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1. 发明专利

JP2010260941A Method for manufacturing azomethine coloring matter or indoaniline coloring matter 审中-公开
标题翻译：制备AZOMETHINE着色剂或INDOANILINE COLORING MATTER的方法
公开(公告)号：JP2010260941A
公开(公告)日：2010-11-18
申请号：JP2009112236
申请日：2009-05-01
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： KUBO SHINJI
IPC分类号： C09B55/00
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing an azomethine coloring matter or the like in a high yield. SOLUTION: The method for manufacturing the azomethine coloring matter or an indoaniline coloring matter comprises an oxidative condensation reaction of a compound expressed by formulas (1) to (4) and a p-phenylene diamine derivative in the presence of a base and an oxidizing agent, wherein the reaction is carried out to react them in the coexistence of glycols or glycerins. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供以高产率制备偶氮甲碱色素等的方法。解决方案：制备偶氮甲碱色素或吲哚苯胺着色剂的方法包括式（1）至（4）表示的化合物与对苯二胺衍生物在碱存在下的氧化缩合反应和氧化剂，其中进行反应以在二醇或甘油的共存下使它们反应。版权所有（C）2011，JPO＆INPIT

2. 发明专利

JP2008166538A Organic electroluminescent element 审中-公开
标题翻译：有机电致发光元件
公开(公告)号：JP2008166538A
公开(公告)日：2008-07-17
申请号：JP2006355176
申请日：2006-12-28
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： WANG YAHUI , TOMINAGA TETSUYA , KUBO SHINJI
IPC分类号： H01L51/50 , C07C211/54 , C09K11/06
摘要： PROBLEM TO BE SOLVED: To provide an organic EL element of high brightness and high durability by incorporating an organic material having high film formation property, high carrier mobility and thermal stability.
SOLUTION: The organic EL element exhibits high light output and high durability by incorporating a compound No.1-1, for example (a compound expressed by a general formula (1) wherein R1 to R4 are methyl group).
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：解决的问题：通过引入具有高成膜性，高载流子迁移率和热稳定性的有机材料来提供高亮度和高耐久性的有机EL元件。解决方案：通过引入化合物No.1-1（由通式（1）表示的化合物，其中R 1至R 4是甲基），有机EL元件显示出高的光输出和高的耐久性。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2011116898A Manufacturing method for azomethine dye or indoaniline dye 审中-公开
标题翻译：氨基甲酸染料或吲哚尼尔染料的制备方法
公开(公告)号：JP2011116898A
公开(公告)日：2011-06-16
申请号：JP2009276915
申请日：2009-12-04
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： HONDA MUTSUMI , NGUYEN CHUNG THANH , KUBO SHINJI
IPC分类号： C09B67/20 , C09B55/00
摘要： PROBLEM TO BE SOLVED: To provide a method of making azomethine dye or indoaniline dye stably at a high yield and with high purity even during large quantity-production. SOLUTION: A manufacturing method for azomethine dye or indoaniline dye includes carrying out oxidization condensation of a compound expressed by any of formula (1)-(3) and a p-phenylene diamine derivative under the coexistence of a compound expressed by formula (4) or (5), wherein Q represents a hydrogen atom or leaving group; A represents an oxygen atom or -C(R12) (R13)-; n is an integer of 2-6; a plurality of As may be the same or different; X represents a nitrogen atom, or is N→O, provided that when X is a nitrogen atom, at least one of R9-R11 is an OH group; Y represents -N (R14)- or -N[(R15)→O], provided that at least one of As is an oxygen atom, or an OH group as at least one of R12-14 or an OH group is present; or Y represents -N[(R15)→O]-; and R1-15 and X each independently represent a predetermined atom or predetermined group. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供即使在大批量生产期间也以高产率稳定地制备偶氮甲碱染料或吲哚苯胺染料的方法。解决方案：偶氮甲碱染料或吲哚苯胺染料的制造方法包括在式（1） - （3）表示的化合物与对苯二胺衍生物的共存下进行氧化缩合，式（4）或（5），其中Q表示氢原子或离去基团; A表示氧原子或-C（R 12）（R 13） - ; n为2-6的整数; 多个As可以相同或不同; X表示氮原子，或为N→O，条件是当X为氮原子时，R 9 -R 11中的至少一个为OH基; Y表示-N（R 14） - 或-N [（R 15）→O]，条件是As中的至少一个为氧原子，或者存在作为R 12-14或OH基中的至少一个的OH基; 或Y表示-N [（R 15）→O] - ; R1-15和X各自独立地表示预定的原子或预定的基团。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2011251943A Process for producing arylamine compound 有权
标题翻译：生产芳香胺化合物的方法
公开(公告)号：JP2011251943A
公开(公告)日：2011-12-15
申请号：JP2010127241
申请日：2010-06-02
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： KUBO SHINJI , HAYASHI HIROYASU
IPC分类号： C07C209/10 , C07B61/00 , C07C211/54 , C07D209/82 , C07D409/14
摘要： PROBLEM TO BE SOLVED: To provide a process for producing an arylamine, particularly a diarylamine compound and a triarylamine compound useful as materials for electronic materials or intermediates thereof with extremely high purity at a low cost.SOLUTION: The process for producing a diarylamine or a triarylamine comprises subjecting a specific aromatic halogen compound and a specific aromatic amine compound to condensation reaction in the presence of a copper catalyst and a base, and a compound represented by formula (1) (wherein R23 is hydrogen or a predetermined substituent; R24 is hydrogen or a predetermined substituent; Z is oxygen or -N(R25)-; and R25 is an alkyl group, an alkenyl group, an aryl group or a heterocyclic residue) is allowed to be present in the condensation reaction.
摘要翻译：待解决的问题：提供以低成本制备用作电子材料的材料或其中间体的芳基胺，特别是二芳基胺化合物和三芳基胺化合物的方法，其具有非常高的纯度。解决方案：二芳基胺或三芳基胺的制备方法包括在铜催化剂和碱以及式（1）表示的化合物的存在下，使特定的芳香族卤素化合物和特定的芳香族胺化合物进行缩合反应，（其中R 23为氢或预定取代基; R 24为氢或预定取代基; Z为氧或-N（R 25） - ; R 25为烷基，烯基，芳基或杂环残基）存在于缩合反应中。版权所有（C）2012，JPO＆INPIT

5. 发明专利

JP2011012231A Method of synthesizing azomethine dye or indoaniline dye 审中-公开
标题翻译：合成AZOMETHINE DYE或INDOANILINE DYE的方法
公开(公告)号：JP2011012231A
公开(公告)日：2011-01-20
申请号：JP2009159927
申请日：2009-07-06
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： KUBO SHINJI , KAKIZAKI SHINICHI , HONDA MUTSUMI
IPC分类号： C09B53/00 , B41M5/385 , B41M5/39 , C09B55/00
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing an azomethine dye or an indoaniline dye with high purity and high yield, enabling the production in an industrial level.SOLUTION: In the method of manufacturing an azomethine dye or an indoaniline dye, where a compound, represented by either one of formula (1) to (3), and a p-phenylene diamine derivative are subjected to oxidative condensation in water alone or mixed solvents of water and an organic solvent in the presence of a base and an oxidizing agent, this method of manufacturing the azomethine dye or indoaniline dye carries out the reaction in the co-presence of at least one compound selected from glycerols or glycols represented by formula (4) or (5). In the formulae, each symbol represents a specific atom or group.
摘要翻译：要解决的问题：提供一种制备具有高纯度和高产率的偶氮甲碱染料或吲哚苯胺染料的方法，使得能够在工业水平上生产。方法：在制备偶氮甲碱染料或吲哚苯胺染料的方法中，其中由式（1）至（3）中的任何一个表示的化合物和对苯二胺衍生物在水和单独的水和有机溶剂的混合溶剂中在碱和氧化剂的存在下进行氧化缩合制备偶氮甲碱染料或吲哚苯胺染料的方法是在至少一种选自式（4）或（5）表示的甘油或二醇的化合物的共存下进行反应。在公式中，每个符号表示特定的原子或基团。

6. 发明专利

JP2013071922A Method for producing triphenylene compound 有权
标题翻译：生产三苯乙烯化合物的方法
公开(公告)号：JP2013071922A
公开(公告)日：2013-04-22
申请号：JP2011213405
申请日：2011-09-28
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： KUBO SHINJI , NGUYEN CHUNG THANH
IPC分类号： C07D493/14 , C07C2/82 , C07C15/38 , C07C37/055 , C07C39/12 , C07C41/30 , C07C43/20
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a 2,3,6,7,10,11-hexasubstituted triphenylene compound in a high yield which enables mass production at a low cost and on an industrial scale and reduces the load to the environment as much as possible.SOLUTION: The method for producing a 2,3,6,7,10,11-hexasubstituted triphenylene compound by the trimerization reaction of a 1,2-disubstituted benzene compound in the presence of a compound including a divalent or trivalent iron ion comprises using at least one reaction solvent selected from the group consisting of carboxylic acid esters, lactones, carbonic acid esters, and sulfurous esters in the reaction.
摘要翻译：待解决的问题：提供一种以高产率制备2,3,6,7,10,11-六取代三亚苯基化合物的方法，其能够以低成本和工业规模批量生产并减少尽可能地加载到环境中。解决方案：在包含二价或三价铁的化合物的存在下，通过1,2-二取代的苯化合物的三聚反应制备2,3,6,7,10,11-六取代的三亚苯化合物的方法离子包括在反应中使用至少一种选自羧酸酯，内酯，碳酸酯和亚硫酸酯的反应溶剂。版权所有（C）2013，JPO＆INPIT

7. 发明专利

JP2008158436A Electrophotographic photoreceptor, electrophotographic device and process cartridge 审中-公开
标题翻译：电子照相机，电子照相设备和工艺盒
公开(公告)号：JP2008158436A
公开(公告)日：2008-07-10
申请号：JP2006349861
申请日：2006-12-26
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： WANG YAHUI , TOMINAGA TETSUYA , KUBO SHINJI
IPC分类号： G03G5/06
CPC分类号： C07C211/54 , G03G5/0614
摘要： PROBLEM TO BE SOLVED: To provide an electrophotographic photoreceptor, an electrophotographic photoreceptor device and a process cartridge having high sensitivity, high durability and high output, in which a film formed as a photosensitive layer is stable, with a high carrier mobility and free from precipitation of crystals or formation of pinholes during film formation. SOLUTION: The electrophotographic photoreceptor, the electrophotographic device and the process cartridge contain a compound expressed by general formula (1). In formula (1), each of R1 to R4 independently represents an alkyl group, arylalkyl group, aryl group or arylalkenyl group. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种电子照相感光体，电子照相感光体装置和具有高灵敏度，高耐久性和高输出性的处理盒，其中形成为感光层的膜具有稳定的高载流子迁移率和在成膜期间不析晶或形成针孔。解决方案：电子照相感光体，电子照像装置和处理盒含有由通式（1）表示的化合物。式（1）中，R 1〜R 4各自独立地表示烷基，芳烷基，芳基或芳基烯基。版权所有（C）2008，JPO＆INPIT

8. 发明专利

JP2006234966A Refining process of charge transport material 有权
标题翻译：充电运输材料精炼过程
公开(公告)号：JP2006234966A
公开(公告)日：2006-09-07
申请号：JP2005045978
申请日：2005-02-22
申请人： Fujifilm Finechemicals Co Ltd , 富士フイルムファインケミカルズ株式会社
发明人： FUJII SATORU , KUBO SHINJI , SHIKAKURA KOICHI
IPC分类号： G03G5/06 , G03G5/07
摘要： PROBLEM TO BE SOLVED: To provide the refining process of a charge transport material in which deterioration the material, such as oxidation, is drastically reduced and is industrially excellent in terms of cost and environmental influence. SOLUTION: The refining process of the charge transport material, with which the charge transport material for an organic semiconductor element or its intermediate is dissolved in an organic solvent and the solution thereof is brought into contact with adsorbents, is characterized in that at least one of the adsorbents, is a clay ore adsorbent having a specific surface area of 260 m 2 /g. COPYRIGHT: (C)2006,JPO&NCIPI

9. 发明专利

JP2006347964A METHOD FOR PRODUCING ARYLAMINE 审中-公开
公开(公告)号：JP2006347964A
公开(公告)日：2006-12-28
申请号：JP2005176809
申请日：2005-06-16
申请人： FUJIFILM FINECHEMICALS CO LTD
发明人： KUBO SHINJI
IPC分类号： C07C209/10 , C07B61/00 , C07C211/54 , C07C211/55 , C07D209/86
摘要： PROBLEM TO BE SOLVED: To provide a method with which an arylamine, especially a triarylamine or a diarylamine, useful as a material for electronic materials such as an electrophotographic photoreceptor or an organic electroluminescent element and an intermediate therefor is inexpensively produced in high purity. SOLUTION: The method for producing the arylamine is characterized as follows. An amine compound, a chlorinated aromatic compound and an inorganic bromide or the amine compound, a brominated aromatic compound and an inorganic iodide are made to coexist and react in the presence of a copper element-containing catalyst, a base and a heterocyclic tertiary amine compound. COPYRIGHT: (C)2007,JPO&INPIT

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