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1. 发明专利

JP2007023329A Chromium-free insulating film agent for electromagnetic steel sheet 有权
标题翻译：用于电磁钢板的无铬绝缘膜
公开(公告)号：JP2007023329A
公开(公告)日：2007-02-01
申请号：JP2005206215
申请日：2005-07-14
申请人： Catalysts & Chem Ind Co Ltd , Nippon Steel Corp , Nittetsu Plant Designing Corp , 新日本製鐵株式会社 , 日鐵プラント設計株式会社 , 触媒化成工業株式会社
发明人： TANAKA OSAMU , FUJII HIROYASU , TAKEDA KAZUTOSHI , TAKAHASHI FUMIAKI , NISHIDA HIROYASU , SENJU NOBORU
IPC分类号： C23C22/00 , C01B33/149 , C21D9/46 , H01F1/18
CPC分类号： C23C22/74 , C23C22/08 , C23C22/62
摘要： PROBLEM TO BE SOLVED: To provide a grain oriented electromagnetic steel sheet product having excellent corrosion resistance, annealing resistance, film tension or the like in insulating treatment using a chromium-free phosphate as a base, and to provide a treatment agent.
SOLUTION: The chromium-free insulating film agent for an electromagnetic steel sheet comprises: (I) a phosphate by 100 pts.mass; (II) colloidal silica by 35 to 100 pts.mass in terms of an SiO
2 solid content; and (III) a dispersed liquid of a colloidal compound comprising one or more metallic elements selected from Fe, Al, Ga, Ti and Zr by 0.1 to 20 pts.mass in terms of the metallic element(s).
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种在使用无铬磷酸盐作为基底的绝缘处理中具有优异的耐腐蚀性，耐退火性，膜张力等的晶粒取向电磁钢板产品，并提供处理剂。解决方案：用于电磁钢板的无铬绝缘膜剂包括：（I）磷酸盐100磅; （II）胶体二氧化硅，按SiO 2 SB固体含量计35〜100磅/立方米。和（III）包含一种或多种选自Fe，Al，Ga，Ti和Zr的金属元素的胶体化合物的分散液体，以金属元素换算为0.1-20质点。版权所有（C）2007，JPO＆INPIT

2. 发明专利

JP2012144776A Method of manufacturing grain-oriented electromagnetic steel sheet 审中-公开
标题翻译：制造面向导电电磁钢板的方法
公开(公告)号：JP2012144776A
公开(公告)日：2012-08-02
申请号：JP2011004307
申请日：2011-01-12
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： TAKAHASHI FUMIAKI , USHIGAMI YOSHIYUKI , MIZUKAMI KAZUSANE , NAKAMURA SHUICHI , FUJII NOBUNORI , YAMAMOTO NORIHIRO , URASATO MASAHIDE
IPC分类号： C22C38/00 , C21D8/12 , C22C38/60 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To provide a means for obtaining a grain-oriented electromagnetic steel sheet having excellent magnetic characteristics.SOLUTION: In a raw material for the electromagnetic steel sheet, which contains, by mass%, 0.8-7% Si, 0.01-0.065% acid-soluble Al, 0.004-0.012% N, 0.05-1% Mn, 0.0005-0.0080% B, 0.003-0.015% in total of at least one kind selected from a group comprising S and Se, 0.085% or less C, and the remainder comprising Fe and inevitable impurities, a hot-rolled steel sheet satisfies expression 1: SB≥5%, when B in the steel after a hot-rolling process is analyzed by PSA analysis using spark discharge optical emission spectrometry method. The SB is a value obtained from the total amount, insoluble component amount, and solid solution component amount of the specified components in the metal based on a pulse intensity order drawing in which optical emission intensity of specified components obtained by discharge using the optical emission spectrometry method is rearranged in order.
摘要翻译：要解决的问题：提供一种获得具有优异磁特性的晶粒取向电磁钢板的方法。解决方案：在电磁钢板的原料中，以质量％计含有0.8〜7％的Si，0.01〜0.065％的酸溶性Al，0.004〜0.012％的N，0.05〜1％的Mn，0.0005 -0.0080％B，0.003-0.015％，选自由S和Se组成的组中的至少一种，C组为0.085％以下，余量为Fe和不可避免的杂质，热轧钢板满足式1：当使用火花放电发射光谱法进行PSA分析，热轧过程中钢中的B分析时，S Insol B≥5％。 S Insol B是从金属中的特定成分的总量，不溶成分量和固溶成分量基于脉冲强度次序图得到的值，其中使用光发射光谱法通过放电获得的特定成分的光发射强度按顺序重新排列。版权所有（C）2012，JPO＆INPIT

3. 发明专利

JP2012046825A Heat resistant adhesive insulating film 有权
标题翻译：耐热胶粘剂绝缘胶片
公开(公告)号：JP2012046825A
公开(公告)日：2012-03-08
申请号：JP2011214497
申请日：2011-09-29
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： YAMADA NORIKO , FUJII HIROYASU , KUBO YUJI , TAKEDA KAZUTOSHI , TAKAHASHI FUMIAKI , ARITA YOSHIHIRO , OHATA YOSHIFUMI
IPC分类号： C23C26/00 , C09J5/06 , C09J11/04 , C09J133/04 , C09J161/06 , C09J163/00 , C09J183/04 , C09J201/00 , H01F1/18 , H01F41/02
CPC分类号： C23C26/00 , C09J11/04 , H01F1/18 , H01F3/02
摘要： PROBLEM TO BE SOLVED: To provide: an electromagnetic steel sheet having a surface covered with a heat resistant adhesive insulating film which, after lamination, can be bonded by pressing and heating and can achieve strain relieving annealing; an iron core using the electromagnetic steel sheet; and a process for manufacturing the same.SOLUTION: The electromagnetic steel sheet is covered with a heat resistant adhesive insulating film comprising a resin which softens at room temperature or above and 300°C or below, and a low-melting inorganic component having a softening temperature of 1,000°C or below as measured by a differential thermal analysis method, and formed by mixing the resin and the low melting point inorganic component at a mixing ratio of 20% or more and 500% or less by mass fraction. A strain-relieving-annealable bonded fixed iron core is provided by stacking this electromagnetic steel sheet and conducting press fixation.
摘要翻译：要解决的问题：提供一种具有覆盖有耐热粘合绝缘膜的表面的电磁钢板，其在层压之后可以通过加压和加热结合，并且可以实现应变消除退火; 使用电磁钢板的铁芯; 及其制造方法。解决方案：电磁钢板被包含在室温以上且300℃以下软化的树脂的耐热粘合绝缘膜和软化温度为1000℃的低熔点无机成分覆盖以下，通过差热分析法测定，通过以20质量％以上且500质量％以下的混合比混合树脂和低熔点无机成分而形成。通过堆叠该电磁钢板并进行压力固定来提供应变消除退火的粘结固定铁芯。版权所有（C）2012，JPO＆INPIT

4. 发明专利

JP2010043293A Coating liquid for insulation film to be used for grain-oriented electromagnetic steel sheet, and method for forming insulation film 有权
标题翻译：用于面向导电电磁钢板的绝缘膜用涂料液及形成绝缘膜的方法
公开(公告)号：JP2010043293A
公开(公告)日：2010-02-25
申请号：JP2008206000
申请日：2008-08-08
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： YAMAZAKI SHUICHI , TAKAHASHI FUMIAKI , TAKEDA KAZUTOSHI , FUJII HIROYASU
IPC分类号： C23C22/00 , C21D9/46 , H01F1/16 , H01F1/18
摘要： PROBLEM TO BE SOLVED: To provide an insulation film for a grain-oriented electromagnetic steel sheet, which has a larger tensile strength than a conventional insulation film. SOLUTION: This method for forming the insulation film which imparts a great effect of reducing iron loss to the grain-oriented electromagnetic steel sheet includes applying the coating liquid, in which a primary phosphate in an amount of a fixed range is mixed with a fine powder of a hydrous silicate, to the surface of the grain-oriented electromagnetic steel sheet, drying the same, and then baking the dried film at 600°C or higher. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种具有比常规绝缘膜更大的拉伸强度的取向电磁钢板的绝缘膜。解决方案：用于形成对晶粒取向电磁钢板具有减少铁损的巨大效果的绝缘膜的形成方法包括将其中固定范围的一次磷酸盐与将含水硅酸盐的细粉末涂覆到取向电磁钢板的表面，使其干燥，然后在600℃以上烘干。版权所有（C）2010，JPO＆INPIT

5. 发明专利

JP2010037602A Coating liquid for insulating film used for grain-oriented electromagnetic steel sheet and method for forming the insulating film 有权
标题翻译：用于晶粒电磁钢片绝缘膜用涂料液及形成绝缘膜的方法
公开(公告)号：JP2010037602A
公开(公告)日：2010-02-18
申请号：JP2008202352
申请日：2008-08-05
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： YAMAZAKI SHUICHI , TAKAHASHI FUMIAKI , TAKEDA KAZUTOSHI , FUJII HIROYASU
IPC分类号： C23C22/00 , C21D9/46 , H01F1/18
CPC分类号： C23C22/74 , C23C22/08
摘要： PROBLEM TO BE SOLVED: To provide an insulating film for a grain oriented electromagnetic steel sheet, which is excellent in insulating property and tensile force, hardly sticks, and contains no hexavalent chromium as a raw material.
SOLUTION: A coating liquid is prepared by mixing a phosphate and a hydrous silicate fine powder with colloidal silica. The insulating film having excellent tensile force and seizing resistance after stress-relieving annealing is formed on the surface of a grain oriented electromagnetic steel sheet by applying the coating liquid on the surface of the steel sheet, then drying the applied coating liquid, and baking the resulting film at a temperature of ≥600°C. A method for forming the insulating film is also provided.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：解决的问题：为了提供绝缘性和拉伸力优异的晶粒取向电磁钢板用绝缘膜，几乎不粘附，不含六价铬作为原料。解决方案：通过将胶体二氧化硅与磷酸盐和含水硅酸盐细粉混合来制备涂布液。通过将涂布液涂布在钢板的表面上，然后干燥涂布液，并在烘烤后，在晶粒取向电磁钢板的表面上形成具有优异的拉伸力和应力消除退火后的耐烧结性的绝缘膜在≥600℃的温度下形成膜。还提供了形成绝缘膜的方法。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2011219803A Annealing separation agent for grain-oriented magnetic steel sheet and method of manufacturing grain-oriented magnetic steel sheet 有权
标题翻译：用于面向导电磁性钢板的退火分离剂及制造面向导向的磁性钢板的方法
公开(公告)号：JP2011219803A
公开(公告)日：2011-11-04
申请号：JP2010088869
申请日：2010-04-07
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： TAKAHASHI FUMIAKI
IPC分类号： C23C22/00 , C21D9/46 , C22C38/00 , C22C38/06 , C23C8/26 , H01F1/16
摘要： PROBLEM TO BE SOLVED: To stably manufacture a grain-oriented magnetic steel sheet excellent in a coating property and magnetic characteristics.SOLUTION: The annealing separation agent for the grain-oriented magnetic steel sheet is characterized by containing, as an additive, 2 to 30 mass% of a compound that discharges an oxygen-containing gas when heated in a nitrogen/hydrogen mixture air stream at a normal pressure and reduces its weight by 2% or more by the discharge of the gas in the temperature range of 500 to 950°C.
摘要翻译：要解决的问题：为了稳定地制造涂布性和磁特性优异的晶粒取向电磁钢板。解决方案：晶粒取向电磁钢板的退火分离剂的特征在于，在氮/氢混合气体中加热时，含有2〜30质量％的排出含氧气体的化合物作为添加剂在正常压力下流动，并通过在500至950℃的温度范围内排放气体将其重量减少2％或更多。版权所有（C）2012，JPO＆INPIT

7. 发明专利

JP2006161106A Method for producing grain-oriented magnetic steel sheet having no film defect 有权
标题翻译：用于生产具有无膜缺陷的晶粒磁性钢板的方法
公开(公告)号：JP2006161106A
公开(公告)日：2006-06-22
申请号：JP2004354866
申请日：2004-12-08
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： YAMAZAKI SHUICHI , TAKAHASHI FUMIAKI , FUJII NOBUNORI , YAMAMOTO NORIHIRO , KATAOKA TAKEHARU
IPC分类号： C21D9/46 , C22C38/00 , C22C38/06 , C23C8/18 , C23C8/26 , H01F1/16 , H01F27/245 , H01F41/02
摘要： PROBLEM TO BE SOLVED: To prevent a loss type film defect from being generated in the production of a grain-oriented magnetic steel sheet using AlN as an inhibiter. SOLUTION: The method for producing the grain-oriented magnetic steel sheet having no film defect, when the temperature of a finish-annealing is risen to this steel sheet using the AlN as the inhibiter, in the whole coil edge parts of the finish-annealed coil, oxygen potential P H2O /P H2 in the atmosphere in contact with the edge parts in the finish-annealing is made to ≥0.1 in the temperature range of 600-650°C of the coil edge parts, and made to ≤0.5 in the temperature range of ≥900°C of the coil edge parts. In this way, in the finish-annealing, condition for generating the loss type film defect can be avoided over the whole length. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：为了防止在使用AlN作为抑制剂的晶粒取向电磁钢板的生产中产生损失型膜缺陷。解决方案：在使用AlN作为抑制剂的最终退火温度升高到该钢板的情况下，在整个线圈边缘部分中制造没有膜缺陷的晶粒取向电磁钢板的制造方法在完成退火的线圈中，与最终退火中的边缘部分接触的气氛中的氧气电位P H2O / P H2 在温度范围内为≥0.1 线圈边缘部件为600-650°C，线圈边缘部件的≥900°C的温度范围为≤0.5。以这种方式，在最终退火中，可以避免在整个长度上产生损耗型膜缺陷的条件。版权所有（C）2006，JPO＆NCIPI

8. 发明专利

JP2010013692A Insulating film treatment agent, grain-oriented electrical steel sheet coated with the film treatment agent and insulating film treatment method therefor 有权
标题翻译：绝缘膜处理剂，涂有电镀处理剂和绝缘膜处理方法的面向电镀钢板
公开(公告)号：JP2010013692A
公开(公告)日：2010-01-21
申请号：JP2008174103
申请日：2008-07-03
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： TAKEDA KAZUTOSHI , TAKAHASHI FUMIAKI , YAMAZAKI SHUICHI , FUJII HIROYASU , ANDO FUMIKAZU , NATORI YOSHIAKI
IPC分类号： C23C22/00 , C21D9/46 , H01F1/18
摘要： PROBLEM TO BE SOLVED: To improve the magnetic properties of a grain-oriented electrical steel sheet free from chromic acid by increasing tensile strength of an electrical insulating film of the grain-oriented electrical steel sheet higher than before.
SOLUTION: An insulating film treatment agent contains a phosphate and colloidal silica as principal elements, wherein the ratio of the colloidal silica to 100 pts.wt. of the phosphate is 30 to 70 pts.wt. and in metal components in the phosphate, the content of bivalent metallic elements is 20 to 80 wt.%, the content of trivalent metals is 10 to 70 wt.% and the content of metallic elements having 4 or more valences is 3 to 20 wt.%. The grain-oriented electrical steel sheet has a high tensile strength insulating film with a composition obtained by applying the above treatment liquid onto the surface of the steel sheet and baking the liquid.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：通过提高比以前更高的方向性电磁钢板的电绝缘膜的抗拉强度，提高不含铬酸的方向性电磁钢板的磁性能。解决方案：绝缘膜处理剂含有磷酸盐和胶体二氧化硅作为主要元素，其中胶体二氧化硅与100重量份的比例的磷酸盐为30〜70重量份在磷酸盐中的金属成分中，二价金属元素的含量为20〜80重量％，3价金属的含量为10〜70重量％，4价以上的金属元素的含量为3〜20重量％％。晶粒取向电工钢板具有高拉伸强度的绝缘膜，其具有通过将上述处理液施加到钢板的表面上并烘烤该液体而得到的组成。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2009235568A Grain-oriented electrical steel sheet and its manufacturing method 有权
标题翻译：面向电磁钢板及其制造方法
公开(公告)号：JP2009235568A
公开(公告)日：2009-10-15
申请号：JP2009049911
申请日：2009-03-03
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： TAKAHASHI FUMIAKI , TAKEBAYASHI KIYONORI , YAMAZAKI SHUICHI , NATORI YOSHIAKI
IPC分类号： C22C38/00 , C21D8/12 , C21D9/46 , C22C38/06 , C23C22/00 , H01F1/16 , H01F1/18
摘要： PROBLEM TO BE SOLVED: To provide a grain oriented electrical steel sheet having satisfactory glass film excellent in magnetic characteristics and free from defects.
SOLUTION: The grain oriented electrical steel sheet includes: (a) the amount of oxygen over the entire part of the steel sheet after carburization annealing is 400 to 1,500 ppm; (b) the region where the precipitates including silicon oxide of ≥8 in linearity of two-dimensional shape in the oxide layer on the steel sheet surface exist in a range of ≥3 pieces/μm
2 is ≥30% over the entire part of the oxide layer; (c) the state that there are no oxides within the oxide layer exists intermittently or does not exist continuously in a region of a thickness of ≥0.2 μm in a sheet thickness direction; and, if necessary, (d) the surface thickening rate of silicon in the surface oxide layer is ≥0.3 to ≤0.85. The grain oriented electrical steel sheet is manufactured by switching the oxygen potential of the atmosphere during decarburization annealing during the course of soaking.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供具有良好的磁特性和无缺陷的令人满意的玻璃膜的晶粒取向电工钢板。解决方案：晶粒取向电工钢板包括：（a）渗碳退火后钢板整个氧气的量为400〜1500ppm; （b）在钢板表面的氧化物层中存在二维形状的二氧化硅≥8的析出物的区域存在≥3个/μm 2 的范围为≥ 在氧化物层的整个部分上为30％; （c）在厚度方向上厚度≥0.2μm的区域内，氧化物层内没有氧化物间断地或不连续地存在的状态; 如果需要，（d）表面氧化物层中的硅的表面增厚率为≥0.3〜≤0.85。在浸渍过程中，通过在脱碳退火时切换大气的氧气来制造晶粒取向电工钢板。版权所有（C）2010，JPO＆INPIT

10. 发明专利

JP2005303237A Electrostatic chuck 审中-公开
标题翻译：静电卡
公开(公告)号：JP2005303237A
公开(公告)日：2005-10-27
申请号：JP2004121342
申请日：2004-04-16
申请人： Nippon Steel Corp , 新日本製鐵株式会社
发明人： ANDO AKIRO , TAKAHASHI FUMIAKI , OKITA TAKUSHI , SUGAWARA JUN , MORITA HIDEHIKO
IPC分类号： C04B35/00 , C04B35/495 , H01L21/027 , H01L21/68 , H01L21/683 , H02N13/00
摘要： PROBLEM TO BE SOLVED: To provide an electrostatic chuck capable of stably carrying out electrostatic chucking by the Johnsen-Rahbeck force. SOLUTION: The electrostatic chuck has a dielectric part composed of a material which is substantially a single-phase material and has the absolute value of the thermal expansion coefficient at room temperature of 6×10 -7 /K or lower, bulk density of 95% or higher, and volume resistivity of 1×10 12 Ωcm or higher and lower than 1×10 14 Ωcm. The material constituting the dielectric part has Young's modulus of 100 GPa or larger and specific rigidity of 40 GPa/g or larger. The chemical composition of the material constituting the dielectric part is in the ranges of MgO: 8.0 to 17.2 mass%, Al 2 O 3 : 22.0 to 38.0 mass %, SiO 2 : 49.5 to 65.0 mass%, and Li 2 O: 1 to 2.5 mass%, while the mass ratios of the chemical composition are (SiO 2 -8×Li 2 O)/MgO≥3.0 and (SiO 2 -8×Li 2 O)/Al 2 O 3 ≥1.2. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供能够通过Johnsen-Rahbeck力稳定地进行静电吸附的静电卡盘。解决方案：静电卡盘具有由基本上为单相材料的材料构成的介电部分，并且室温下的热膨胀系数的绝对值为6×10 -7 / K或更低，体积密度为95％或更高，体积电阻率为1×10 12 / SP>Ωcm或更高且低于1×10 14 / SP>Ωcm。构成电介质部件的材料的杨氏模量为100GPa以上，比刚性为40GPa / g以上。构成电介质部件的材料的化学组成在MgO：8.0〜17.2质量％的范围内，Al 2 O 3 / SB 3：22.0〜38.0质量％，SiO 2， SB> 2 ：49.5〜65.0质量％，Li 2 -8×Li 2 O）/MgO≥3.0和（SiO 2 -8×Li 2 O）/ Al 0 3 ≥1.2。版权所有（C）2006，JPO＆NCIPI

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