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1. 发明专利

JP2013212447A Method for regenerating and using heavy oil hydrotreating catalyst, and the heavy oil hydrotreating catalyst 审中-公开
标题翻译：再生和使用重油加氢催化剂和重油加氢催化剂的方法
公开(公告)号：JP2013212447A
公开(公告)日：2013-10-17
申请号：JP2012083120
申请日：2012-03-30
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社 , Japan Petroleum Energy Center , 一般財団法人石油エネルギー技術センター
发明人： IINO AKIRA , INAMURA KAZUHIRO , TAKAHASHI NOBUYUKI
IPC分类号： B01J29/90 , B01J38/04 , C10G45/12
摘要： PROBLEM TO BE SOLVED: To provide a method for regenerating a heavy oil hydrotreating catalyst that effectively improves catalytic performance by minimizing impairment such as a fall in catalytic performance or wear strength of the heavy oil hydrotreating catalyst whose catalytic activity is deteriorated by the adhesion of coke.SOLUTION: A method for regenerating a heavy oil hydrotreating catalyst which is a catalyst carrying a metal compound containing at least one kind of active metal selected from metals belonging to groups VI, IX and X of the periodic table, in an inorganic oxide carrier containing crystalline aluminoslicate and a porous inorganic oxide, includes a heat treatment process for removing adhering coke by heat-treating a spent heavy oil hydrotreating catalyst after allowing heavy oil to pass through to hydrotreat the heavy oil.
摘要翻译：要解决的问题：提供一种再生重油加氢处理催化剂的方法，其通过最小化诸如催化活性由于焦炭粘附而劣化的重油加氢处理催化剂的催化性能或磨损强度的降低而有效地改善催化性能解决方案：一种重油加氢处理催化剂的再生方法，该催化剂是含有选自属于周期表第VI，IX和X族的金属的至少一种活性金属的金属化合物的催化剂，该无机氧化物载体含有结晶性铝酸钾和多孔无机氧化物，包括通过在使重油通过以重油加氢处理之后通过热处理废重油加氢处理催化剂来除去附着焦炭的热处理方法。

2. 发明专利

JP2013213107A Hydrodesulfurization apparatus using hydrocracking catalyst and hydroprocessing method of heavy oil 审中-公开
标题翻译：使用水解催化剂的氢化装置和重油加氢方法
公开(公告)号：JP2013213107A
公开(公告)日：2013-10-17
申请号：JP2012083097
申请日：2012-03-30
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社 , Japan Petroleum Energy Center , 一般財団法人石油エネルギー技術センター
发明人： KAGAMI SHIGEARI , INAMURA KAZUHIRO , TAKAHASHI NOBUYUKI
IPC分类号： C10G65/12 , C10G45/08 , C10G47/20
摘要： PROBLEM TO BE SOLVED: To provide a hydrocracking-hydrodesulfurization apparatus with which sufficient cracking activity and desulfurization activity are exhibited by using only a small amount of a hydrocracking catalyst, and to provide a hydroprocessing method of heavy oil using the apparatus.SOLUTION: In a hydrocracking-hydrodesulfurization apparatus: a hydrocracking catalyst layer formed of a hydrocracking catalyst constituted of a crystalline aluminosilicate-containing carrier with an active metal supported thereon; and an upstream side hydrodesulfurization catalyst layer formed of a hydrodesulfurization catalyst constituted of an alumina carrier with an active metal supported thereon, are accommodated in a reaction tower in such a way that the upstream side hydrodesulfurization catalyst layer is located to the side more upstream than the hydrocracking catalyst layer. In a hydroprocessing method of heavy oil, low sulfur heavy oil is produced by supplying the heavy oil to the hydrocracking-hydrodesulfurization apparatus.
摘要翻译：要解决的问题：提供一种通过仅使用少量加氢裂化催化剂显示足够的裂解活性和脱硫活性的加氢裂化加氢脱硫装置，并使用该装置提供重油的加氢处理方法。加氢裂化加氢脱硫装置：由负载有活性金属的含结晶硅铝酸盐的载体构成的加氢裂化催化剂形成的加氢裂化催化剂层; 由负载有活性金属的氧化铝载体构成的加氢脱硫催化剂形成的上游侧加氢脱硫催化剂层被容纳在反应塔中，使得上游侧加氢脱硫催化剂层位于比上述加氢裂化催化剂层。在重油的加氢处理方法中，通过向加氢裂化加氢脱硫装置供给重油来生产低硫重油。

3. 发明专利

JP2013212449A Crystalline aluminosilicate, hydrocracking catalyst for heavy oil, and method for manufacturing same 有权
标题翻译：用于重油的水晶铝氧化物，氢化裂化催化剂及其制造方法
公开(公告)号：JP2013212449A
公开(公告)日：2013-10-17
申请号：JP2012083134
申请日：2012-03-30
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社 , Jgc Catalysts & Chemicals Ltd , 日揮触媒化成株式会社 , Japan Petroleum Energy Center , 一般財団法人石油エネルギー技術センター
发明人： INAMURA KAZUHIRO , WATABE MITSUNORI , EURA SHINYA
IPC分类号： B01J29/16 , B01J37/02 , B01J37/04 , C01B39/24 , C10G47/16
CPC分类号： B01J29/084 , C01B39/24 , C10G47/16 , C10G47/18 , C10G47/20
摘要： PROBLEM TO BE SOLVED: To provide: a crystalline aluminosilicate for use in a carrier material for achieving a hydrocracking catalyst for heavy oil superior in both desulfurization activity and the cracking activity; a hydrocracking catalyst for heavy oil, having the crystalline aluminosilicate as the carrier material; and a method for manufacturing same.SOLUTION: The present invention is a crystalline aluminosilicate, a hydrocracking catalyst for heavy oil having the crystalline aluminosilicate as a component, and a method for manufacturing same. The crystalline aluminosilicate is used as a carrier material for a hydrocracking catalyst for heavy oil, wherein (a) the crystalline aluminosilicate is an ultra-stable Y-type zeolite or a metal-supported ultra-stable Y-type zeolite, and (b) the volume fraction of particles having a particle size of 10 μm or less as analyzed from particle size distribution data of a volume reference obtained by laser diffractive scattering is 95% or more.
摘要翻译：要解决的问题：提供：用于实现脱硫活性和裂化活性优异的重油加氢裂化催化剂的载体材料中的结晶性硅铝酸盐，用于重油的加氢裂化催化剂，其具有结晶硅铝酸盐作为载体材料; 及其制造方法。解决方案：本发明是结晶硅铝酸盐，具有结晶硅铝酸盐作为组分的重油加氢裂化催化剂及其制造方法。结晶硅铝酸盐用作重油加氢裂化催化剂的载体材料，其中（a）结晶硅铝酸盐是超稳定Y型沸石或金属负载型超稳定Y型沸石，（b）从通过激光衍射散射获得的体积参考值的粒度分布数据分析，粒径为10μm以下的粒子的体积分率为95％以上。

4. 发明专利

JP2011031194A Hydrocracking catalyst for heavy oil and method for hydrotreating heavy oil using the same 有权
标题翻译：用于重油的氢化裂化催化剂和使用其加氢重油的方法
公开(公告)号：JP2011031194A
公开(公告)日：2011-02-17
申请号：JP2009180946
申请日：2009-08-03
申请人： Idemitsu Kosan Co Ltd , Jgc Catalysts & Chemicals Ltd , Petroleum Energy Center , 出光興産株式会社 , 日揮触媒化成株式会社 , 財団法人石油産業活性化センター
发明人： INAMURA KAZUHIRO , IINO AKIRA , TAKAHASHI NOBUYUKI , SUNAGAWA YOJI , WATABE MITSUNORI , YAMAHATA YUICHI , EURA SHINYA , SHIRAHAMA YUJI
IPC分类号： B01J29/16 , B01J35/10 , C10G47/12 , C10G47/20
CPC分类号： C10G47/18 , B01J29/064 , B01J29/076 , B01J29/106 , B01J29/166 , B01J29/42 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/108 , B01J37/0009 , B01J37/0203 , B01J37/20 , B01J2229/42 , C10G47/20
摘要： PROBLEM TO BE SOLVED: To provide a hydrocracking catalyst achieving both the cracking activity and the desulfurization activity to the heavy oil and excellent in both functions.
SOLUTION: The heavy oil hydrocracking catalyst is obtained by supporting an active metal on a support containing crystalline aluminosilicate and a porous inorganic oxide except the crystalline aluminosilicate, wherein (a) the support contains ≥45 mass% and 40 mass% and ≤55 mass% porous inorganic oxide except the crystalline aluminosilicate, based on the total amount of the crystalline aluminosilicate and the porous inorganic oxide except the crystalline aluminosilicate; (b) the active metal comprises at least one kind of metal among group VI, group VIII, group IX and group X in the periodic table; and (c) in the pore distribution of the heavy oil hydrocracking catalyst, the total pore volume defined by 50-10,000 Å pore diameter is ≥0.40 cc/g and the ratio of middle mesopore volume having ≥100 Å and
摘要翻译：要解决的问题：提供一种加氢裂化催化剂，同时实现对重油的裂化活性和脱硫活性，并且两者的功能均优异。解决方案：重油加氢裂化催化剂通过在含有结晶硅铝酸盐的载体和除结晶硅铝酸盐之外的多孔无机氧化物的载体上负载活性金属而获得，其中（a）载体含有≥45质量％和<60质量％的结晶基于结晶硅铝酸盐和结晶硅铝酸盐以外的多孔无机氧化物的总量，结晶硅铝酸盐以外的多孔无机氧化物，≤40质量％和≤55质量％的多孔无机氧化物; （b）活性金属包含元素周期表中VI族，VIII族，IX族和X族中的至少一种金属; 和（c）在重油加氢裂化催化剂的孔分布中，孔径为50-10,000埃的孔隙体积为≥0.40立方厘米/厘米3，中孔介体体积比为≥100埃，孔径<200埃占总孔体积的≥60％。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2005082619A Method for preliminarily sulfurizing hydrogenation treatment catalyst and method for desulfurizing gas oil 有权
标题翻译：用于预硫化氢化处理催化剂的方法和用于对气体进行除油的方法
公开(公告)号：JP2005082619A
公开(公告)日：2005-03-31
申请号：JP2003312904
申请日：2003-09-04
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： HIRANO TOMOAKI , KOJIKA HIROMICHI , INAMURA KAZUHIRO
IPC分类号： B01J27/19 , C10G45/08
摘要： PROBLEM TO BE SOLVED: To provide a method for preliminarily sulfurizing a hydrogenation treatment catalyst carrying a hydrogenation active metal component in a high dispersed state, by which the catalyst can be sulfurized to exhibit the original hydrogenation activity without needing the hydrogenation of the catalyst on a preliminary sulfurization.
SOLUTION: This method for preliminarily sulfurizing the hydrogenation treatment catalyst which is specified with a reduction profile obtained by a temperature program reduction method (TPR method) and has a reduction area of ≥5% based on the total reduction area at ≤380°C is characterized by involving a process for performing a reduction treatment up to a sulfurization degree of ≥50% in a range of 120 to 230°C.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题：提供一种预先硫化含有高分散状态的氢化活性金属组分的氢化处理催化剂的方法，通过该方法，催化剂可被硫化以显示原始氢化活性，而不需要氢化催化剂进行初步硫化。
解决方案：用于通过温度程序降低法（TPR法）获得的具有还原曲线的氢化处理催化剂预硫化的方法，并且基于总还原面积≤380减小面积≥5％其特征在于涉及在120〜230℃的范围内进行至少为50％的硫化度的还原处理的方法。版权所有（C）2005，JPO＆NCIPI

6. 发明专利

JP2009242487A Method for decomposing atmospheric distillation residual oil 有权
标题翻译：用于分解大气蒸馏残留油的方法
公开(公告)号：JP2009242487A
公开(公告)日：2009-10-22
申请号：JP2008088607
申请日：2008-03-28
申请人： Idemitsu Kosan Co Ltd , Petroleum Energy Center , 出光興産株式会社 , 財団法人石油産業活性化センター
发明人： IINO AKIRA , INAMURA KAZUHIRO
IPC分类号： C10G69/04 , C10G11/00 , C10G47/16
摘要： PROBLEM TO BE SOLVED: To provide a method for decomposing an atmospheric distillation residual oil which enables to decompose an atmospheric distillation oil of a crude oil so that yield rates of individual distillates such as desulfurized naphtha, desulfurized kerosene and desulfurized gas oil are increased, while a yield rate of desulfurized heavy oil is decreased, further which enables to decompose the desulfurized heavy oil being a residual oil so that yield rates of an LPG distillate and an FCC gasoline distillate are increased and a yield rate of an LCO distillate is decreased.
SOLUTION: This method for decomposing the atmospheric distillation residual oil by hydrocracking the atmospheric distillation residual oil and submitting the obtained product oil to fluid catalytic cracking is characterized in that (a) the catalyst used for the hydrocracking is one carrying a metal on a support comprising a mixture of 45-70 mass% crystalline aluminosilicate and 30-55 mass% porous inorganic oxide, and (b) the raw material of the fluid catalytic cracking is a mixture of a residual oil obtained by the hydrocracking and a distillate with 120-400°C boiling point, and the mixing rate of the distillate in the mixture is 1-30 vol.%.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种分解常压蒸馏残油的方法，其能够分解原油的常压蒸馏油，使得脱硫石脑油，脱硫煤油和脱硫瓦斯油等各种馏出物的产率为而脱硫重油的产率进一步降低，能够使作为残油的脱硫重质油分解，使得LPG馏出物和FCC汽油馏分的产率提高，LCO馏出物的产率为减少。解决方案：通过加氢裂化常压蒸馏残油并将所得产物油提取到流化催化裂化中分解常压蒸馏残油的方法的特征在于：（a）用于加氢裂化的催化剂是将金属包含45-70质量％结晶硅铝酸盐和30-55质量％多孔无机氧化物的混合物的载体，和（b）流化催化裂化的原料是通过加氢裂化获得的残油与馏出物的混合物与 120-400℃沸点，混合物中馏出物的混合比例为1-30体积％。版权所有（C）2010，JPO＆INPIT

7. 发明专利

JP2008178843A Titanium-carrying fire-resistant inorganic oxide carrier, hydrotreating catalyst of hydrocarbon oil, and hydrotreatment method using the same 有权
标题翻译：含钛耐火无机氧化物载体，烃油的加氢催化剂和使用其的水解方法
公开(公告)号：JP2008178843A
公开(公告)日：2008-08-07
申请号：JP2007016001
申请日：2007-01-26
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： HIRANO TOMOAKI , KOJIKA HIROMICHI , INAMURA KAZUHIRO
IPC分类号： B01J27/199 , B01J37/02 , C10G45/04
摘要： PROBLEM TO BE SOLVED: To provide a titanium-carrying fire-resistant inorganic oxide carrier which has a high activity and little degradation, and is most suitable for a hydrotreating catalyst, the hydrotreating catalyst having a high activity and obtained at low cost using the same, a hydrotreatment method enabling an efficient manufacture of a hydrocarbon oil of a low sulfur content using the hydrotreating catalyst, and in addition, to provide a method of manufacturing the titanium-carrying fire-resistant inorganic oxide carrier which allows the fire-resistant inorganic oxide to carry titanium uniformly and easy.
SOLUTION: The titanium-carrying fire-resistant inorganic oxide carrier controlling a carbon amount of remaining organic matter in the titanium-carrying fire-resistant inorganic oxide carrier in a suitable range, and its manufacturing method are provided. Further, at least one selected from metals belonging to groups VI, VIII, IX, and X is supported by the fire-resistant inorganic oxide carrier to turn the hydrotreating catalyst. The hydrotreatment is carried out using the catalyst.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：为了提供具有高活性和低降解性，最适用于加氢处理催化剂的钛载体耐火无机氧化物载体，加氢处理催化剂具有高活性并以低成本获得使用该加氢处理方法能够使用加氢处理催化剂高效地制造低硫含量的烃油，另外，提供一种制造携带钛的耐火无机氧化物载体的方法，耐磨无机氧化物均匀且容易地携带钛。解决方案：提供在适当范围内控制载钛耐火无机氧化物载体中剩余有机物的碳量的载钛耐火无机氧化物载体及其制造方法。此外，选自属于VI，VIII，IX和X族的金属中的至少一种由耐火无机氧化物载体负载以转化加氢处理催化剂。使用催化剂进行加氢处理。版权所有（C）2008，JPO＆INPIT

8. 发明专利

JP2007289835A Method for judging continuous availability of used catalyst 审中-公开
标题翻译：评估使用催化剂连续可用性的方法
公开(公告)号：JP2007289835A
公开(公告)日：2007-11-08
申请号：JP2006119499
申请日：2006-04-24
申请人： Idemitsu Kosan Co Ltd , Tohoku Univ , 出光興産株式会社 , 国立大学法人東北大学
发明人： INAMURA KAZUHIRO , HIRANO TOMOAKI , KOIZUMI NAOTO , YAMADA MUNEYOSHI
IPC分类号： B01J37/00 , B01J23/88 , C10G45/10
摘要： PROBLEM TO BE SOLVED: To provide a method for quickly and correctly judging whether a used catalyst can be used continuously or not without being regenerated. SOLUTION: The method for judging the continuous availability of the used catalyst comprises the steps of: using such an analytical method of temperature-programmed oxidation that carbonaceous deposits on the used catalyst are subjected to temperature-programmed oxidation to produce carbon oxides and a relation between the amount of carbon oxides and the temperature every moment is detected and profiled; and selecting such the used catalyst that the amount of carbon oxides to be produced at ≥400°C is ≤3 mass% of the used catalyst before oxidized in terms of carbon. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种用于快速且正确地判断所使用的催化剂是否可以连续使用而不被再生的方法。用于判断所用催化剂的持续可用性的方法包括以下步骤：使用温度程序化氧化的分析方法，使所用催化剂上的碳质沉积物进行温度程序化氧化以产生碳氧化物，检测和分析碳氧化物的量与每一时刻的温度之间的关系; 并选择这样的使用催化剂，使得在≥400℃下生成的碳氧化物的量在碳的氧化之前为所使用的催化剂的3质量％。版权所有（C）2008，JPO＆INPIT

9. 发明专利

JP2008297471A Method for production of catalytically reformed gasoline 审中-公开
标题翻译：催化改性汽油的生产方法
公开(公告)号：JP2008297471A
公开(公告)日：2008-12-11
申请号：JP2007146087
申请日：2007-05-31
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： IINO AKIRA , INAMURA KAZUHIRO
IPC分类号： C10G69/08 , B01J29/076 , B01J35/10 , B01J37/02 , C10G35/04 , C10G45/02 , C10G47/20 , C10G65/02
摘要： PROBLEM TO BE SOLVED: To provide a method for production of catalytically reformed gasoline increasing production of catalytically reformed gasoline fraction, and increasing production of 6-8C aromatic hydrocarbons such as benzene, toluene and xylene, etc.
SOLUTION: The method for production of catalytically reformed gasoline comprises catalytic reformation of mixed fraction of naphtha fraction obtained by atmospheric distillation of crude oil and purified naphtha fraction obtained by hydrogenation of heavy hydrocarbons as raw materials.
COPYRIGHT: (C)2009,JPO&INPIT

10. 发明专利

JP2005013848A Carrier for hydrogenation catalyst, hydrogenation catalyst of hydrocarbon oil and hydrogenation method using the hydrogenation catalyst 审中-公开
标题翻译：氢化催化剂载体，烃油加氢催化剂和加氢催化剂加氢方法
公开(公告)号：JP2005013848A
公开(公告)日：2005-01-20
申请号：JP2003181246
申请日：2003-06-25
申请人： Idemitsu Kosan Co Ltd , Petroleum Energy Center , 出光興産株式会社 , 財団法人石油産業活性化センター
发明人： KOJIKA HIROMICHI , HIRANO TOMOAKI , SUZUKI YASUYUKI , INAMURA KAZUHIRO
IPC分类号： B01J23/10 , B01J27/19 , B01J32/00 , C10G45/04 , C10G45/08
摘要： PROBLEM TO BE SOLVED: To provide a carrier for hydrogenation catalyst which is highly active, hardly causes the deterioration and is suitable as hydrogenation catalyst, to provide a hydrogenation catalyst utilizing the carrier which is highly active and can be obtained at a low cost and a method for efficiently manufacturing hydrocarbon oil of low sulfur content which uses the hydrogenation catalyst.
SOLUTION: The carrier for hydrogenation catalyst is made by incorporating a basic oxide in a fire-resistant inorganic oxide having acidity, has a total acid amount of ≥470 μmol/g and has the ratio of strong acid amount and weak acid amount of ≤0.37. The hydrogenation catalyst of hydrocarbon oil is made by carrying at least one kind of metal selected from metals belonging to group 6, group 8 to group 10 of the periodic table. In the hydrogenation method, hydrocarbon oil is treated by using the catalyst.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供高活性的氢化催化剂载体，几乎不引起劣化并且适合作为氢化催化剂，以提供使用高活性的载体的氢化催化剂，并且可以在低成本和使用氢化催化剂的低硫含量的烃油有效生产的方法。解决方案：氢化催化剂载体是通过在具有酸性的耐火无机氧化物中引入碱性氧化物制成的，总酸量≥470μmol/ g，并且具有强酸量和弱酸量的比例 ≤0.37。烃油的氢化催化剂是通过携带选自属于周期表第6族，第8族至第10族的金属的至少一种金属而制成的。在氢化方法中，使用催化剂处理烃油。版权所有（C）2005，JPO＆NCIPI

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