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    • 5. 发明专利
    • Purification method and manufacturing method for metal complex salt compound
    • 金属复合盐化合物的纯化方法和制备方法
    • JP2011032483A
    • 2011-02-17
    • JP2010231868
    • 2010-10-14
    • Hodogaya Chem Co Ltd保土谷化学工業株式会社
    • OKUBO MASAKINANAUMI YUTAKASAWANO MASATAKA
    • C09B45/01C09B67/54C09B45/12C09B45/14G03G9/097
    • C09B45/14G03G9/09783
    • PROBLEM TO BE SOLVED: To provide a toner having good rising of electrification and capable of reproducing stable images for a long time without being affected with temperature and moisture even though repeated developments are carried out in a continuous use. SOLUTION: There is disclosed a purification method of a metal complex salt compound shown by a general formula (1) (wherein M denotes a coordination center metal such as Fe or the like, Ar is a substituted or unsubstituted aryl group, X and Y are -O- or the like, K + denotes a sodium ion or the like, and may be a mixture thereof; m denotes 1, 2, 3 or 6, p is the valence of a metal M, n denotes 1, 2 or 4, and q denotes 0 or an integer). The purification method and manufacturing method of the metal complex salt compound are characterized in that the metal complex salt compound is prepared so that the electroconductivity when the metal complex salt compound is dispersed in ion-exchanged water in an amount of 1 wt.% may be at most 110 μS/cm. COPYRIGHT: (C)2011,JPO&INPIT
    • 要解决的问题:即使在连续使用中进行重复的开发,也可以提供一种具有良好的起电升高并且能够长时间再现稳定图像而不受温度和湿度影响的调色剂。 解决方案:公开了由通式(1)表示的金属络盐化合物的纯化方法(其中M表示配位中心金属如Fe等,Ar为取代或未取代的芳基,X Y表示-O-等,K表示钠离子等,也可以是它们的混合物,m表示1,2,3或6,p表示 金属M,n表示1,2或4,q表示0或整数)。 金属络盐化合物的纯化方法和制造方法的特征在于制备金属络盐化合物,使金属络盐化合物分散在离子交换水中的量为1重量%时的导电性可以为 至多110μS/ cm。 版权所有(C)2011,JPO&INPIT
    • 7. 发明专利
    • Method for refining electrophotographic photoreceptor material, and electrophotographic photoreceptor material or intermediate of electrophotographic photoreceptor material refined with the method
    • 电子照相光电材料的制备方法,电子照相光电材料或电子照相光电材料的中间体
    • JP2005266514A
    • 2005-09-29
    • JP2004080867
    • 2004-03-19
    • Hodogaya Chem Co Ltd保土谷化学工業株式会社
    • ABE KATSUMITAKEI ATSUSHIOKUBO MASAKIANZAI MITSUTOSHI
    • G03G5/00G03G5/06
    • PROBLEM TO BE SOLVED: To provide a method for refining an electrophotographic photoreceptor material with which its electric characteristic is improved by identifying an impurity imparting most adverse effect on the electric characteristic of the electrophotographic photoreceptor and efficiently removing the impurity while avoiding repetition of the refining step in pursuing high purity and having no need to fabricate the electrophotographic photoreceptor and to measure its electric characteristic for every manufacture. SOLUTION: In the method for refining the electrophotographic photoreceptor material, its electric characteristic is improved by reducing a content of an aromatic amine compound, which is the impurity and which has a phenylenediamine substructure expressed by a general formula (2) (in the formula, R2, R3, R4 and R5 are optionally identical to or different from one another and express a hydrogen atom, a 1-4C alkyl group, a 1-4C alkoxy group, or a halogen atom, wherein R2 and R3 or R4 and R5 may optionally be bonded to each other so as to form a ring) in its molecule, to ≤0.50 mass %. The electrophotographic photoreceptor material or an intermediate of the electrophotographic photoreceptor material is refined with the method. COPYRIGHT: (C)2005,JPO&NCIPI
    • 要解决的问题:提供一种电子照相感光体材料的精制方法,通过鉴定对电子照相感光体的电特性产生最不利影响的杂质,并且有效地除去杂质,同时避免重复 精炼步骤追求高纯度,并且不需要制造电子照相感光体并测量其每个制造的电特性。 解决方案:在电子照相感光体材料的精制方法中,通过降低作为杂质的芳族胺化合物的含量,并且具有由通式(2)表示的苯二胺亚结构(在 式R2,R3,R4和R5任选地彼此相同或不同,表示氢原子,1-4C烷基,1-4C烷氧基或卤素原子,其中R2和R3或R4 并且R 5可以任选地彼此键合以形成环)至≤0.50质量%。 通过该方法精制电子照相感光体材料或电子照相感光体材料的中间体。 版权所有(C)2005,JPO&NCIPI
    • 8. 发明专利
    • Charge control agent
    • 充电控制代理
    • JP2012198553A
    • 2012-10-18
    • JP2012116374
    • 2012-05-22
    • Hodogaya Chem Co Ltd保土谷化学工業株式会社
    • OKUBO MASAKINANAMI YUSAWANO MASATAKA
    • C09B45/01G03G9/097C07F15/02C09B45/14C09B45/22G03G5/047G03G5/05G03G5/147
    • C09B45/14G03G9/09783
    • PROBLEM TO BE SOLVED: To provide toner having a favorable rise from charging and capable of reproducing a stable image for a long period without being affected by a change in temperature and humidity even when performing repeated development by continuous use.SOLUTION: A method for stably applying static charge to toner for electrostatic charge image development comprises a step of including a charge control agent which includes a metal-complex compound represented by a general formula (1), in the toner for electrostatic charge image development. When 1 wt.% of the metal-complex compound is dispersed in ion-exchange water, an electric conductivity thereof is 110 μS/cm or less. (In the formula, M represents a metal coordination center such as Fe. Ar is a substituted or non-substituted aryl group. X and Y are -O- or the like. Krepresents a sodium ion or the like or may be a mixture thereof. m represents 1, 2, 3 or 6, p is an atomic valence of metal M, n represents 1, 2, or 4, and q represents 0 or an integer.)
    • 要解决的问题:即使在通过连续使用进行反复显影时,也不会受到温度和湿度的变化的影响,提供具有充电上升的调色剂,并且能够长时间地再现稳定的图像。 < P>解决方案:静电荷调色剂稳定地用于静电荷图像显影的方法包括将包含通式(1)表示的金属络合物的电荷控制剂包括在用于静电荷的调色剂中的步骤 形象发展。 当1重量%的金属络合物分散在离子交换水中时,其导电率为110μS/ cm以下。 (式中,M表示Fe等金属配位中心,Ar表示取代或未取代的芳基,X和Y表示-O-等),K + SP >表示钠离子等或可以是其混合物,m表示1,2,3或6,p表示金属M的原子价,n表示1,2或4,q表示0或整数 。)版权所有(C)2013,JPO&INPIT
    • 10. 发明专利
    • Method for purifying electronic article material
    • 净化电子材料的方法
    • JP2005289842A
    • 2005-10-20
    • JP2004103986
    • 2004-03-31
    • Hodogaya Chem Co Ltd保土谷化学工業株式会社
    • TAKEI ATSUSHIABE KATSUMIOKUBO MASAKIANZAI MITSUTOSHI
    • G03G5/00C07C213/10C07C217/84C09K11/06G03G5/06H01L51/50H05B33/14H05B33/22
    • PROBLEM TO BE SOLVED: To provide an electronic article material having excellent electrical properties by a purification step which does not require any material, produces a markedly small amount of wastes, may be an abridged one, and does not require any large-scale distillation apparatus. SOLUTION: The method comprises performing vacuum distillation under high-vacuum conditions of 10 Pa or below in order to improve the electrical properties of a stilbene derivative represented by formula (1) (wherein Ar 1 is an aromatic hydrocarbon group or a heterocyclic-aromatic hydrocarbon group; Ar 2 is an aromatic hydrocarbon group, a heterocyclic-aromatic group, or hydrogen; Ar 3 is a divalent aromatic hydrocarbon group; R 1 and R 2 , which may be the same of different from each other, are each an aliphatic hydrocarbon group, an aromatic hydrocarbon group, or a heterocyclic-aromatic group; and n is 0 or 1). COPYRIGHT: (C)2006,JPO&NCIPI
    • 要解决的问题:为了提供一种通过不需要任何材料的净化步骤具有优异的电性能的电子制品材料,产生明显少量的废物,可以是一个节省的,并且不需要任何大的 - 规模蒸馏装置。 解决方案:该方法包括在10Pa或更低的高真空条件下进行真空蒸馏,以改善由式(1)表示的二苯乙烯衍生物的电性能(其中Ar 1 为 芳香族烃基或杂环 - 芳香族烃基; Ar 2 是芳香族烃基,杂环 - 芳香族基团或氢原子; Ar 3 是二价芳香族烃 基团;可以彼此不同的R SB 1和R SB 2各自分别是脂族烃基,芳族烃基或杂环芳族 组; n为0或1)。 版权所有(C)2006,JPO&NCIPI