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1. 发明专利

JPH0674285B2 失效
公开(公告)号：JPH0674285B2
公开(公告)日：1994-09-21
申请号：JP1577386
申请日：1986-01-29
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： KASAI KYOSHI , HATSUTORI MASAYUKI , TAKEUCHI HIROMI , HIRAI HARUHIRO , SAKURAI NOBUO
IPC分类号： C08F2/16 , C08F2/18 , C08F2/22

2. 发明专利

JPS5947214A Production of improved rubber-like polymer 失效
标题翻译：改进的橡胶状聚合物的生产
公开(公告)号：JPS5947214A
公开(公告)日：1984-03-16
申请号：JP15822082
申请日：1982-09-13
申请人： Japan Synthetic Rubber Co Ltd
发明人： TAGATA NOBUO , TAKEUCHI HIROMI , TAKEUCHI YOSHIHIRO , ODA MASARU
IPC分类号： C08F2/00 , B01J19/18 , C08F36/00 , C08F36/04 , C08F236/00 , C08F236/10
CPC分类号： B01J19/1862 , B01J2219/00168
摘要： PURPOSE: To obtain a polymer of uniform quality in the polymerization process of a synthetic rubber, by measuring the Mooney viscosity, Mooney viscosity- polymer conversion, overall styrene content and solution viscosity by means of a GPC device and automatically controlling the process so as to eliminate the differences between the measured and the set values.
CONSTITUTION: During and after the polymerization reaction of a synthetic rubber, the polymerization mixture is shunted and diluted in an automatic sampling/ diluting device 4, and the diluted mixture is passed through a GPC device 5. From the GPC chromatogram produced by the above device, at least one factor for controlling the reaction selected from the group consisting of viscosity, viscosity-conversion, overall styrene content and solution viscosity is determined by means of an arithmetic estimation unit 6. Then, the above at least one reaction-controlling factor is controlled according to its difference from the set value to obtain the desired polymer. From the factors obtained from the above GPC chromatogram, the Mooney viscosity is determined according to the estimating equations I , II, and III wherein MV is a Mooney viscosity, A is a Mn or the like, B is Mn/M or the like, C is λ, D is IP, and K, K
0W5 , α, β, and γ are constants.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：为了在合成橡胶的聚合过程中获得均匀质量的聚合物，通过GPC装置测量门尼粘度，门尼粘度 - 聚合物转化率，总苯乙烯含量和溶液粘度，并自动控制工艺，消除测量值和设定值之间的差异。构成：在合成橡胶的聚合反应过程中和之后，将聚合混合物分流并在自动取样/稀释装置4中稀释，稀释的混合物通过GPC装置5.从由上述装置产生的GPC色谱图通过算术估计单元6确定至少一个用于控制选自粘度，粘度转化率，总苯乙烯含量和溶液粘度的反应的因子。然后，上述至少一个反应控制因子是根据其与设定值的差异来控制以获得所需的聚合物。根据上述GPC色谱图得到的因子，根据估计方程式I，II和III，其中MV为门尼粘度，A为Mn等，B为Mn / M等，测定门尼粘度， C是λ，D是IP，K，K0-5，α，β和γ是常数。

3. 发明专利

JPS61215605A PRODUCTION OF POLYMER PARTICLE 失效
公开(公告)号：JPS61215605A
公开(公告)日：1986-09-25
申请号：JP5784585
申请日：1985-03-22
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： HATTORI MASAYUKI , TAKEUCHI HIROMI , KASAI KIYOSHI , SAKURAI NOBUO
IPC分类号： C08F2/00 , C08F2/18 , C08F212/00 , C08F212/08
摘要： PURPOSE:To obtain polymer particles of a large particle diameter, by allowing seed particles dispersed in water to swell by the absorption of an organic swelling agent of a small water solubility, allowing the swollen seed particles to absorb a polymerizable monomer and polymerizing the monomer in this dispersion in the presence of a suspension protecting agent at a specified rate of polymerization. CONSTITUTION:Seed particles such as polystyrene, polyvinyl acetate or the like particles are dispersed in a dispersing medium. A swelling aid comprising an organic compound of a water solubility

4. 发明专利

JPS6187734A Production of hollow polymer particle 失效
标题翻译：中空聚合物颗粒的生产
公开(公告)号：JPS6187734A
公开(公告)日：1986-05-06
申请号：JP20617284
申请日：1984-10-03
申请人： Japan Synthetic Rubber Co Ltd
发明人： HATTORI MASAYUKI , TAKEUCHI HIROMI , KASAI KIYOSHI , SAKURAI NOBUO
IPC分类号： C08F2/00 , B01J13/18 , C08F2/18 , C08F2/44 , C08F2/50 , C08J9/28 , C08J9/32
CPC分类号： B01J13/185 , Y10T428/2987
摘要： PURPOSE:To facilitate the formation of hollow polymer particles, by polymerizing a suspension containing a hydrophilic monomer, a crosslinking monomer and an oily substance and removing the oil substance contained within the produced capsular polymer particles. CONSTITUTION:A suspension containing 100pts.wt. monomer component containing 5-70pts.wt. hydrophilic monomer (e.g., vinylpyridine or 2- hydroxyethyl methacrylate) and 1-40pts.wt. crosslinking monomer (e.g., divinylbenzene or ethylene glycol dimethacrylate) and 1-1,000pts.wt. oily substance (e.g., benzene or toluene) is prepared. The monomer component is polymerized by suspension polymerization to produce capsular polymer particles containing the oil substance within their insides. The oily substance contained within them is removed by evaporation to obtain hollow polymer particles suitable as an organic filler or the like.
摘要翻译：目的：为了促进中空聚合物颗粒的形成，通过聚合含有亲水性单体，交联单体和油性物质的悬浮液并除去生产的胶囊聚合物颗粒中所含的油物质。构成：含有100pts.wt。单体组分含5-70pts.wt。亲水性单体（例如乙烯基吡啶或甲基丙烯酸2-羟乙酯）和1-40pts.wt。交联单体（例如二乙烯基苯或乙二醇二甲基丙烯酸酯）和1-1,000pts.wt。制备油状物质（如苯或甲苯）。单体组分通过悬浮聚合聚合以产生其内部含有油物质的囊状聚合物颗粒。通过蒸发除去其中所含的油状物质，得到适合作为有机填料等的中空聚合物颗粒。

5. 发明专利

JPH0468324B2 失效
公开(公告)号：JPH0468324B2
公开(公告)日：1992-11-02
申请号：JP26606485
申请日：1985-11-28
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： KASAI KYOSHI , HATSUTORI MASAYUKI , TAKEUCHI HIROMI , SAKURAI NOBUO
IPC分类号： C08L51/00 , B01J13/02 , C08F2/18 , C08F2/44 , C08F257/00 , C08F257/02 , C08F265/00 , C08F265/02 , C08F265/06 , C08F279/00 , C08F279/02 , C08K5/00 , C08L51/02 , C08L101/00

6. 发明专利

JPS62121701A PRODUCTION OF POLYMER PARTICLE 失效
公开(公告)号：JPS62121701A
公开(公告)日：1987-06-03
申请号：JP1577386
申请日：1986-01-29
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： KASAI KIYOSHI , HATTORI MASAYUKI , TAKEUCHI HIROMI , HIRAI HARUHIRO , SAKURAI NOBUO
IPC分类号： C08F2/16 , C08F2/18 , C08F2/22
摘要： PURPOSE:To facilitate the formation of polymer particles of a large diameter, by finely dispersing a polymerizable monomer in an aqueous medium to prepare a dispersion containing dispersed monomer drops having a specified number- average particle diameter, mixing this dispersion with a dispersion of seed particles and polymerizing the monomer. CONSTITUTION:A polymerizable monomer (e.g., styrene) is finely dispersed in an aqueous dispersion to prepare an aqueous polymerizable monomer dispersion which has a number-average particle diameter of dispersed liquid monomer drops not more than the number-average particle diameter of seed particles and satisfies the relationship of the formula, wherein Dm is the number-average diameter of the dispersed liquid monomer drops in a metastable state and D is the desired number-average particle diameter of the final polymer particles. This monomer dispersion is mixed with a dispersion of seed particles (e.g., polystyrene particles) to effect absorption or adsorption of the polymerizable monomer by the seed particles. The polymeizable monomer is polymerized in the presence of a polymerization initiator to obtain large polymer particles having a particle diameter of 0.1-500mum.

7. 发明专利

JPS61215604A PRODUCTION OF POLYMER PARTICLE 失效
公开(公告)号：JPS61215604A
公开(公告)日：1986-09-25
申请号：JP5613685
申请日：1985-03-22
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： HATTORI MASAYUKI , TAKEUCHI HIROMI , KASAI KIYOSHI , SAKURAI NOBUO
IPC分类号： C08F2/00 , C08F2/18 , C08F8/12 , C08F212/00 , C08F212/08
摘要： PURPOSE:To facilitate the formation of monodisperse polymer particles of a relatively large particle diameter, by mixing an aqueous dispersion of seed particles with an organic swelling aid of a specified property, allowing the seed particles to swell by the absorption of the aid, adding a polymerizable monomer to this dispersion to allow the seed particles to adsorb it and polymerizing the monomer in this dispersion. CONSTITUTION:An aqueous dispersion of seed particles comprising polystyrene, polyvinyl acetate or the like is mixed with an aqueous dispersion of a swelling aid comprising an organic compound having a wager solubility

8. 发明专利

JPS61190504A PRODUCTION OF POLYMER PARTICLES 失效
公开(公告)号：JPS61190504A
公开(公告)日：1986-08-25
申请号：JP2929485
申请日：1985-02-19
申请人： JAPAN SYNTHETIC RUBBER CO LTD
发明人： HATTORI MASAYUKI , TAKEUCHI HIROMI , KASAI KIYOSHI , SAKURAI NOBUO
IPC分类号： C08F2/00 , C08F2/16 , C08F2/18 , C08F2/22
摘要： PURPOSE:To obtain easily the titled spherical particles having relatively large particle diameters and high monodispersion, by blending seed particles with a swelling auxiliary in an aqueous dispersion state to give swelling particles at the first stage, making the swelling particles absorb a monomer, and polymerizing the monomer. CONSTITUTION:In the first stage, an aqueous dispersion of seed particles is blended with an aqueous dispersion of a swelling auxiliary consisting of an organic compound having

9. 发明专利

JPS6195016A Spacer 失效
标题翻译： SPACER
公开(公告)号：JPS6195016A
公开(公告)日：1986-05-13
申请号：JP21524584
申请日：1984-10-16
申请人： Japan Synthetic Rubber Co Ltd
发明人： KASAI KIYOSHI , HATTORI MASAYUKI , TAKEUCHI HIROMI , SAKURAI NOBUO
IPC分类号： C08F297/00 , B41M5/132 , C08F291/00 , C08F297/08 , G02F1/133 , G02F1/1339
摘要： PURPOSE: A spacer having particle diameters with high uniformity, improved reliability of liquid crystal display device, etc., comprising polymer particles obtained by making seed polymer particles dispersed in an aqueous dispersing medium absorb a lipophilic substance, absorb a monomer, and polymerizing it with an oil-soluble polymerization initiator.
CONSTITUTION: Seed polymer particles (e.g., polystyrene, etc.) having particle diameters with high uniformity is dispersed into water to give an aqueous dispersion, a lipophilic substance (e.g., 1-chlorododecane, etc.) is emulsified and dispersed into water with soap, etc., and is added to the aqueous dispersion. A monomer (e.g., stylene, etc.) is absorbed in the seed polymer particles, incorporated with an oil-soluble polymerization initiator (e.g., azobisisobutyronitrile, etc.), and, if necessary, a polymerization adjustor (e.g., carbon tetrachloride, etc.), a water-soluble polymerization inhibitor (e.g., hydroquinone, etc.) and a polymerization reaction is done to give the aimed polymer particles.
EFFECT: A liquid crystal display device keeping thickness of liquid crystal layer in high accuracy uniformly, having high reliability and improved durability, is formed.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过使分散在水性分散介质中的种子聚合物粒子吸收亲水性物质，吸收单体，使其聚合而得到的聚合物粒子，具有均匀性高，粒径均匀性提高的液晶显示装置的可靠性提高的间隔物，油溶性聚合引发剂。构成：将具有高均匀度的粒径的种子聚合物颗粒（例如聚苯乙烯等）分散在水中以得到水分散体，将亲脂性物质（例如，1-氯十二烷等）乳化并用肥皂分散在水中等，并加入到水分散体中。将单体（例如，苯乙烯等）吸收在种子聚合物颗粒中，与油溶性聚合引发剂（例如偶氮二异丁腈等）结合，并且如果需要，可以使用聚合调节剂（例如四氯化碳等）），水溶性聚合抑制剂（例如氢醌等）和聚合反应进行，得到目标聚合物颗粒。效果：形成了具有高精度均匀地保持液晶层的厚度，具有高可靠性和耐久性的液晶显示装置。

10. 发明专利

JPS6191264A Pigment for cosmetic 失效
标题翻译：化妆品颜料
公开(公告)号：JPS6191264A
公开(公告)日：1986-05-09
申请号：JP21272884
申请日：1984-10-12
申请人： Japan Synthetic Rubber Co Ltd
发明人： TAKEUCHI HIROMI , ITO NOBUYUKI , KASAI KIYOSHI , SAKURAI NOBUO
IPC分类号： C09B67/20
摘要： PURPOSE: The titled pigment which has excellent skin hiding power and softly applicable properties, consisting of a specified crystalline conjugated diene polymer.
CONSTITUTION: A catalyst obtained by the interaction of a Co compound (A) (e.g., cobalt octylate) with an organometallic compound of a Group IWIII metal or its hydrogenated product (B) (e.g., tributylaluminum) in the presence of a conjugated diene in an amount of 1W100 times by mol that of component A, and at least one compound selected from among CS
2 , phenyl isocyanate, and a xanthogen compound are combined to give a catalyst system. In the presence of this catalyst system, a 4W5C conjugated diene (e.g., butadiene) is polymerized in an aqueous medium containing a surface active agent, a protective colloid, a metal chloride and/or calcium phosphate, giving an organic pigment which consists of a crystalline conjugated diene polymer having a degree of crystallinity of 10W100% and an average particle diameter of 0.5W20μm, used for cosmetics.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：具有优异的皮肤遮盖力和柔软性能的标题颜料，由特定的结晶共轭二烯聚合物组成。构成：通过Co化合物（A）（例如，辛酸钴）与I-III族金属的有机金属化合物或其氢化产物（B）（例如三丁基铝）在共轭物质的存在下相互作用获得的催化剂二烯的量为组分A的1-100倍摩尔量，和选自CS2，异氰酸苯酯和黄原酸化合物中的至少一种化合物组合，得到催化剂体系。在该催化剂体系的存在下，4-5C共轭二烯（例如丁二烯）在含有表面活性剂，保护胶体，金属氯化物和/或磷酸钙的水性介质中聚合，得到有机颜料，其组成为的结晶共轭二烯聚合物，其结晶度为10-100％，平均粒径为0.5-20μm，用于化妆品。

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