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1. 发明专利

JP2013173841A Resin composition 有权
标题翻译：树脂组合物
公开(公告)号：JP2013173841A
公开(公告)日：2013-09-05
申请号：JP2012038897
申请日：2012-02-24
申请人： Ajinomoto Co Inc , 味の素株式会社 , Kao Corp , 花王株式会社
发明人： OHASHI SEIICHIRO , NARABASHI HIROHISA , KOMATSU MASAKI , YANO AKIHIRO
IPC分类号： C08L63/00 , C08J5/24 , C08K3/36 , C08K7/26 , C09J7/02 , C09J11/04 , C09J11/06 , C09J163/00 , H05K1/03 , H05K3/46
摘要： PROBLEM TO BE SOLVED: To provide a resin composition sufficiently low in all of dielectric constant, dielectric loss tangent and coefficient of thermal expansion, particularly, a resin composition having a sufficiently small dielectric constant and a low dielectric loss tangent, and a sufficiently low coefficient of thermal expansion at 150°C or higher.SOLUTION: A resin composition includes: an epoxy resin, a curing agent, hollow silica and fused silica.
摘要翻译：要解决的问题：为了提供足够低的介电常数，介电损耗角正切和热膨胀系数的树脂组合物，特别是具有足够小的介电常数和低介电损耗角正切的树脂组合物和足够低的系数在150℃以上的热膨胀。树脂组合物包括：环氧树脂，固化剂，中空二氧化硅和熔融二氧化硅。

2. 发明专利

JP2013128468A Method of manufacturing sugar 审中-公开
标题翻译：制造糖的方法
公开(公告)号：JP2013128468A
公开(公告)日：2013-07-04
申请号：JP2011281919
申请日：2011-12-22
申请人： Kao Corp , 花王株式会社
发明人： YANO AKIHIRO , TANOUE AKIHIRO
IPC分类号： C12P19/14
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing sugar, which is excellent in productivity, being able to efficiently manufacture sugar from a cellulose raw material.SOLUTION: The method of manufacturing sugar has a step (1) and a step (2) below, and the step (1) and/or the step (2) are/is performed under existence of a nitrogen-containing compound (A). The step (1) is a step of grinding a cellulose raw material under existence of an inorganic base compound (B) to get a ground cellulose product, and the step (2) is a step of saccharifying the cellulose ground product, obtained in the step (1), with oxygen.
摘要翻译：要解决的问题：提供一种制造糖的方法，其生产率优异，能够有效地从纤维素原料制造糖。方法：制造糖的方法具有步骤（1）和步骤（2）在含氮化合物（A）的存在下进行步骤（1）和/或步骤（2）。步骤（1）是在存在无机碱化合物（B）的情况下研磨纤维素原料以得到磨碎的纤维素产品的步骤，步骤（2）是将所得纤维素研磨产物糖化步骤（1），用氧气。

3. 发明专利

JP2010222147A Method for producing plate-like silica particle 有权
标题翻译：生产类似二氧化硅颗粒的方法
公开(公告)号：JP2010222147A
公开(公告)日：2010-10-07
申请号：JP2009067963
申请日：2009-03-19
申请人： Kao Corp , 花王株式会社
发明人： YANO AKIHIRO , KOMATSU MASAKI
IPC分类号： C01B33/18
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a plate-like silica particle having low relative permittivity and/or low dielectric loss tangent and having high anisotropy, and the plate-like silica particle. SOLUTION: (1) The method for producing the plate-like silica particle having the relative permittivity of ≤3.5 and/or the dielectric loss tangent of ≤0.01 includes a step of pulverizing a hollow silica particle in which nanopores are substantially not present and (2) the plate-like silica particle having the relative permittivity of ≤3.5 and/or the dielectric loss tangent of ≤0.01 is obtained by using the production method. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种生产具有低相对介电常数和/或低介电损耗角正切并且具有高各向异性的板状二氧化硅颗粒的方法和板状二氧化硅颗粒。 <1>解决方案：（1）相对介电常数为≤3.5和/或介电损耗角正切为≤0.01的板状二氧化硅粒子的制造方法包括：将纳米孔基本上不是的中空二氧化硅粒子粉碎的工序和（2）通过使用该制造方法获得相对介电常数为≤3.5的平板状二氧化硅粒子和/或介电损耗角正切为≤0.01的板状二氧化硅粒子。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2010208907A Production method of mesoporous silica particle 有权
标题翻译： MESOPOROUS二氧化硅颗粒的生产方法
公开(公告)号：JP2010208907A
公开(公告)日：2010-09-24
申请号：JP2009058321
申请日：2009-03-11
申请人： Kao Corp , 花王株式会社
发明人： YAMASHITA RISAKO , YANO AKIHIRO , HOSOKAWA KOJI
IPC分类号： C01B37/00
摘要： PROBLEM TO BE SOLVED: To provide an efficient production method of mesoporous silica particles having two or more kinds of pore periodic intervals and the mesoporous silica particles.
SOLUTION: The production method of the mesoporous silica particles includes a step of adding a silica source (c) and a second surfactant into a dispersion (A) containing composite silica particles produced using a first surfactant as a template with time for reaction, wherein the first surfactant and the second surfactant are respectively quaternary ammonium salts expressed by one of formula (1) and formula (2), the first surfactant is different from the second surfactant and the mesoporous silica particle has two or more kinds of the pore periodic intervals, where formula (1) is [R
1 (R
3 )
3 N]
+ X
- and formula (2) is [R
1 R
2 (R
3 )
2 N]
+ X
- , in the formula, each of R
1 and R
2 expresses independently a 4-22C alkyl group, R
3 expresses a 1-3C alkyl group and X expresses a univalent anion.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供具有两种或更多种孔周期性间隔的介孔二氧化硅颗粒和介孔二氧化硅颗粒的有效的制备方法。解决方案：介孔二氧化硅颗粒的制备方法包括将二氧化硅源（c）和第二表面活性剂加入到使用第一表面活性剂作为模板制备的复合二氧化硅颗粒的分散体（A）中随时间进行反应的步骤其中第一表面活性剂和第二表面活性剂分别是由式（1）和式（2）之一表示的季铵盐，第一表面活性剂不同于第二表面活性剂，介孔二氧化硅颗粒具有两种或更多种孔周期性间隔，其中公式（1）为[R 1 （R 3 ） 3 N] SP> - 和式（2）是[R SP SP] 2 R 2 （R 3 ） 2 1 和R 2 中的每一个独立地表示4个 -22C烷基，R 3表示1-3C烷基，X表示一价阴离子。版权所有（C）2010，JPO＆INPIT

5. 发明专利

JP2010138004A Method for manufacturing mesoporous silica particle powder 有权
标题翻译：制造MESOPOROUS二氧化硅颗粒粉末的方法
公开(公告)号：JP2010138004A
公开(公告)日：2010-06-24
申请号：JP2008313613
申请日：2008-12-09
申请人： Kao Corp , 花王株式会社
发明人： HOSOKAWA KOJI , YANO AKIHIRO
IPC分类号： C01B37/00
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing mesoporous silica particles which does not change primary particle structures of mesoporous silica particles and produces less coarse particles.
SOLUTION: The method is for manufacturing mesoporous silica particle powder in which agglomerates are reduced, where mesoporous silica powder containing agglomerates is dry-pulverized using a rotary pulverizer under the condition that the electric power consumption is 0.01-30 kWh per 1 kg of mesoporous silica powder.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种制造介孔二氧化硅颗粒的方法，其不会改变介孔二氧化硅颗粒的一次颗粒结构并且产生较少的粗颗粒。解决方案：该方法用于制造介孔二氧化硅颗粒粉末，其中使用旋转式粉碎机将含有附聚物的中孔二氧化硅粉末粉碎，其中在每1kg消耗电力为0.01-30kWh的条件下，的介孔二氧化硅粉末。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2010037150A Method for producing hollow silica particle 有权
标题翻译：生产中空二氧化硅颗粒的方法
公开(公告)号：JP2010037150A
公开(公告)日：2010-02-18
申请号：JP2008202270
申请日：2008-08-05
申请人： Kao Corp , 花王株式会社
发明人： YANO AKIHIRO , HOSOKAWA KOJI , YAMASHITA RISAKO
IPC分类号： C01B37/02 , C01B33/18
摘要： PROBLEM TO BE SOLVED: To provide a hollow silica particle which has periodicity in a single nano-area, small average particle size and a small specific surface area and to provide a method for producing the hollow silica particle. SOLUTION: The method for producing the hollow silica particle, which shows one or more peaks at a diffraction angle (2θ) corresponding to 1-10 nm crystal lattice spacing (d) when measured by a powder X-ray diffraction method and which has ≤30 m 2 /g BET specific surface area when measured by a nitrogen adsorption method, comprises the steps of: packing a carbon-containing compound, which is carbonized when fired in a non-oxidizing atmosphere, into a mesopore of a mesoporous silica particle having a hollow structure, mesopores on the outer shell thereof and ≥100 m 2 /g BET surface area; firing the carbon-containing compound-packed mesoporous silica particle at ≥800°C in the non-oxidizing atmosphere to transform the carbon-containing compound into a carbon support; and heating the carbon support-packed mesoporous silica particle in an oxidizing atmosphere to remove the carbon support. The hollow silica particle is provided which shows one or more peaks at the diffraction angle (2θ) corresponding to 1-10 nm crystal lattice spacing (d) when measured by the powder X-ray diffraction method and which has 0.05-2 μm average particle size and ≤30 m 2 /g BET specific surface area when measured by the nitrogen adsorption method. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种具有单一纳米区域的周期性，小的平均粒径和小比表面积的中空二氧化硅颗粒，并提供一种中空二氧化硅颗粒的制造方法。解决方案：制备中空二氧化硅颗粒的方法，其通过粉末X射线衍射法测量时，其以衍射角（2θ）表示对应于1-10nm晶格间距（d）的一个或多个峰;以及其通过氮吸附法测量时具有≤30m2 / SP / g BET比表面积的步骤包括以下步骤：包装含碳化合物，其在非氧化性气氛中焙烧时被碳化进入具有中空结构的介孔二氧化硅颗粒的中孔，其外壳上的介孔和BET表面积≥100m2 / SP / g / 在非氧化性气氛中将含碳化合物填充的介孔二氧化硅粒子在≥800℃下烧成，将含碳化合物转化为碳载体; 并在氧化气氛中加热碳载体填充的介孔二氧化硅颗粒以除去碳载体。提供中空二氧化硅颗粒，其通过粉末X射线衍射法测量，其具有对应于1-10nm晶格间距（d）的衍射角（2θ）处的一个或多个峰，并且其平均粒径为0.05-2μm 尺寸和≤30m 2 / g通过氮吸附法测量BET比表面积。版权所有（C）2010，JPO＆INPIT

7. 发明专利

JP2008280226A Method of preparing mesoporous titania 审中-公开
标题翻译：制备MESOPOROUS TITANIA的方法
公开(公告)号：JP2008280226A
公开(公告)日：2008-11-20
申请号：JP2007128339
申请日：2007-05-14
申请人： Kao Corp , 花王株式会社
发明人： SAWADA TAKUYA , YANO AKIHIRO
IPC分类号： C01G23/053 , C01B37/00
摘要： PROBLEM TO BE SOLVED: To provide mesoporous titania having a small diameter, which can be used widely in industry, and to provide its preparation method.
SOLUTION: (1) The method of preparing amorphus mesoporous titania includes a process I of carrying out a dehydration condensation at 5-100°C by adding a quaternary ammonium surfactant, alkoxy titanium and/or hydroxy titanium to an aqueous alkaline solution. (2) The amorphus mesoporous titania is prepared by the method and has a peak top of 1-2 nm obtained by BJH method from a nitrogen adsorption isotherm and a pore volume of 0.2-0.5 cm
3 /g.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供可广泛应用于工业中的小直径的介孔二氧化钛，并提供其制备方法。（1）制备阳离子介孔二氧化钛的方法包括通过向碱性水溶液中加入季铵表面活性剂，烷氧基钛和/或羟基钛，在5-100℃下进行脱水缩合的方法I 。（2）通过该方法制备了amorphus介孔二氧化钛，并且通过BJH法从氮吸附等温线获得的峰顶部为1-2nm，孔体积为0.2-0.5cm 3 / SP 。版权所有（C）2009，JPO＆INPIT

8. 发明专利

JP2007196140A Esterification catalyst 有权
标题翻译：纯化催化剂
公开(公告)号：JP2007196140A
公开(公告)日：2007-08-09
申请号：JP2006018048
申请日：2006-01-26
申请人： Kao Corp , 花王株式会社
发明人： YANO AKIHIRO , SAWADA TAKUYA
IPC分类号： B01J21/08 , B01J35/10 , B01J37/08 , C07B61/00 , C07C67/03 , C07C69/24 , C07C69/58
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a heterogeneous catalyst excellent in esterification reactivity and a method for producing the same. SOLUTION: [1] The peak top of the pore size distribution of the esterification catalyst obtained by a BJH method is within the range of 0.6-8 nm; and the catalyst includes a silicate containing 0.1-5 mass% of Al. [2] The method for producing the esterification catalyst comprises a process (a) of preparing an aqueous solution of a specific quaternary ammonium salt, a quaternary ammonium salt containing an Al source and a Si source, a process (b) of depositing a complex by heating the aqueous solution at a temperature of 100-160°C, and a process (c) of removing the quaternary ammonium salt by calcining the complex. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供酯化反应性优异的多相催化剂及其制造方法。解决方案：[1]通过BJH法获得的酯化催化剂的孔径分布的峰顶在0.6-8nm的范围内; 催化剂含有0.1〜5质量％的Al的硅酸盐。 [2]制备酯化催化剂的方法包括制备特定季铵盐的水溶液，含有Al源和Si源的季铵盐的方法（a），沉积络合物的方法（b）通过在100-160℃的温度下加热水溶液，以及通过煅烧该络合物除去季铵盐的方法（c）。版权所有（C）2007，JPO＆INPIT

9. 发明专利

JP2012136363A Hollow silica particle 有权
标题翻译：中空硅胶颗粒
公开(公告)号：JP2012136363A
公开(公告)日：2012-07-19
申请号：JP2010288441
申请日：2010-12-24
申请人： Kao Corp , 花王株式会社
发明人： YANO AKIHIRO , KOMATSU MASAKI
IPC分类号： C01B33/18 , H01B3/12
摘要： PROBLEM TO BE SOLVED: To provide extremely minute hollow silica particles, and a method for producing the same.SOLUTION: [1] The hollow silica particles have a volume average particle diameter of 0.05-0.45 μm measured with the laser diffraction/scattering method wherein the maximum particle diameter is 5 times of the volume average particle diameter or less, a void ratio is 20-70 vol.%, and a BET specific surface area is less than 30 m/g, and SiOof 98 mass% or more is contained. [2] The method for producing the hollow silica particles includes: a step (I) to prepare an aqueous solution containing a hydrophobic organic compound (a), a quaternary ammonium salt (b), and a silica source (c) to generate a silanol compound with hydrolysis; a step (II) to prepare an aqueous dispersion of core-shell type silica particles having shells composed of silica and the hydrophobic organic compound (a) as cores by stirring the obtained aqueous solution at a temperature of 10-100°C; and a step (III) to obtain the hollow silica particles by separating the obtained core-shell type silica particles and calcining them at a temperature of 950°C or more.
摘要翻译：要解决的问题：提供极微小的中空二氧化硅颗粒及其制造方法。 <1>解决方案：[1]中空二氧化硅颗粒的体积平均粒径为0.05-0.45μm，用激光衍射/散射法测量，其中最大粒径为体积平均粒径的5倍或更小，比例为20-70体积％，BET比表面积小于30微米，SiO 2 98质量％以上。 [2]中空二氧化硅粒子的制造方法包括：制备含有疏水性有机化合物（a），季铵盐（b）和二氧化硅源（c）的水溶液的工序（I），以生成硅烷醇化合物与水解; 通过在10-100℃的温度下搅拌所得水溶液，制备具有由二氧化硅和疏水性有机化合物（a）组成的壳的核 - 壳型二氧化硅颗粒的水分散体的步骤（II）以及通过分离所获得的核 - 壳型二氧化硅颗粒并在950℃以上的温度下煅烧来获得中空二氧化硅颗粒的步骤（III）。版权所有（C）2012，JPO＆INPIT

10. 发明专利

JP2011122097A Coating composition 审中-公开
标题翻译：涂料组合物
公开(公告)号：JP2011122097A
公开(公告)日：2011-06-23
申请号：JP2009281998
申请日：2009-12-11
申请人： Kao Corp , 花王株式会社
发明人： KOMATSU MASAKI , YANO AKIHIRO
IPC分类号： C09D7/12 , C09D5/33 , C09D201/00
摘要： PROBLEM TO BE SOLVED: To provide a coating composition containing a pigment composite body exhibiting a heat-shielding property by selectively reflecting an infrared ray, suppressing reflection of a visible light and facilitating color matching. SOLUTION: The coating composition includes the hollow composite particle, and in the coating composition having an average diameter of the hollow part of 0.1-10 μm, the hollow composite particle includes an outer shell part and the hollow part at the inside of the outer shell part and contains a colored pigment supported on the outer shell part. COPYRIGHT: (C)2011,JPO&INPIT

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