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    • 5. 发明专利
    • METHOD FOR SEPARATING BILE ACID
    • JPS61260097A
    • 1986-11-18
    • JP10287085
    • 1985-05-15
    • HITACHI LTD
    • MATSUZAKI HARUMIKUBOTA MASAYOSHITAKAHASHI SANKICHIYOSHIDA MASAHIROTAKAKUSAKI TSUNEHIKOSATO JOSHIRO
    • C07J9/00
    • PURPOSE:To readily separate bile acid of high purity even in the case where a raw material with a low bile acid content is used, by separating the bile acid from an alcohol obtained by extracting an esterification solution of a raw material containing the bile acid with a supercritical gas or liquefied gas. CONSTITUTION:A raw material containing bile acid, e.g. fish oil, is esterified with a lower alcohol under conditions to form an excess alcohol, and the resultant esterification solution 10 is then introduced into an extraction tank 1 and brought into contact with, for example, a supercritical gaseous carbon dioxide 20 to dissolve preferentially a fatty acid ester, alcohol and bile acid ester in the supercritical gaseous carbon dioxide. The esterification solution 10 and supercritical gaseous carbon dioxide are separated by specific gravity difference to introduce the supercritical gaseous carbon dioxide 20' into the first-stage separation tank 2 and lower the density of the critical gaseous carbon dioxide. Thus, the fatty acid ester 12 is preferantially separated. The alcohol 11 and free bile acid ester 14 are then separated in the secon-stage separation tank 3, and the resultant bile acid ester is separated by crystallization.
    • 8. 发明专利
    • NON-CONTACT MEASUREMENT OF THREE-DIMENSIONAL SHAPE
    • JPS63187103A
    • 1988-08-02
    • JP1816887
    • 1987-01-30
    • HITACHI LTD
    • HARANO MASAMITAKAKUSAKI TSUNEHIKOYOSHIDA MASAHIROSATO JOSHIROTAKAGI YUSUKE
    • G01B11/24
    • PURPOSE:To enhance measuring accuracy by permitting no reception of the auxiliary beam path of irradiation beam due to a concaved shape by a sensor, by a method wherein an angle changing mechanism is formed of a biaxial constitution consisting of the rotary axis in a plane, which is right-angled to the irradiation optical axis of a beam spot position detecting sensor and contains the irradiation optical axis and a beam receiving axis, and the rotary axis passing the intersecting point of the rotary axis and the irradiation optical axis and right-angled to said two axes. CONSTITUTION:An angle changing mechanism 2 is formed of a biaxial constitution consisting of a rotary axis Z right-angled to the irradiation optical axis 8 of a beam spot detection sensor 1 and containing the irradiation optical axis 8 and a beam receiving axis 9, and a rotary axis Y passing the intersecting point P of the rotary axis Z and the irradiation optical axis 8 and right-angled to said two axes. This mechanism 2 is combined with a three- dimensional drive mechanism 3 to constitute a non-contact measuring system and an object 5 to be measured is placed on a moving table 4 moving in an X-direction. The beam from the beam source 3 is allowed to irradiate the P-point on the object 5 and the irregular reflected beam from the P-point is received by the beam receiving lens 10 arranged on a beam receiving optical axis 9 forming an angle gamma with respect to the irradiation optical axis 8 and detected by a beam receiver 11 to prevent the auxiliary beam path of irradiation beam due to a concave shape from being received by the sensor 1.
    • 10. 发明专利
    • Extractive separation apparatus
    • 提取分离装置
    • JPS61129003A
    • 1986-06-17
    • JP24957484
    • 1984-11-28
    • Hitachi Ltd
    • SUGAI HIROSHIYOSHIDA MASAHIROTAKAKUSAKI TSUNEHIKOSATO JOSHIROTAKAHASHI SANKICHIMATSUZAKI HARUMI
    • A23L27/10B01D11/02C10G1/04C10G21/00C11B9/00C11B9/02C12N9/00
    • PURPOSE: To extract and separate an objective substance with high efficiency, by enabling the change-over of extraction tanks and continuously extracting a substance to be extracted while independently controlling the pressures and temps. in the extraction tanks and a separation tank.
      CONSTITUTION: After an objective substance was introduced into an extraction tank 27A, the fluid of a fluid source 1 is allowed to gradually fill the whole of the system through pipings 2, 3, 6, 14. Next, a liquefier 53 is operated to liquefy the fluid. Subsequently, the substance to be extracted, which was extracted in the extraction tank 27A, is mixed with an super-critical fluid to be sent to a separation tank 34 where the fluid is separated from the extracted substance to be sent to a gassification tank 48. The fluid issued from the gassification tank 48 is passed through the liquefier 53 to be perfectly liquefied and sent to a recirculation pump 10 to be recycled and utilized. Further, the extraction time of the objective substance in the extraction tank or the extraction amount of the objective substance in the separation tank is set as a change- over condition and the change-over of extraction tanks 27A, 27B is performed by a change-over control mechanism consisting of automatic valves 19A, 19B, 28A, 28B.
      COPYRIGHT: (C)1986,JPO&Japio
    • 目的:高效率提取和分离目标物质,可独立控制压力和温度,能够切换提取罐,连续萃取提取物质。 在提取罐和分离罐中。 构成:将目标物质引入提取槽27A后,允许流体源1的流体通过管道2,3,6,14逐渐填充整个系统。接下来,液化器53被操作以液化 流体。 随后,将在提取槽27A中提取的待提取物质与超临界流体混合,送至分离槽34,在该分离槽34中,将被萃取的物质与流出的物质分离,送至气化槽48 来自放气罐48的液体通过液化器53被完全液化并送到再循环泵10中以便再循环使用。 此外,将提取罐中的目标物质的萃取时间或分离罐中的目标物质的提取量设定为转换条件,并且提取罐27A,27B的转换通过改变条件进行, 控制机构由自动阀19A,19B,28A,28B组成。