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1. 发明专利

JP2014196559A 方向性電磁鋼板およびその製造方法有权
标题翻译：面向电磁钢板及其生产方法
公开(公告)号：JP2014196559A
公开(公告)日：2014-10-16
申请号：JP2014044312
申请日：2014-03-06
申请人： Jfeスチール株式会社 , Jfe Steel Corp
发明人： MATSUDA HIROSHI , HAYAKAWA YASUYUKI , WATANABE MAKOTO , ARAGAKI YUKIHIRO , YAMAGUCHI HIROSHI , WAKISAKA YUIKO
IPC分类号： C22C38/00 , C21D8/12 , C22C38/04 , C22C38/60 , H01F1/16
摘要：【課題】増硫法を用いて製造する場合に懸念された下地被膜の不安定形成を有利に解消して、下地被膜の被膜密着性ひいては磁気特性に優れた方向性電磁鋼板を安定して得る。【解決手段】フォルステライト下地被膜付き方向性電磁鋼板の表面から板厚中心方向へのMgおよびMnの成分プロファイル分析において、Mgの濃度変化が鋼板表層部においてピークを呈し、一方、Mnの濃度変化は、鋼板表層部の濃度が板厚中心部の地鉄に比べて低いか、または鋼板表層部に板厚中心部の地鉄に比べて高い濃度ピークを有する場合には、鋼板表面からMnおよびMgの濃度ピーク位置までの距離をそれぞれt(Mn)、t(Mg)とするとき、t(Mn)>t(Mg)の関係を満足させる。【選択図】図2
摘要翻译：要解决的问题：为了稳定地获得通过使用硫增加方法有利地消除在生产中可能发生的基板膜的不稳定形成的基板膜的膜粘合性优异的磁特性的方向性电磁钢板解决方案：在从镁橄榄石基材薄膜提供的晶粒取向电工钢板的表面到中心的Mg和Mn的成分分布的分析中，Mg的浓度变化在钢板表面层部分。对于Mn的浓度变化，当钢板表面层部分的浓度在板厚的中心部分显示出比碱铁低的峰值，或者显示出高于中心部分中的碱铁的峰值在钢板表面层部分的板厚度中，晶粒取向电工钢板满足t（Mn）> t（Mg）的关系，其中t（Mn）是从钢板表面到浓度的距离 Mn的峰值位置，t（Mg）是从钢板表面到Mg的浓度峰值位置的距离。

2. 发明专利

JP2013064178A Method for producing grain-oriented electromagnetic steel sheet excellent in iron loss characteristic 有权
标题翻译：用于生产优质铁素体电磁特性的方法
公开(公告)号：JP2013064178A
公开(公告)日：2013-04-11
申请号：JP2011203349
申请日：2011-09-16
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： ARAGAKI YUKIHIRO , WATANABE MAKOTO , SENDA KUNIHIRO
IPC分类号： C21D8/12 , C22C38/00 , C22C38/60 , H01F1/16
CPC分类号： C21D8/1261 , C21D8/1222 , C21D8/1233 , C21D8/1266 , C21D8/1272 , C21D2201/05 , C22C38/001 , C22C38/002 , C22C38/008 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/08 , C22C38/12 , C22C38/14 , C22C38/16 , C22C38/34 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To produce a grain-oriented electromagnetic steel sheet which is low in iron loss over the entire length of a coil as a product.SOLUTION: This method for producing a grain-oriented electromagnetic steel sheet includes: hot-rolling a steel slab containing, by mass%, 0.001-0.10% C, 1.0-5.0% Si, 0.01-0.5% Mn, 0.003-0.050% sol.Al, 0.0010-0.020% N, and 0.005-0.040%, in total, of one or two elements selected from S and Se, cold-rolling the hot-rolled slab to a steel sheet, subjecting the steel sheet to primary recrystallization annealing, and subjecting the resultant steel sheet to final annealing. In the course of temperature rise in the primary recrystallization annealing, the speed S1 of temperature rise between T1(°C): 500+2×(NB-NA) and T2(°C): 600+2×(NB-NA) is 80°C/sec or more, and the average speed S2 of temperature rise between the temperature T2 and 750°C is 0.1-0.7 time the S1, wherein NA is the amount of N deposited after the cold rolling; and NB is the amount of N deposited after the primary recrystallization annealing.
摘要翻译：要解决的问题：制造作为产品的线圈整个长度上铁损低的晶粒取向电磁钢板。＆lt;解决方案＆gt;用于制造晶粒取向电磁钢板的方法包括：以质量％计，含有0.001-0.10％C，1.0-5.0％Si，0.01-0.5％Mn，0.003- 0.050％sol.Al，0.0010-0.020％N和0.005-0.040％，总共选自S和Se中的一种或两种元素，将热轧板坯冷轧成钢板，将钢板一次再结晶退火，并对所得到的钢板进行最终退火。在一次再结晶退火过程中，T1（℃）：500 + 2×（NB-NA）和T2（℃）：600 + 2×（NB-NA）之间的温度升高速度S1 为80℃/秒以上，温度T2和750℃之间的温度上升的平均速度S2为S1的0.1-0.7倍，其中NA为冷轧后沉积的N量; NB是在一次再结晶退火后沉积的N量。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2012207278A Method for manufacturing grain-oriented electromagnetic steel sheet 有权
标题翻译：制造面向导电电磁钢板的方法
公开(公告)号：JP2012207278A
公开(公告)日：2012-10-25
申请号：JP2011074313
申请日：2011-03-30
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： SENDA KUNIHIRO , WATANABE MAKOTO , ARAGAKI YUKIHIRO , OMURA TAKESHI
IPC分类号： C21D8/12 , C22C38/00 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a grain-oriented electromagnetic steel sheet in which secondary recrystallized grains are made into fine grains over the whole length of a product coil and iron loss is reduced.SOLUTION: In the method for manufacturing the grain-oriented electromagnetic steel sheet, a steel slab containing 0.001-0.20% C, 1.0-5.0% Si, 0.03-1.0% Mn, 0.005-0.040% one or two of S and Se, 0.003-0.050% sol.Al, and 0.0010-0.020% N, is hot-rolled, is cold-rolled to obtained a final sheet thickness, then is subjected to primary recrystallization annealing, and is subjected to final finish annealing after applied with an annealing separating agent consisting of mainly MgO. In the temperature rising step in the primary recrystallization annealing, a temperature rising rate Sduring 300-600°C is set at ≥100°C/s, a temperature rising rate Sduring 600-700°C is set in the range of 30 to (0.5×S)°C/s, and an oxidizing potential P/Pduring 300-700°C is preferably ≤0.05.
摘要翻译：要解决的问题：提供一种制造在产品线圈的整个长度上将二次再结晶晶粒制成细晶粒的方向性电磁钢板的方法，并且减少铁损。解决方案：在晶粒取向电磁钢板的制造方法中，将含有0.001-0.20％C，1.0-5.0％Si，0.03-1.0％Mn，0.005-0.040％S中的一种或两种的钢坯和 Se，0.003-0.050％sol.Al和0.0010-0.020％N进行热轧，冷轧以获得最终的板厚，然后进行一次再结晶退火，并在施加后进行最终成品退火具有由MgO组成的退火分离剂。在一次再结晶退火的升温阶段，在300〜600℃的温度上升速度S 1 设定为≥100℃/ s，升温速度S 600-700°C的 2 设定在30〜（0.5×S 1 ）°C / s的范围内，并且在300-700℃期间的氧化电位P H2 优选≤0.05。版权所有（C）2013，JPO＆INPIT

4. 发明专利

JP2012093185A Salt solution spray device 审中-公开
标题翻译：盐溶液喷雾装置
公开(公告)号：JP2012093185A
公开(公告)日：2012-05-17
申请号：JP2010239900
申请日：2010-10-26
申请人： Jfe Steel Corp , Jfe Techno Research Corp , Jfeスチール株式会社 , Jfeテクノリサーチ株式会社 , Suga Test Instr Co Ltd , スガ試験機株式会社
发明人： NAKAHARA HISANAO , FUJITA SAKAE , FUJIBAYASHI NOBUE , SUGA SHIGEO , WATANABE MAKOTO
IPC分类号： G01N17/00
摘要： PROBLEM TO BE SOLVED: To provide a salt solution spray device capable of uniformly spraying salt solution particles on a surface of a specimen and controlling coating weight.SOLUTION: A salt solution spray device comprises a device body 11 which constitutes a solution spray chamber 12 for spraying a salt solution on a surface of a metal specimen 13, and a solution sprayer 15 which is arranged in the solution spray chamber 12 and has a gas-liquid injection nozzle in downward direction. The solution spray chamber 12 is provided with a blower 25 which sends air to the solution spray chamber 12 from above the solution sprayer 15, and an exhaust system 28 which exhausts the air sent from the blower 25 to the solution spray chamber 12 from a position below a specimen stand 17 transported to a lower position of the solution sprayer 15.
摘要翻译：要解决的问题：提供能够在试样表面上均匀地喷洒盐溶液颗粒并控制涂层重量的盐溶液喷雾装置。解决方案：盐溶液喷雾装置包括装置主体11，其构成用于在金属试样13的表面上喷射盐溶液的溶液喷雾室12和布置在溶液喷雾室12中的溶液喷雾器15 并具有向下方向的气液注入喷嘴。溶液喷雾室12设置有鼓风机25，其从溶液喷雾器15的上方将空气送到溶液喷雾室12;以及排气系统28，其将从鼓风机25送出的空气排出到溶液喷雾室12的位置在样品架17下方运送到溶液喷雾器15的较低位置。版权所有（C）2012，JPO＆INPIT

5. 发明专利

JP2011068968A Method for manufacturing grain-oriented electrical steel sheet 有权
标题翻译：制造面向导电电工钢板的方法
公开(公告)号：JP2011068968A
公开(公告)日：2011-04-07
申请号：JP2009222294
申请日：2009-09-28
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： WATANABE MAKOTO , HAYAKAWA YASUYUKI , TAKASHIMA MINORU
IPC分类号： C21D8/12 , C22C38/00 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide an advantageous method for manufacturing a grain-oriented electrical steel sheet, which can stably manufacture the grain-oriented electrical steel sheet superior in properties of the coating film and magnetic properties as well. SOLUTION: In a process of manufacturing the grain-oriented electrical steel sheet which includes: preparing a steel slab which contains 0.01-0.10% C, 1.0-5.0% Si, 0.5% or less Mn without containing an inhibitor or further contains an appropriate amount of Al, N, Mn, S and/or Se as an inhibitor; hot-rolling the steel slab; annealing the hot-rolled plate; cold-rolling the plate twice while sandwiching intermediate annealing to reduce the sheet thickness to the final thickness; subsequently subjecting the sheet to primary recrystallization annealing; and subjecting the sheet to secondary recrystallization annealing, the method for manufacturing the grain-oriented electrical steel sheet further includes controlling the depth of a desiliconized layer to be obtained after the hot-rolled plate has been annealed to 1 μm or more by adjusting the annealing condition for the hot-rolled plate and/or the subsequent descaling condition, and also removing the scale produced after the intermediate annealing. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：解决问题的方案：提供一种制造方向性电磁钢板的有利方法，其可以稳定地制造出优异的涂膜性能和磁性能的方向性电磁钢板。解决方案：在制造方向性电磁钢板的方法中，其包括：制备含有0.01-0.10％C，1.0-5.0％Si，0.5％或更少的Mn而不含有抑制剂的钢坯，或进一步包含适量的Al，N，Mn，S和/或Se作为抑制剂; 热轧钢板; 退火热轧板; 冷却板两次，夹着中间退火，将板厚减至最终厚度; 随后对片材进行一次再结晶退火; 并且对片材进行二次再结晶退火时，方向性电磁钢板的制造方法还包括通过调整退火来控制将热轧板退火至1μm以上后得到的脱硅层的深度热轧板的条件和/或随后的除垢条件，以及除去中间退火后产生的氧化皮。版权所有（C）2011，JPO＆INPIT

6. 发明专利

JP2014095129A Grain oriented silicon steel sheet and method for producing the same 有权
标题翻译：颗粒导向硅钢板及其制造方法
公开(公告)号：JP2014095129A
公开(公告)日：2014-05-22
申请号：JP2012247717
申请日：2012-11-09
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： WATANABE MAKOTO , HAYAKAWA YASUYUKI , YAMAGUCHI HIROSHI
IPC分类号： C22C38/00 , C21D8/12 , C21D9/46 , C22C38/04 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To obtain a grain oriented silicon steel sheet, even in the case where a film containing no chromium is applied as a tension film, having high hygroscopic properties on a level same as that in the case where a chromium-containing film is formed.SOLUTION: Regarding the grain oriented silicon steel sheet in which the surface of a steel sheet is provided with a forsterite-based base film and a phosphate-based tension application film containing no chromium, the tension application film is formed by applying a phosphate-based coating treatment liquid containing no chromium to the surface of the forsterite-based base film containing Mn by 0.02 to 0.20 g/mexpressed in terms of weight and S by 0.01 to 0.10 g/mexpressed in terms of weight after final finish annealing and performing baking.
摘要翻译：要解决的问题为了获得晶粒取向硅钢板，即使在不含铬的膜作为张力膜的情况下，具有高吸湿性的水平与含铬膜的情况相同形成。解决方案：关于钢板的表面设置有镁橄榄石基底膜的晶粒取向硅钢片和不含铬的磷酸盐系张力施加膜，通过施加张力施加膜，形成张力施加膜含有不含铬的磷酸盐系涂布处理液含有以重量计0.02〜0.20g /重量的Mn的镁橄榄石类基膜表面，S为最终成品退火后的重量0.01〜0.10g / 进行烘烤。

7. 发明专利

JP2014025106A Method for producing grain oriented silicon steel sheet 有权
标题翻译：生产面向硅的钢板的方法
公开(公告)号：JP2014025106A
公开(公告)日：2014-02-06
申请号：JP2012165516
申请日：2012-07-26
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： IMAMURA TAKESHI , ARAGAKI YUKIHIRO , WATANABE MAKOTO , SUEHIRO RYUICHI , TAKAMIYA TOSHIHITO
IPC分类号： C21D8/12 , C21D9/46 , C22C38/00 , C22C38/60 , H01F1/16
CPC分类号： C21D9/46 , C21D6/004 , C21D6/005 , C21D6/008 , C21D8/12 , C21D8/1222 , C21D8/1233 , C21D8/1255 , C21D8/1261 , C21D8/1266 , C21D8/1272 , C21D8/1283 , C21D2201/05 , C22C38/00 , C22C38/001 , C22C38/002 , C22C38/008 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/12 , C22C38/16 , C22C38/34 , C22C38/40 , C22C38/60 , H01F1/14775 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a grain oriented silicon steel sheet having a low core loss and a reduced variation in iron core value compared with the conventional technique by adjusting a temperature rising pattern upon carburization annealing.SOLUTION: The method for producing a grain oriented silicon steel sheet is characterized in that, in a method for producing a grain oriented silicon steel sheet composed of a series of steps in which a steel stock comprising, by mass, 0.002 to 0.10% C, 2.0 to 8.0% Si and 0.005 to 1.0% Mn is subjected to hot rolling to form into a hot-rolled sheet, is, if required subjected to hot rolled sheet annealing, is subjected to cold rolling for one time or two or more times including process annealing to form into a cold-rolled sheet with a final sheet thickness, and is subjected to decarburization annealing also worked as primary recrystallization annealing, and the surface of the steel sheet is coated with a separation agent for annealing, and finish annealing is performed, in the decarburization annealing, rapid heating is performed at 50°C/s or higher in the section of 200 to 700°C, it is held for 1 to 10 seconds at any temperature in the range of 250 to 600°C.
摘要翻译：要解决的问题：提供一种通过调节渗碳退火时的升温图案，与传统技术相比，具有低铁损和铁芯值变化的晶粒取向硅钢板的制造方法。解决方案：制造晶粒取向硅钢板的特征在于，在由以下的一系列工序构成的晶粒取向硅钢板的制造方法中，其中，通过以质量计含有0.002〜0.10％的C，2.0〜8.0％的Si，将0.005〜1.0％的Mn进行热轧成型为热轧板，如果需要进行热轧板退火，则进行冷轧1次以上2次以上的加工退火，形成将具有最终板厚的冷轧板进行一次再结晶退火，并进行脱碳退火，并且将钢板的表面涂覆有分离剂f 或退火，并进行最终退火，在脱碳退火中，在200〜700℃的部分中以50℃/ s以上进行快速加热，在任意温度范围内保持1〜10秒钟 250〜600℃。

8. 发明专利

JP2013057119A Method for producing grain-oriented electrical steel sheet 有权
标题翻译：生产面向电工钢板的方法
公开(公告)号：JP2013057119A
公开(公告)日：2013-03-28
申请号：JP2012161139
申请日：2012-07-20
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： WATANABE MAKOTO , ARAGAKI YUKIHIRO , TAKAMIYA TOSHITO , OKUBO TOMOYUKI , SENDA KUNIHIRO
IPC分类号： C21D8/12 , C22C38/00 , C22C38/60 , H01F1/16
CPC分类号： C21D8/1272 , C21D8/12 , C21D8/1244 , C21D8/1283 , C21D2201/05 , C22C38/001 , C22C38/004 , C22C38/02 , C22C38/04 , C22C38/06 , C22C38/16 , C22C38/60 , C23C22/33 , C23C22/74 , H01F1/14775 , H01F1/16 , H01F41/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a grain-oriented electrical steel sheet excellent in core loss property and film characteristic.SOLUTION: In the method for producing a grain-oriented electrical steel sheet in which a steel slab that contains by mass, C:0.001-0.10%, Si:1.0-5.0%, Mn:0.01-1.0%, S and Se: 0.01-0.05% in total, sol.Al:0.003-0.050%, and N:0.001-0.020% is subjected to hot rolling, cold rolling, the primary recrystallization annealing, the application of an annealing separation agent by using MgO as the principal ingredient, and finishing annealing, the rate of temperature rise S1 between 500-600°C in the primary recrystallization annealing is at least 100°C/s, the rate of temperature rise S2 between 600-700°C is 30-0.6×S1°C/s, and the total content W (mol%) to MgO of the elements contained in the annealing separation agent in which the ion radius is 0.6-1.3 Å and the attraction between the ion and oxygen is at most 0.7 Å-2 is regulated to satisfy 0.01S2-5.5≤Ln(W)≤0.01S2-4.3.
摘要翻译：解决的问题：提供一种磁芯损耗特性和膜特性优异的方向性电磁钢板的制造方法。解决方案：在用于制造质量为C：0.001-0.10％，Si：1.0-5.0％，Mn：0.01-1.0％的钢坯的S型钢板的制造方法中，S和 Se：0.01-0.05％，sol.Al:0.003-0.050%，N：0.001-0.020％进行热轧，冷轧，一次再结晶退火，使用MgO作为退火分离剂主要成分和精加工退火，一次再结晶退火中的500-600℃之间的升温速度S1至少为100℃/ s，600-700℃之间的升温速度为30-0.6 ×S1℃/ s，离子半径为0.6〜1.3的退火分离剂中所含的元素的MgO的总含量W（摩尔％），离子与氧之间的吸引力为0.7以下 -2被调节为满足0.01S2-5.5≤Ln（W）≤0.01S2-4.3。版权所有（C）2013，JPO＆INPIT

9. 发明专利

JP2012158799A Treatment liquid for chromeless stress coating, and method for forming chromeless stress coating 有权
标题翻译：用于无色应力涂层的处理液和形成无色应力涂层的方法
公开(公告)号：JP2012158799A
公开(公告)日：2012-08-23
申请号：JP2011018926
申请日：2011-01-31
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： TERAJIMA TAKASHI , TAKASHIMA MINORU , WATANABE MAKOTO
IPC分类号： C23C22/22 , C23C22/00
CPC分类号： C23C22/22 , C23C22/08 , C23C22/188 , C23C22/20 , C23C22/74
摘要： PROBLEM TO BE SOLVED: To provide a treatment liquid capable of obtaining a chromeless stress coating having both excellent moisture absorption resistance and high iron loss reduction effect by sufficient tension application.SOLUTION: Colloidal silica of 20 pts.mass in terms of solid content is blended with 10 to 80 pts.mass of one or more kinds selected from the phosphates of Mg, Al, Ca, Fe, Ba, Sr, Zn and Mn, and 1 to 30 pts.mass of a nitrogen-containing compound in such a manner that the N/P ratio in the coating is 0.10 or more in terms of mass ratio.

10. 发明专利

JP2012057190A Method of manufacturing grain-oriented magnetic steel sheet 有权
标题翻译：制造面向磁性的钢板的方法
公开(公告)号：JP2012057190A
公开(公告)日：2012-03-22
申请号：JP2010198813
申请日：2010-09-06
申请人： Jfe Steel Corp , Jfeスチール株式会社
发明人： OKUBO TOMOYUKI , WATANABE MAKOTO , TAKAMIYA TOSHITO
IPC分类号： C21D9/46 , C22C38/00 , C22C38/60 , C23C22/00
摘要： PROBLEM TO BE SOLVED: To provide a method of advantageously manufacturing a grain-oriented magnetic steel sheet excelling in an iron loss characteristic.SOLUTION: When manufacturing a grain-oriented magnetic steel sheet using a steel slab containing, by mass%, 0.02-0.12% of C, 2.0-4.0% of Si, 0.02-0.20% of Mn, 0.01-0.05% of sol. Al, 0.004-0.012% of N, 0.01-0.20% of Sb, 0.005-0.20% of Cu and 0.010-0.040% of S and/or Se, an annealing separating agent containing 1-10 pts.mass of SnOin 100 pts.mass of MgO and 0.001-10 pts.mass of a B compound in terms of B is used, wherein SnOand the B compound satisfy a relationship of [B compound (pts.mass in terms of B)]>0.034×10, and final finish annealing is performed wherein the annealing separating agent is kept at 700-860°C of an elevated temperature process for 10-200 h, and a temperature region of 900-1,050°C is heated at 2-50°C/h in a H-containing atmosphere.
摘要翻译：要解决的问题：提供一种有利地制造优异的铁损特性的晶粒取向电磁钢板的方法。＆lt;解决方案＆gt;使用以质量％计含有C：0.02〜0.12％，Si：2.0〜4.0％，Mn：0.02〜0.20％，Mn：0.01-0.05％溶胶。 Al，0.004-0.012％的N，0.01-0.20％的Sb，0.005-0.20％的Cu和0.010-0.040％的S和/或Se，退火分离剂，含有1-10质量度的SnO 2 B化合物满足[B化合物（B））> 0.034×10 <= 0.119×[SnO 2（pts.mass）] 的关系，进行最终成品退火，其中退火分离剂在高温工艺的700-860℃保持10-200小时，900-150℃的温度区域以2-50℃/ h加热一个H 2 的气氛。版权所有（C）2012，JPO＆INPIT

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