI , MURAKI MINEO
IPC分类号： B24B7/12 , B23K31/00 , C21D9/46
摘要： PROBLEM TO BE SOLVED: To propose a pre-welding grinding method causing no plate rupture of a pre-welding grinding part in a secondarily recrystallized electromagnetic steel plate.
SOLUTION: When grinding a surface before welding the secondarily recrystallized electromagnetic steel plate, the grinding direction is set in the direction of at an angle of 60 degrees or less relative to the line pass direction of the plate.
COPYRIGHT: (C)2004,JPO

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